Sharif Digital Repository

In the present investigation, the mechanical alloying (MA) technique was employed to produce nanocrystalline Al-Ti Powder mixtures. Elemental Al and Ti powders were mixed with different compositions (0, 5, 10, and 20 wt.% Ti) and then, milled in a vibratory mill up to 7 hr. The variations of powder morphology and particle size, apparent and tap densities, microstructure, grain size, lattice strain, and microhardness were studied with increasing the milling time. While dissolution of Ti in the Al matrix resulted to the formation of supersaturated Al-Ti solid solution in the samples containing 5 and 10 wt.% Ti, the specimen with 20 wt.% Ti, eventually, led to nanocomposite powder with... 

In the present investigation, the mechanical alloying (MA) technique was employed to produce nanocrystalline Al-Ti alloys. Elemental Al and Ti powders were mixed with different compositions (0, 5, 10, and 20 wt.% Ti) and then, milled in a planetary ball-mill up to 40 h. The variations of powder morphology and particle size, apparent and tap densities, microstructure, grain size, lattice strain, and microhardness were studied with increasing the milling time. While dissolution of Ti in the Al matrix resulted to the formation of supersaturated Al-Ti solid solution in the samples containing 5 and 10 wt.% Ti, the specimen with 20 wt.% Ti, eventually, led to nanocomposite powder with different... 

Al /Al3Ti in-situ composite have been fabricated by mechanical alloying and two-step hot pressing of powders containing Al and 20%wt Ti. Samples were characterized by using optical microscopy, density measurement, brinel hardness, XRD analysis. An increasing density was observed with increasing pressure until certain pressure and after that the density of composite decreased, which can be attributed to the increase in the level of porosity level and the amount of forming Al3Ti. The samples that hot pressed under cycle 5 and 6, showed the most volume fraction of in-situ phases on the matrix. The wear behavior of Al based composites reinforced with in situ Al3Ti particles has been investigated... 

In this study insitu Al-Al3Ti-Al2O3 nanocomposite has been fabricated based on thermal decomposition of tialite (Al2TiO5) precursor in aluminium matrix through powder metallurgy method. Also the effect of high energy mechanical milling and hot extrusion on this procedure has been investigated. In the first step nano-structured tialite were synthesized through citrate sol gel methods. Then, different volume fraction of tialte was mixed with aluminium by high energy vibratory milling. The results of X-ray differaction analysis, scanning electron microscopy and differential thermal analysis showed that mechanical milling can degrade stability of tialite and cause strain-induced decomposition,... 

The aim of this research was to fabricate an in-situ Al-Al3Ti nanocomposite from pure microsized aluminum and titanium powders by mechanical alloying and hot extrusion without any usage of nanometric particles or applying secondary heat treatments. The focus of the present research was fabricating a nanocomposite material with high strength, modulus and hardness accompanied with high fracture toughness that could be comparable with aluminum alloys in terms of fracture toughness. Mechanical alloying and hot extrusion techniques were employed to produce in-situ fully dense Al-Ti composites. Platenary and high energy vibratiory mill was used to produce composites with different percent of... 

In this study, Al6063-Al203 nanocomposite powders were synthesized by reaction mechanical milling method. Nanometric reinforcement particles were formed via high- energy ball milling under a controlled oxygen containing atmosphere. Morphological and microstructural evolutions of nanocomposite powders were investigated by using X-ray diffraction (XRD), thermal analysis (DTA), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) methods at different milling times. The results showed that mechanical milling stages were accelerated and the time for reaching steady- state condition was decreased by an increase in the oxygen content in the milling atmosphere. The in-situ... 

In this study, Aluminium based nanocomposite with Al3Ti and Al2O3 nanoparticles have been elaborated by mechanical alloying. For this purpose, Al and TiO2 powders have been blended with weight ratios of 10, 20 and 30 percents and were milled using a planetary mill. Morphological variations in different timing periods of mechanical milling process was investigated by Scaning Electron Microscopy (SEM) and The optimal times for alloying were determined for each combination. The pure Aluminium and the powder with 10, 20 and 30%wt reinforcement had coax morphology after respectively for 44, 30, 24 and 14 hours. after studing phase transformations by XRD analysis, the final powders were cold... 

In this study, in situ Al-Al3Ti-Al2O3 nanocomposite has been fabricated on thermal decomposition of tialite (Al2TiO5 or AT) precursor in the aluminum matrix through powder metallurgy method. The high-temperature mechanical property of Al-Al3Ti-Al2O3 on this procedure has been investigated. In the first step nano-structured tialite were synthesized through citrate sol-gel methods. Then 3.5 wt.% tialite powder was mixed with aluminum by high energy vibratory milling for 3 hours. In the next step, green compacts of mechanically milled powder mixtures were sintered at 530°С for 6 hours under argon atmosphere. In the final step, hot extrusion as a consolidation method reduces the sample voids,...