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    Characterization of mechanically alloyed Fe100-xSix and Fe83.5Si13.5Nb3 nanocrystalline powders

    , Article Journal of Materials Processing Technology ; Volume 203, Issue 1-3 , 2008 , Pages 554-560 ; 09240136 (ISSN) Miraghaei, S ; Abachi, P ; Madaah Hosseini, H. R ; Bahrami, A ; Sharif University of Technology
    2008
    Abstract
    In present research, nanocrystalline Fe100-xSix (x = 6.5, 10, 13.5, 20 and 25 at.%) and Fe83.5Si13.5Nb3 alloy powders were prepared by mechanical alloying using high-energy ball milling. The resulting powders mainly consist of micron-sized particles with an average grain size of less than 20 nm. According to the XRD test results, by increasing the milling time and/or the Si content the lattice parameter decreases and the internal microstrain increases. In addition, the specific saturation magnetization diminishes as Si content increases. The coercive forces of the as-milled nanocrystalline powders are much higher than those of corresponding Fe-Si bulk alloys with a minimum at 13.5 at.% Si....