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    Effect of growth conditions on zinc oxide nanowire array synthesized on Si (100) without catalyst

    , Article Materials Science in Semiconductor Processing ; Volume 16, Issue 1 , 2013 , Pages 171-178 ; 13698001 (ISSN) Rajabi, M ; Dariani, R. S ; Iraji Zad, A ; Sharif University of Technology
    2013
    Abstract
    A uniformly distributed ZnO nanowire array has been grown on silicon (100) substrates by catalyst-free chemical vapor transport and condensation. The effect of growth conditions including source heating temperature, substrate temperature, and gas flow rate on growth properties of ZnO nanowire arrays are studied. Scanning electron microscopy, X-ray diffraction, and room temperature photoluminescence are employed to study the structural features and optical properties of the samples. The results show a correlation among experimental growth parameters. There is a zone for substrate temperature, by controlling gas flow rate, that uniformly distributed and well aligned ZnO nanowire arrays can be... 

    Effects of morphology on photocatalytic performance of Zinc oxide nanostructures synthesized by rapid microwave irradiation methods

    , Article Superlattices and Microstructures ; Volume 51, Issue 4 , 2012 , Pages 512-522 ; 07496036 (ISSN) Kajbafvala, A ; Ghorbani, H ; Paravar, A ; Samberg, J. P ; Kajbafvala, E ; Sadrnezhaad, S. K ; Sharif University of Technology
    2012
    Abstract
    In this study, two different chemical solution methods were used to synthesize Zinc oxide nanostructures via a simple and fast microwave assisted method. Afterwards, the photocatalytic performances of the produced ZnO powders were investigated using methylene blue (MB) photodegradation with UV lamp irradiation. The obtained ZnO nanostructures showed spherical and flower-like morphologies. The average crystallite size of the flower-like and spherical nanostructures were determined to be about 55 nm and 28 nm, respectively. X-ray diffraction (XRD), scanning electronic microscopy (SEM), Brunauer-Emmett-Teller (BET), room temperature photoluminescence (RT-PL) and UV-vis analysis were used for... 

    Microwave-assisted synthesis of narcis-like zinc oxide nanostructures

    , Article Journal of Alloys and Compounds ; Volume 497, Issue 1-2 , May , 2010 , Pages 325-329 ; 09258388 (ISSN) Kajbafvala, A ; Zanganeh, S ; Kajbafvala, E ; Zargar, H. R ; Bayati, M. R ; Sadrnezhaad, S. K ; Sharif University of Technology
    2010
    Abstract
    Through a fast, simple, low cost, surfactant-free and convenient microwave-assisted route, narcis-like ZnO nanostructures (10-15 nm size) with flower diameters in the range of 1-2.5 μm were synthesized. X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FTIR) spectroscopy and room temperature photoluminescence (PL) measurements were used to characterize the produced ZnO nanostructures. The principle raw materials - ammonium hydroxide (NH4OH) and zinc acetate dihydrate [Zn(CH3COO)2·2H2O] - were both inexpensive. The method was fast, simple and surfactant-free capable of producing larger quantities of zinc oxide...