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epinephrine
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Simultaneous Voltammetric Determination of Epinephrine and UricAcid in Presence of Ascorbic Acid Using Pyrolytic Graphite Electrode Modified with Nano- diamond/graphite Film & Voltammetric Determination of Levothyroxine at the Surface of Edge Plane Pyrolytic Graphite Electrode
,
M.Sc. Thesis
Sharif University of Technology
;
Shahrokhian, Saeed
(Supervisor)
Abstract
Part 1: A novel modified pyrolytic graphite electrode with nanodiamond/graphite was fabricated. The electrochemical response characteristics of the modified electrode toward the epinephrine (EN) and uric acid (UA) are studied by means of cyclic and linear sweep voltammetry. The structural morphology and thickness of the film was characterized by SEM technique.The prepared electrode shows an excellent catalytic activity in the electrochemical oxidation of EN and UA, leading to remarkable enhancements in the corresponding peak currents and lowering the peak potentials. The prepared modified electrode acts as a highly sensitive sensor for simultaneous determination of EN and UA in the presence...
, Ph.D. Dissertation Sharif University of Technology ; Shahrokhian, Saeed (Supervisor)
Abstract
In the first part, preparation of different kinds of polypyrrole/carbon composites and their application for drug analysis are described. In the first work, A very sensitive electrochemical sensor constructed from a glassy carbon electrode modified with a layer-by-layer MWCNT/doped overoxidized polypyrrole (oppy/MWCNT /GCE) was used for the determination of acetaminophen (AC) in the presence of codeine and ascorbic acid (AA). In comparison to the bare glassy carbon electrode, a considerable shift in the peak potential together with an increase in the peak current was observed for AC on the surface of oppy/MWCNT/GCE, which can be related to the enlarged microscopic surface area of the...