Sharif Digital Repository

Hydroxyapatite (HA) coatings in and onto anodized TiO2 nanotube arrays were presented and prepared by electrophoretic deposition technique (EPD). Coatings were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). EPD proved to be an innovative and versatile technique to coat HA on and into nanotubular structures of TiO2 with enhanced adhesion between nanotubes and HA particles provided by mechanical interlocking. After EPD of HA on TiO2 layer, samples were sintered at 400 °C, 600 °C and 800 °C for 2 h in an Ar atmosphere. Effect of EPD processing parameters on thickness of the deposits and rate of deposition was elucidated for HA coatings on the nanotubular TiO2... 

This paper examines the use of pre-fabricated interlocking arms/threading in enhancing the strength of friction stir spot welded hybrid joints of AA2219/PP-C30S polypropylene polymer by varying parameter combination. The process involves the fabrication of a pre-threaded hole on the Al alloy prior to the joining process, and the threading/crest-pitch profile aids mechanical interlocking. The peak temperature, crest-pitch interlocked profiles, microstructural and mechanical properties of the joints were examined. The results show that an increase in the tool rotational speed increases the thickness of the reaction layer (between the Al and the polymer substrates), the shear-tensile load... 

Structural, microstructural and mechanical properties in roll bonding of AA5052 and polypropylene sheets have been evaluated in this study. The surface roughness of the AA5052 sheets, rolling temperature and the surface energy of polymer were selected as the bonding variables. The findings indicated that an increase in the surface energy of polypropylene by grafting maleic anhydride would result in higher bonding strength due to chemical interaction between the AA5052 and the maleic anhydride grafted polypropylene (PP-g-MAH). In fact, this reaction caused the formation of an interphase layer at the polymer side of the interface and the diffusion of aluminum into the PP-g-MAH layer. It was... 

Structural, microstructural and mechanical properties in roll bonding of AA5052 and polypropylene sheets have been evaluated in this study. The surface roughness of the AA5052 sheets, rolling temperature and the surface energy of polymer were selected as the bonding variables. The findings indicated that an increase in the surface energy of polypropylene by grafting maleic anhydride would result in higher bonding strength due to chemical interaction between the AA5052 and the maleic anhydride grafted polypropylene (PP-g-MAH). In fact, this reaction caused the formation of an interphase layer at the polymer side of the interface and the diffusion of aluminum into the PP-g-MAH layer. It was... 

In this study, friction stir soldering (FSS) as an emerging joining process with the aid of a preliminary electroplating process was utilized for the first time to fabricate graphite-copper lap joints aimed at investigation of rotational speed influence on joint interface microstructure and mechanical behaviour. To do so, an Sn-37Pb solder foil was placed between a copper sheet and a copper-coated graphite substrate after which a rotating pin-free tool was plunged into the copper sheet and allowed to travel along the joint. Results indicated that adhesive strength between the electroplated copper coating and graphite substrate was strongly affected by surface roughness and plating current... 

Process optimization to prepare T-joints of poly methyl methacrylate (PMMA) and AA5754 alloy by friction stir welding (FSW) was performed. Effects of processing parameters including tool rotational velocity, traverse speed, tilt angle and plunge depth (TP) were studied. The material flow and formation of interaction layer upon FSW were evaluated and the tensile strength and hardness of the joints were examined. It is shown that by controlling the heat input into stir zone through increasing the rotational velocity or decreasing travelling speed, less defects are formed while the thickness of the interaction layer increases. The optimum condition is attained at 1600 rpm/30 mm min−1 with a... 

In this study, evolution of intermetallic layer of the cold roll bonded bilayer of Aluminum-Steel sheets, during severe plastic deformation (SPD) followed by annealing has been investigated. The effect of such evolution on mechanical properties has been discussed. For this purpose, Constrained Groove Pressing (CGP) was used as a SPD process. Field emission scanning electron microscope equipped with energy dispersive spectroscopy and optical microscopy were used for examination of intermetallic compounds morphology and composition. Meanwhile, tensile properties of the bilayer sheets were evaluated. According to microstructural observations, continuous intermetallic layer was formed during... 

In this research, the feasibility of friction-stir welding (FSW) for dissimilar lap-joining of an aluminium-magnesium alloy (AA5058) and poly-methyl-methacrylate sheets to attain sound and defect-free joints was examined. The inter-mixing flow patterns between the metal and polymer counterparts during FSW were predicted by employing three-dimensional finite element models. It is shown that the bonding mechanism between the dissimilar materials is mechanical interlocking at the interface which controls the joint strength depending on the processing parameters. The most suitable dissimilar lap-joining regarding microstructural soundness is attained at w= 1600 rev min−1 and v = 25 mm min−1....