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    Analysis of Iranian rosemary essential oil: Application of gas chromatography-mass spectrometry combined with chemometrics

    , Article Journal of Chromatography A ; Volume 1218, Issue 18 , May , 2011 , Pages 2569-2576 ; 00219673 (ISSN) Jalali Heravi, M ; Moazeni, R. S ; Sereshti, H ; Sharif University of Technology
    Abstract
    This paper focuses on characterization of the components of Iranian rosemary essential oil using gas chromatography-mass spectrometry (GC-MS). Multivariate curve resolution (MCR) approach was used to overcome the problem of background, baseline offset and overlapping/embedded peaks in GC-MS. The analysis of GC-MS data revealed that sixty eight components exist in the rosemary essential oil. However, with the help of MCR this number was extended to ninety nine components with concentrations higher than 0.01%, which accounts for 98.23% of the total relative content of the rosemary essential oil. The most important constituents of the Iranian rosemary are 1,8-cineole (23.47%), α-pinene... 

    Determination of essential oil components of artemisia haussknechtii boiss. using simultaneous hydrodistillation-static headspace liquid phase microextraction-gas chromatography mass spectrometry

    , Article Journal of Chromatography A ; Volume 1160, Issue 1-2 , 2007 , Pages 81-89 ; 00219673 (ISSN) Jalali Heravi, M ; Sereshti, H ; Sharif University of Technology
    2007
    Abstract
    A novel method for extraction and analysis of volatile compounds of Artemisia haussknechtii Boiss., using simultaneous hydro-distillation and static headspace liquid microextraction followed by gas chromatography-mass spectrometry (SHD-SHLPME-GCMS) is developed. SHLPME parameters including nature of extracting solvent, headspace volume and design, extraction time, sample weight and microdrop volume were optimized. Comparison of hydro-distillation gas chromatography-mass spectrometry and HD-SHLPME-GCMS showed that the latter method is fast, simple, inexpensive and effective for the analysis of volatile compounds of aromatic plants. By using this method, 56 compounds were extracted and...