Loading...
Search for: in-situ-reaction
0.014 seconds

    Preparation of Cu-TiC Nanocomposite and Investigation of Microstructure, physical and Mechanical Properties

    , M.Sc. Thesis Sharif University of Technology Bagheri, Gholamali (Author) ; Pourazarang, Kazem (Supervisor) ; Abachi, Parvin (Co-Advisor)
    Abstract
    In this study, Cu-TiC nanocomposites were produced by high energy ball milling of elemental powders and in situ formation of TiC in the copper base. Cu and 5,10,20 and 40 wt% Ti powder blend were milled for 60 h, then graphite powders were added and milling was continued for 10 h again and Finally Cu-TiC composite powders with 10.68, 20.16, 36.24 and 60.25 vol% of reinforcements (6.18, 12.2, 23.82 and 45.47 wt%) were produced. The effect of time on the solution of titanium in the copper was studied by X-Ray diffraction analysis (XRD). crystallite size and lattice strain of copper were determined 12nm and 1.04% subsequently for Cu-40wt%TiC after 60 h milling. to ensure the formation of... 

    Synthesis of Mg / MgO - Mg2Cu by in-situ Reaction Method and Investigation on Structure and Mechanical Properties

    , M.Sc. Thesis Sharif University of Technology Hemati Kia, Mohammad (Author) ; Abachi, Parvin (Supervisor) ; Salahi, Esmaeil (Supervisor) ; Pour Azarang, Kazem (Co-Advisor)
    Abstract
    In this project formation of MgO & Mg2Cu reinforcement particle in Magnesium matrix was investigated. Firstly Mg & CuO powders mixture in different weight percentage (4, 8%wt CuO) in 20:1 and 30:1 BPR were milled. Finally, according to XRD result 30:1 BPR was selected for milling. Variations in powders morphology, particles size, crystallite size, lattice strain and phase transformation were investigated by X-ray diffraction, scanning electron microscopy and laser particle size analyzer in different milling time. Result showed that during reaction between Mg and CuO, MgO & Mg2Cu reinforcement particles were formed in matrix. Matrix crystallite size was determined about 35-40 nm. Mg-6.3%wt Cu... 

    Comparison of Mechanical Properties of Al-TiB2 Composite in as Cast, Heat Treated and Extruded Condition

    , M.Sc. Thesis Sharif University of Technology Khodabakhsh Pirkalani, Maryam (Author) ; Varahram, Naser (Supervisor) ; Davami, Parviz (Supervisor)
    Abstract
    This research focused on mechanical properties of Al-TiB2 composite in as cast, heat treated and extruded condition. The composites were produced by mixing Al-Ti and Al-B master alloyes. Since some engineering parts during service are supposed to tolerate severe wear conditions, in this research abrasive wear condition was wxamined using pin on disk method. In a fixed load and abrasive disk, composites showed better resistance against wear in comparison with matrix alloy. Furtheremore, T6 heat treatment made composites more resistant against abrasive wear. Finally the best wear resistance was accompolished when composite was extruded and then heat treated. While increase in reinforcement... 

    Control of Formation, Dispersion and Morphology of TiB2 Particles in Al-TiB2 Metal Matrix In-Situ Composite through Optimization of Melt Condition

    , M.Sc. Thesis Sharif University of Technology Khalatbari, Fatemeh (Author) ; Varahram, Naser (Supervisor) ; Davami, Parviz (Co-Advisor)
    Abstract
    A study has been carried out on the formation of TiB2 particles in an aluminum based in-situ metal matrix composite by mixing master alloys containing Ti and B i.e., Al-10Ti and Al-8B with a Ti:B weight ratio of 5:2. It was shown that the microstructure of the composite was greatly affected by the controlling factors of the in-situ reaction like temperature, reaction time and stirring of the melt. An increasing reaction time leads to the dissolusion of the primary phases (AlB2 and Al3Ti) and the increase in TiB2 volume fraction. Optical microscope and SEM images were used to study these changes and XRD analysis was applied to confirm these observations. The act of melt stirring in short... 

    Production of in Situ Cu/NbC Nanocomposites Powders via Mechanical Alloying and Investigation the Mechanical (Wear Resistance) and Physical (Electrical Conductivity) Properties

    , M.Sc. Thesis Sharif University of Technology Gholami Shiri, Sajjad (Author) ; Abachi, Parvin (Supervisor) ; Purazarang, Kazem (Supervisor)
    Abstract
    For application such as electrical contacts and spot welding electrodes, both high electrical conductivity and wear resistance are required. Additionally, such parts should have structural stability at evaluated temperature. Copper based composites containing carbides or oxides reinforcement can be the good choice for production of such parts. In present work, in-situ Cu/NbC composite via mechanical alloying with homogenous distribution of nano reinforcement particle has been produced. For this purpose, in first stage, copper powder was milled with 5, 8, 10 and 12 wt. % of niobium powder in two types of mills, i. e. vibratory dicky mill and planetary ball mill for 5 and 32 h respectively. At... 

    Fabrication of Al Based Nanocomposite with Al2O3 and Al3Ti Reinforcements by Mechanical Milling and Press and Sintering (In situ method) and Investigation of Its Wear Behavior

    , M.Sc. Thesis Sharif University of Technology Shabani Nezhad, Parisa (Author) ; Seyed Reihani, M (Supervisor)
    Abstract
    In this study, Aluminium based nanocomposite with Al3Ti and Al2O3 nanoparticles have been elaborated by mechanical alloying. For this purpose, Al and TiO2 powders have been blended with weight ratios of 10, 20 and 30 percents and were milled using a planetary mill. Morphological variations in different timing periods of mechanical milling process was investigated by Scaning Electron Microscopy (SEM) and The optimal times for alloying were determined for each combination. The pure Aluminium and the powder with 10, 20 and 30%wt reinforcement had coax morphology after respectively for 44, 30, 24 and 14 hours. after studing phase transformations by XRD analysis, the final powders were cold... 

    The effect of nano-TiO2 additions on the densification and mechanical properties of SiC-matrix composite

    , Article Ceramics International ; Volume 46, Issue 5 , April , 2020 , Pages 6477-6483 Khodaei, M ; Yaghobizadeh, O ; Baharvandi, H. R ; Alipour Shahraki, A ; Mohammadi, H ; Sharif University of Technology
    Elsevier Ltd  2020
    Abstract
    This research studied the effect of adding TiO2 nanoparticles along with Al2O3 and Y2O3 additives on the physical and mechanical properties of a SiC-matrix composite. The samples were fabricated through a pressureless process at 1900 °C. The results showed that the addition of TiO2 nanoparticles up to 4.5 wt% inhibited the excessive growth of SiC grains. According to the investigations, the microstructure and final properties of composites were affected by density, synthesized phases as well as their distribution in the matrix, and grain size. The highest density, Young's modulus, hardness, indentation fracture resistance, and flexural strength, alongside with the lowest brittleness index...