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    Synthesis and Analysis of Nanoparticles by Electrical Arc Discharge in Liquid Nitrogen

    , M.Sc. Thesis Sharif University of Technology gholami, Zainab (Author) ; Irajizad, Azam (Supervisor) ; Ahadian, Mohammad Mahdi (Supervisor)
    Abstract
    Electrical arc discharge in ambient air, vacuum, reactive gas and other environment is an appropriate method for synthesis of different nanostructures. This method can provide stable and ultra pure nanostructures with diverse applications. In this research we focus on synthesis and analysis of titanium nitride nanoparticles in liquid nitrogen(lack of oxygen)by Electrical arc discharge . At the beginning a reactor for the electrical arc discharge process designed and implemented. Titanium nanoparticles have synthesis by this method analyzed. Several characterization techniques such as X-ray diffraction (XRD), dynamic light scattering (DLS), X-ray photo electron spectroscopy (XPS), scanning... 

    Synthesis and Characterization of Nano-photocatalytic Metal Oxide / Graphene Using arc Discharge in Liquid

    , M.Sc. Thesis Sharif University of Technology Shojaee, Vahid (Author) ; Iraji Zad, Azam (Supervisor) ; Ahadian, Mohammad Mahdi (Supervisor)
    Abstract
    In this thesis, graphene/titanium oxide and graphene/tungsten oxide composites were synthesized using arc discharge in liquid and their photocatalytic behavior was studied. Based on physical principles of the arc discharge in liquid, geometry of point-point was used for metallic Ti and W electrodes. TiO2 and WO3 nanoparticles and their nanocomposites with graphene and graphene oxide (GO) were studies using DLS, UV-vis, PL, ICP, FTIR, XRD, Raman and TEM characterization. The concentration of aqueous solution of Rhodamine B mixed with graphene/WO3 and GO/WO3 composites and WO3 nanoparticles under ultraviolet light was measured versus time and reached to 0.1, 0.6 and 0.6 of the initial value... 

    Synthesis and Optical Properties of Titanium Nitride Nanoparticles Prepared by Arc Discharge Method in Liquid Nitrogen

    , M.Sc. Thesis Sharif University of Technology Shabani, Alireza (Author) ; Irajizad, Azam (Supervisor) ; Ahmadian, Mohammad Mehdi (Supervisor)
    Abstract
    Production of nano-particles using arc-discharge method in a liquid nitrogen environment is a proficient way of forming nitride Particles whose formation by other methods is difficult and expensive. Amongstall, Titanium nitride (TiN) is of significant importance because of its high formidability and its optical and electrical metal properties due to plasmonic electrons. This research studies the production of titanium nitride Nano-particles using arc-discharge method and investigates optical properties and features, specially dielectric constant and optical extinction coefficient. Modeling interband Transitions is also discussed to revise Drude's electron theory. First, in experimental... 

    Excitation current optimization of fluxgate magnetometers for active magnetic shielding of SQUID-based magnetocardiography system

    , Article Journal of Superconductivity and Novel Magnetism ; Volume 30, Issue 8 , 2017 , Pages 2323-2328 ; 15571939 (ISSN) Shanehsazzadeh, F ; Kalantari, N ; Jabbari, T ; Fardmanesh, M ; Sharif University of Technology
    Abstract
    In order to achieve stable operation for a developed high-Tc SQUID-based magnetocardiography system, a two-stage active magnetic shielding technique is implemented. This technique is based on a combination of fluxgate and high-Tc SQUID magnetometers feedback loops. While two YBCO rf SQUIDs in a gradiometric configuration are used at liquid Nitrogen temperature as the main sensors for the heart signal detection and low-amplitude noise signals cancellation in one stage, a fluxgate is used to cancel large far-field environmental noise in the other stage feedback loop. The fluxgate sensors working in the fundamental mode under the optimized bias conditions have white noise levels less than 10... 

    Failure analysis of holding yokes made of investment cast 17-4 PH stainless steel

    , Article Engineering Failure Analysis ; Volume 18, Issue 4 , 2011 , Pages 1242-1246 ; 13506307 (ISSN) Etemadi, A. R ; Behjati, P ; Emami, A ; Motiei, S. M. A. D ; Mirsaeedi, S ; Sharif University of Technology
    2011
    Abstract
    Holding yokes made of investment cast 17-4PH stainless steel were too soft (below 20. HRC). Optical microscopy of the parts showed that there is a high fraction of retained austenite after oil quench due to high amount of molybdenum found in parts as an impurity. Subzero treatment in liquid nitrogen after solution heat treating was used to convert retained austenite to martensite but parts became too brittle and fractured during post-heat treating machining. Double and triple aging at 538 °C (1000 °F) after subzero cooling was done on parts. Detailed fractography and tensile testing along with optical microscopy (OM) investigation proved that repeated aging at 538 °C (1000 °F) led to lower... 

    Excitation current optimization of fluxgate magnetometers for active magnetic shielding of SQUID-Based magnetocardiography system

    , Article Journal of Superconductivity and Novel Magnetism ; 2016 , Pages 1-6 ; 15571939 (ISSN) Shanehsazzadeh, F ; Kalantari, N ; Jabbari, T ; Fardmanesh, M ; Sharif University of Technology
    Springer New York LLC 
    Abstract
    In order to achieve stable operation for a developed high-Tc SQUID-based magnetocardiography system, a two-stage active magnetic shielding technique is implemented. This technique is based on a combination of fluxgate and high-Tc SQUID magnetometers feedback loops. While two YBCO rf SQUIDs in a gradiometric configuration are used at liquid Nitrogen temperature as the main sensors for the heart signal detection and low-amplitude noise signals cancellation in one stage, a fluxgate is used to cancel large far-field environmental noise in the other stage feedback loop. The fluxgate sensors working in the fundamental mode under the optimized bias conditions have white noise levels less than 10... 

    Through-space electronic communication of zinc phthalocyanine with substituted [60]Fullerene bearing O2Nxaza-crown macrocyclic ligands

    , Article Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy ; Volume 171 , 2017 , Pages 330-339 ; 13861425 (ISSN) Ghanbari, B ; Shahhoseini, L ; Mahlooji, N ; Gholamnezhad, P ; Taheri Rizi, Z ; Sharif University of Technology
    Elsevier B.V  2017
    Abstract
    Two new macrocyclic ligands containing 17- and 19-membered O2N3-donor aza-crowns anchored to [60]Fullerene were synthesized and characterized by employing HPLC, electrospray ionization mass (ESI-MS), 1H and 13C NMR, UV–vis, IR spectroscopies, as well as powder X-ray diffraction (PXRD) and thermogravimetric analysis (TGA) in solid state. TGA measurements revealed that upon linking each of these macrocycle rings to [60]Fullerene, the decomposition point measured for [60]Fullerene moiety was increased, indicating on the promoted stability of [60]Fullerene backbone during binding to these macrocyclic ligands. Moreover, the ground state non-covalent interactions of [60]Fullerene derivatives of... 

    HTS transformer’s partial discharges raised by floating particles and nitrogen bubbles

    , Article Journal of Superconductivity and Novel Magnetism ; Volume 33, Issue 10 , 6 July , 2020 , Pages 3027-3034 Moradnouri, A ; Vakilian, M ; Hekmati, A ; Fardmanesh, M ; Sharif University of Technology
    Springer  2020
    Abstract
    Presence of defects, conducting particles, nonconducting particles, and nitrogen gas bubbles in the insulation system of high-temperature superconducting (HTS) transformers, mainly inside the liquid nitrogen as its major insulation, can create local field enhancement and consequently partial discharges which eventually lead to the catastrophic failure of the transformer. In this paper, two-dimensional (2D) axisymmetric finite element method (FEM) modeling via COMSOL Multiphysics software has been utilized for the investigation of the impact of size and shape of conducting particles and nitrogen gas bubbles on partial discharge (PD) activities in liquid nitrogen. Conducting particles of... 

    Two phase gas-liquid bubbly flow modeling in vertical mini pipe

    , Article 2010 14th International Heat Transfer Conference, IHTC 14, 8 August 2010 through 13 August 2010 ; Volume 3 , 2010 , Pages 947-956 ; 9780791849385 (ISBN) Kebriaee, M. H ; Karabi, H ; Khorsandi, S ; Saidi, M. H ; Heat Transfer Division ; Sharif University of Technology
    Abstract
    Studies on two-phase flow in small scale pipes have become more important, because of the application of mini-scale devices in several engineering fields including, high heat-flux compact heat exchangers, and cooling systems of various types of equipment. In a mini pipe the behavior of two phase flow is not the same as flow in conventional pipes. The difference is caused by different effective forces; for e. g. inside a mini pipe capillary forces are more important in comparison with gravitational forces. This paper is devoted to numerical simulation of gas-liquid two phase flow in a vertical mini pipe. Prediction of bubble shape and the effects of gas and liquid velocities on flow... 

    Intralesional immunotherapy compared to cryotherapy in the treatment of warts

    , Article International Journal of Dermatology ; Volume 56, Issue 4 , 2017 , Pages 474-478 ; 00119059 (ISSN) Khozeimeh, F ; Jabbari Azad, F ; Mahboubi Oskouei, Y ; Jafari, M ; Tehranian, S ; Alizadehsani, R ; Layegh, P ; Sharif University of Technology
    Blackwell Publishing Ltd  2017
    Abstract
    Background: Warts are the most common clinical manifestation of the human papilloma-virus infection in the skin and mucous membranes. In spite of the various therapeutic modalities for nongenital skin warts, there is still no single method to be used as an approved treatment. In this study, we compared the efficacy of immunotherapy and cryotherapy on wart lesions. Methods: Sixty patients with verruca vulgaris and plantar warts were randomly divided into two groups. One group received intralesional injection of candida antigen repeated every 3 weeks until complete improvement of all warts or for a maximum of three sessions. The second group was treated by cryotherapy with liquid nitrogen for... 

    An expert system for selecting wart treatment method

    , Article Computers in Biology and Medicine ; Volume 81 , 2017 , Pages 167-175 ; 00104825 (ISSN) Khozeimeh, F ; Alizadehsani, R ; Roshanzamir, M ; Khosravi, A ; Layegh, P ; Nahavandi, S ; Sharif University of Technology
    Elsevier Ltd  2017
    Abstract
    As benign tumors, warts are made through the mediation of Human Papillomavirus (HPV) and may grow on all parts of body, especially hands and feet. There are several treatment methods for this illness. However, none of them can heal all patients. Consequently, physicians are looking for more effective and customized treatments for each patient. They are endeavoring to discover which treatments have better impacts on a particular patient. The aim of this study is to identify the appropriate treatment for two common types of warts (plantar and common) and to predict the responses of two of the best methods (immunotherapy and cryotherapy) to the treatment. As an original work, the study was...