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    Polyaniline-nylon-6 electrospun nanofibers for headspace adsorptive microextraction

    , Article Analytica Chimica Acta ; Volume 713 , 2012 , Pages 63-69 ; 00032670 (ISSN) Bagheri, H ; Aghakhani, A ; Sharif University of Technology
    2012
    Abstract
    A headspace adsorptive microextraction technique was developed using a novel polyaniline-nylon-6 (PANI-N6) nanofiber sheet, fabricated by electrospinning. The homogeneity and the porosity of the prepared PANI-N6 sheet were studied using the scanning electron microscopy (SEM) and nanofibers diameters were found to be around 200nm. The novel nanofiber sheet was examined as an extracting medium to isolate some selected chlorobenzenes (CBs), as model compounds, from aquatic media. The extracted analytes were desorbed using μL-amounts of solvent and eventually an aliquot of extractant was injected into gas chromatography-mass spectrometry (GC-MS). Various parameters affecting the extraction and...