Sharif Digital Repository

In this paper, the advantages of numerical simulation to improve the process of copper electroforming are demonstrated. In this regard, the finite element model of copper electroforming for a rotating cone electrode was first prepared and then, the effect of the key parameters, such as applied current density, solution conductivity, electrode spacing, and anode height, on the uniformity of the thickness was investigated. The model combines tertiary current distribution with Bulter–Volmer electrode kinetics and computational fluid dynamics at the turbulent condition. In order to validate the model, a cone-shaped shell was produced by electroforming method in the laboratory. The obtained... 

The nanocomposite Cu–Cr powder was consolidated by flash spark plasma sintering (FSPS), which involves applying an extremely rapid change in the electrical power passing through the bulk of the sample. It was demonstrated that an essentially fully dense material could be obtained in 15 s. Such short-term treatment typically preserves the nanostructured features of the material. However, investigation revealed a nonuniformity in the microstructure of the alloys obtained under such extreme conditions. To better understand the observed effects, the FSPS process was simulated. It was observed that a rapid change in the applied electrical power resulted in nonuniform distributions of current... 

Commercially pure aluminum sheets, AA 1050, are processed by accumulative roll bonding (ARB) up to eight cycles to achieve ultrafine-grained (UFG) aluminum as primary material for mechanical testing. Optical microscopy and electron backscattering diffraction analysis are used for microstructural analysis of the processed sheets. Strain rate sensitivity (m-value) of the specimens is measured over a wide range of strain rates by stress relaxation test under plane strain compression. It is shown that the flow stress activation volume is reduced by decrease of the grain size. This reduction which follows a linear relation for UFG specimens, is thought to enhance the required effective (or... 

Semisolid stir joining has been under deliberation as a possible method for joining of copper alloys. In this study, the effect of temperature and rotational speed of stirrer on macrostructure evaluation and mechanical properties of samples were investigated. Optical microscopy and X-ray diffraction were performed for macro and microstructural analysis. A uniform micro-hardness profile was attained by semisolid stir joining method. The ultimate shear strength and bending strength of welded samples were improved in comparison with the cast sample. There is also lower area porosity in welded samples than the cast metal. The mechanical properties were improved by increasing temperature and... 

The high hydration potential of CaO and MgO phases restricted the application of Mag-Dol refractory composites. In this study, the impact of nano-silica (SiO2) addition on the physical, mechanical, thermo-mechanical as well as microstructure of Mag-Dol refractory composites is investigated. Mag-Dol compositions were prepared by using calcined dolomite and magnesite particles (micron, 0–1, 1–3, 3–5, and 5–8 mm), liquid resin, and 0, 0.5, 1, 1.5, 2, and 2.5 wt% nano SiO2 as additives. Specimens were heated up to 1650 °C for the 3 h soaking period. Fired specimens were characterized by physical (apparent porosity, bulk density, and hydration resistance), mechanical (cold crushing strength), and... 

This research focuses on simulation of the dissimilar materials’ welding, stainless steel and mild steel, using finite element and experiment to enhance the method and better understand the transient temperature profiles and the stress distribution in a cladded pipe. The microstructural come as fenestrated and the computer results show that the temperature distribution in the modelled pipe is a function of the thermal conductivity of each weld metal as well as the distance away from the heat source. © 2018, International Association of Engineers. All rights reserved  

In this paper, two types of carbon black (CB) masterbatch with different carriers, i.e. HDPE and LDPE, are used to produce black compounds using three PE100 resins with various short chain branching distributions. Due to difference in short chain branch (SCB) distribution, the used polyethylene resins behave differently in microstructure development and long-term creep behavior. The microstructural analysis using different DSC techniques and rheological measurements revealed more sensitivity of the polyethylene resin with uniform comonomer distribution to the carbon black aggregates and their polymeric carriers. The Full Notched Creep Test (FNCT) was performed to determine the long-term... 

Herein, the effect of electrodeposition time on the super-capacitive performance of three-dimensional (3D) MnO2/g-C3N4 heterostructured electrodes was investigated. MnO2 nanoparticles were electrodeposited on the g-C3N4 nanosheets drop-casted on the Ni foam substrate. The microstructural analysis, carried out by FE-SEM and TEM, confirmed the homogeneous distribution of MnO2 nanoparticles on g-C3N4 nano-sheet layers. The electrochemical capacitive performances of the MnO2/g-C3N4 electrodes were evaluated by cyclic voltammetry (CV), galvanostatic charge/discharge tests, and electrochemical impedance spectra (EIS). The obtained results suggested that the supercapacitor (SC) performance of all... 

In the present study, 30MSV6 microalloyed steel was heat treated under different conditions, and the relation between its microstructure and mechanical properties was investigated. Scanning electron microscopy and transmission electron microscopy were used to characterize the microstructure of the heat-treated steel, and the effect of microstructure on tensile strength and fatigue behavior was determined. Microstructural analysis indicated that precipitates were formed at different sites such as grain boundaries and sub-grain boundaries. Furthermore, microstructural studies accompanied by the evaluation of mechanical properties revealed that the optimal heat treatment cycle of 30MSV6... 

In this research, the effects of nano-sized MgO in Al2O 3-SiC composites were investigated. The overall changes in the density and mechanical properties of sintered samples (hardness, bending strength and toughness) were evaluated. After mixing, drying and uniaxial compaction of the powders, they were first heat-treated at low temperature in an electric furnace to remove any residuals. They were then heat-treated at high temperature (1700 °C) inside a graphite furnace in argon atmosphere for sintering (at normal and high pressure). The content of MgO in the Al 2O3-10 vol% SiC composite was 0, 500, 1000, and 1500 ppm. Thefracture toughness(KIC)of sintered composite with 10... 

In this paper, the failure of the reformer furnace tube, made of HP-Nb micro alloyed heat resistant steel is investigated. The failure was due to a longitudinal crack developing in the circumferential weld joint close to the outlet end of the tube, where the mean wall temperature had reached the highest value during service. According to the temperature records during the period of 7 years of being in service, the tube had experienced temperatures higher than the tubes designed temperature. This situation besides the occurrence of several sudden shutdowns caused the mechanical properties degradation.Macroscopic and microscopic examinations revealed that the failure had occurred due to the... 

In this study, a multi-scale model is proposed to assess softening kinetics and microstructural changes during isothermal annealing within an aluminum alloy. In the first stage, an elastic-plastic finite element analysis is performed for computing the distributions of effective plastic strain and stress while the stored energy after cold rolling is defined based on the predicted data and then utilized for generation of the initial conditions in the microstructural analysis. In the next stage, an algorithm based on cellular automata coupled with a first order rate equation is used to determine the progress of softening behavior at elevated temperatures while both recrystallization and... 

Mechanical properties and microstructural analysis of Expanded Perlite Aggregate (EPA) concretes are presented. Using 10% EPA, the effects of using various types of fibre were investigated. For all specimens, fibrous and non-fibrous, the compressive and the splitting tensile strengths were obtained. Complete stress–strain curves for fibre-reinforced specimens were obtained. A new index for representing the toughness of fibre-reinforced Perlite concretes is introduced. The addition of fibres substantially increased the splitting tensile strength. Steel fibres with “indentations” had the best performance in this regard. Regarding the toughness, specimens with “hooked” steel fibres performed... 

There are many engineering applications in which composite materials are required to satisfy two or more criteria regarding physical and mechanical properties. In this article, Al-matrix nanocomposites reinforced with different volume fractions of SiC nanoparticles (~ 50 nm; up to 6%) were processed by powder metallurgy (P/M) routes through mechanical milling and hot consolidation techniques. Microstructural studies showed that nano-metric Al2O3 particles with a size of ~ 20 nm and volume fraction of ~ 2% were formed and distributed in the metal matrix, owing to the surface oxides breaking. Microstructural analysis also revealed that the size of cellular structure and the density of... 

This work presents the catalytic graphitization process of phenolic resins (PR's) by addition of in situ nano-Fe particles as catalyst. Pyrolysis treatments of prepared compositions including various contents of nano-Fe particles were carried out at 600–1200 °C for 3 h under reducing atmosphere and graphitization process were evaluated by different techniques such as X-Ray diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM), High Resolution Transmission Electron Microscopy (HRTEM), Simultaneous Thermal Analysis (STA) and Raman spectroscopy that mainly performed to identify the phase and microstructural analysis, oxidation resistance and extend of graphitized carbon... 

Mechanical properties and microstructural analysis of Expanded Perlite Aggregate (EPA) concretes are presented. Using 10% EPA, the effects of using various types of fibre were investigated. For all specimens, fibrous and non-fibrous, the compressive and the splitting tensile strengths were obtained. Complete stress–strain curves for fibre-reinforced specimens were obtained. A new index for representing the toughness of fibre-reinforced Perlite concretes is introduced. The addition of fibres substantially increased the splitting tensile strength. Steel fibres with “indentations” had the best performance in this regard. Regarding the toughness, specimens with “hooked” steel fibres performed... 

The friction stir welding of AA2024-T6 to AA6061-T6 plates with a 4 mm thickness has been studied at constant traverse and rotational speeds of 1000 rpm and 100 mm/min, respectively. The position of alloys and the effects of precipitation hardening heat treatment in retreating and advancing side in the friction stir welding were analyzed. The tool with taper threaded pin was used for welding. Macro and microstructural analysis were investigated by using Optical and Field Emission-Scanning Electron Microscopes (FE-SEM) to check out the welded joints. Micro-hardness and Tensile tests were also done to study mechanical attributes of the joints. Microstructural analysis revealed some grain... 

Electro Discharge Machining (EDM) can be an element of a sustainable manufacturing system. In the present study, the sustainability implications of EDM of special-purpose steels are investigated. The machining quality (minimum surface roughness), productivity (material removal rate) improvement and cost (electrode wear rate) minimization are considered. The influence and correlation of the three most important machining parameters including pulse on time, current and pulse off time have been investigated on sustainable production. Empirical models have been established based on response surface methodology for material removal rate, electrode wear rate and surface roughness. The... 

The present study focuses on simultaneous influence of graphene nanoplatelets (GNP) and hydroxyapatite (HAp) nanopowder on microstructural, wear, tensile and biofunctional behavior of UHMWPE based nanocomposites used in biomedical applications, with the aim to utilize GNP's mechanical strength and wear resistance, while benefitting from HAp's biocompatibility at the same time. 0.1, 0.5 and 1 wt% GNP with 10 wt% optimized concentration of HAp were added to the UHMWPE matrix through an easy two-step approach consisting of solvent mixing and ultrasonication in ethanol as a liquid media. The dried nanocomposite samples of powder were then hot pressed at an optimized temperature and pressure to... 

This paper presents the influence of the severe shot peening process on the fatigue life of the laser-cladded Inconel 718 specimens which can be employed during refurbishment of components enduring high mechanical cyclic loads such as gas turbine components. In order to quantitatively evaluate the destructive effect of laser cladding on the fatigue endurance, fatigue tests are first performed on the as-received and laser-cladded specimens. Then, microstructural analysis by scanning electron microscope (SEM) is carried out to identify the root causes of the drawback of laser cladding. Moreover, by employing a comprehensive laser-cladding FE analysis considering cyclic plastic material...