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    Mixed-phase TiO2 nanoparticles preparation using sol-gel method

    , Article Journal of Alloys and Compounds ; Volume 478, Issue 1-2 , 2009 , Pages 586-589 ; 09258388 (ISSN) Mahshid, S ; Askari, M ; Sasani Ghamsari, M ; Afshar, N ; Lahuti, S ; Sharif University of Technology
    2009
    Abstract
    Biphase TiO2 nanoparticles have been prepared by sol-gel method. Water/titanium molar ratio (r) has been used to control the hydrolysis and condensation of titanium isopropoxide in solution producing titanium oxide with two different polymorphs. The influence of crystallite size and morphology of prepared TiO2 on the phase transformation of the resultant materials has been investigated. Synthesized powders were characterized by X-ray diffraction, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Different trends can be observed in the phase transformation and particle growth of the prepared titanium oxide nanomaterial. It was concluded that, the rate of particle...