Sharif Digital Repository

This article presents results of an investigation on age-hardening behavior of superalloy AEREX 350. Microhardness testing was employed to evaluate the age-hardening response of the alloy while optical, scanning, and transmission electron microscopy techniques were used to characterize the major phases formed during the aging process. No significant hardening was found in solution-treated samples aged at temperatures up to about 680 °C. Aging at 700 °C up to 950 °C, however, caused a characteristic hardening response. This hardening was concurrent with the formation of γ', an ordered phase with L12 structure, as fine precipitate distributed throughout the fcc matrix. In the temperature range... 

In this work, the influence of the clearance and post-braze heat treatment on the microstructure of 4130 steel joint brazed by BNi-4 filler metal was investigated. Samples with different clearances were heated to 1100°C and hold for 9 min. Then, some were reheated to 800°C(2hr) and 800°C(2hr)+1000°C(2hr), cycle 1 and cycle 2, respectively. Microscopy techniques and micro-hardness test were used to evaluate the microstructures. Results suggested that in this case 25μm clearance can be considered as the optimum value. Also, it was found that high temperature post-braze heat treatment can be applied as a useful technique for decreasing the fraction of the brittle phases at the joint main body  

The cast-decant-cast is a new method for the preparation of the functionally graded components that has been developed in recent years. The functionally graded cylindrical shape component with a radial gradient, e.g. the first alloy (A390) with high wear resistance on the surface of the piece and toughness and the second alloy (A356) of low machining costs in the core of the piece can be produced via this melt process. The effect of the second alloy superheat at temperatures of 750, 820 and 860 °C as well as the effect of the first alloy solidified layer at 25, 35 and 45 s decanting time on achieving the perfect interface between the two alloys was investigated. The characterization of the... 

Utilizing the Finite Element Method (FEM), the strain field in the radial forging process of tube is calculated at different process conditions and compared with the experimental results achieved using the microhardness test. The effect of various process parameters such as friction, axial feed, back push and front pull forces and die angles on the strain field are investigated. Using the results of the analysis, it is shown that the deformation inhomogeneity, introduced by an Inhomogeneity Factor (IF), is maximum in the inner zone of tube, while the minimum and the maximum effective strains are appeared at the inner zone of tube and about the core of the tube thickness, respectively. Also,... 

NiTi alloys have exhibited significant potential as a matrix of wear resistant composites. In this study, in order to examine the effect of starting materials on the wear performance of NiTi-based composites, both elemental Ni/Ti and prealloyed NiTi powders were used to fabricate NiTi-6wt% nano-Al2O3 composites using hot isostatic pressing (HIP). Nanoindentation and microhardness test results indicate that the composite samples produced from the elemental Ni/Ti powders exhibited higher hardness and lower pseudoelasticity properties than those of the samples fabricated from the prealloyed NiTi powders; this is attributed to the higher amount of... 

Natural aging behavior of the aluminum 6061 alloy after a novel Severe Plastic Deformation process called Tube Channel Pressing (TCP) was studied. For this purpose, Vickers microhardness test was used to investigate the changes of mechanical properties while TEM and XRD observations were utilized in order to characterize microstructural evolution during natural aging. Results show that Si-enriched precipitates appear and coarsen rapidly in the first few days of natural aging of TCPed aluminum 6061 alloy which causes consecutive increase and decrease of Vickers microhardness, respectively. Similarly, other alloying elements such as Cu and Fe lead to formation of coarse precipitates during... 

Semisolid stir joining of AZ91 alloy was investigated by using mechanical stirring and Mg-25. wt%Zn interlayer. A 2. mm-thick interlayer was located between two 7.5. mm-thick AZ91 pieces. Then, they were heated to 530. °C, the semisolid temperature of both base metal and interlayer. A stirrer with a rotational speed of 1600. rpm was introduced into the weld seam. Optical microscopic and scanning electron microscope (SEM) investigation, microhardness test, shear punch test (SPT), and three points bending test were carried out to assess the properties of the joint. Results showed three distinctive zones: stir zone (SZ), compacted zone (CZ), and diffusional-mechanical affected zone (DMAZ). SEM... 

An experimental study of wear characteristics of electroless Ni-10% P coating sliding against hard AISI 52100 steel pin is investigated. Experiments are carried out at room and 550°C temperatures. Heat treatment effects on tribological behavior of this coating are studied. The wear surface and the microstructure of the coatings are analyzed using optical microscopy, scanning electron microscopy, energy dispersion analysis X-ray, and microhardness testing equipment. It is observed that the forming of continuous oxide film on contacting surfaces of pin and disk improves wear resistance and decreases friction coefficient of the Ni-10% P coating. The results indicate that the wear resistance of... 

In this study, Al-20Si-5Fe-3Cu-1Mg-XMn (X=0,1.5,3) alloys were synthesized by the gas atomizing technique. The microstructure and mechanical properties of the powders were investigated using optical microscopy, scanning electron microscopy, X-ray diffractometery method, and microhardness test. Microstructure of the powders composed of α-Al, Si and iron intermetallic compounds. As the powder particle size decreases, the phases become finer. A significant refinement in the size of iron-containing compounds was observed by addition of Mn. The microstructural refinement by controlling the particle size leads to an increase in the hardness of the powder particles in the amount of 33-45% dependent... 

Al-1100/St-12 aluminum clad steel sheets were produced using roll bonding process at different reductions in thickness and with various supplemental annealing treatments. Experiments were conducted by applying the Taguchi method to obtain optimum condition for maximizing the joint strength. The joint strengths of the bi-layer sheets were evaluated by peel test. The Al/Fe intermetallic phases at the joint interface and the peeled surfaces were examined using scanning electron microscopy (SEM). Energy dispersive spectroscopy (EDS) and Vickers microhardness test were performed to characterize the intermetallic compounds. The results indicate that at the optimum condition of 0.50 reduction in... 

The as-cast FSX-414 Co-based superalloy samples were solution treated at 1150°C for 4h and then aged at 980°C for 4h. Specimens for joining were cut from the as-cast ingot and TLP bonding carried out at the same conditions as for the solution and solution+aging treatment, using MBF-30 interlayer. Microstructures were studied for as-cast, heat treated and TLP bonded specimens. These studies showed that the ununiform distributed carbides of MC type in the as-cast specimens replaced by M23C6 type carbides with uniform distribution in the heat treated microstructure. Due to complete isothermal solidification, no eutectic structure in the bond region were wasobserved, but some intermetallics in... 

Effects of the zinc, copper and brass interlayers were studied on the microstructure evolution and mechanical properties of the wrought aluminum friction stir welds. Optical and scanning electron microscopes (SEM) as well as X-ray diffraction (XRD) analysis were used for investigation of the distribution, dissolution and reactions of the interlayers, grain structure in the stir zone and fracture surfaces. Longitudinal and transverse tensile and microhardness tests were also carried out in order to evaluate the mechanical properties of the welds. The results showed that without insertion of the interlayer, the joint efficiency (ratio of the weld strength to the aluminum base metal strength)... 

This study aimed to investigate the changes in crystalline structure and resistance to demineralization of human dental surface enamel treated with erbium-doped yttrium aluminium garnet laser (Er:YAG) laser and fluoride. The enamel surfaces were divided into four groups according to the treatment process including, (L): irradiated with Er:YAG; (F): treated with acidulated phosphate fluoride gel (LF): Pre-irradiated surfaces with Er:YAG subjected to acidulated phosphate fluoride gel and (FL): laser irradiation was performed on the fluoridated enamel surface. Before and after the treatment procedure, the samples were evaluated using X-ray diffraction, scanning electron microscope (SEM) and the... 

Al-1050 clad St-12 sheets were first produced by cold roll bonding process with clad layer thickness of 350 and 1000 μm. Then, Al-5052 aluminum alloy and Al-1050/St-12 sheets were lap joined using gas tungsten arc welding with Al–Si filler metal. The effects of the clad layer thickness and welding current were studied on the joint properties. Macro/microstructural observations were done using optical and scanning electron microscopes (SEM) equipped with energy dispersive spectroscopy (EDS). Shear-tensile and microhardness tests were used for evaluation of the mechanical behavior of the joint. The results indicated that presence of the aluminum clad layer reduced the Al–Fe intermetallic... 

In this work, nanocrystalline Al6063 composite powder reinforced with nanometric oxide ceramic particles was synthesized via an in situ solid-gas reaction during high-energy mechanical alloying under a mixture of argon-oxygen atmosphere. The effect of oxygen volume fraction on the morphological evolution and microstructural changes during mechanical alloying was studied by various analytical techniques including optical and electron microscopy, X-ray diffraction, laser particle size analysis, apparent density measurement, and microhardness test. The reactive mechanical alloying resulted in the formation of amorphous Al- and Al-Mg-Si-Fe oxides with a size range of 40-100. nm and volume...