Sharif Digital Repository

Silver chloride nanoparticles (AgCl NPs) have been widely used in various areas such as medicine industry, photographic materials, catalytic materials, pigments, and photochromic materials. Therefore, various studies were conducted for their synthesizes. In the present work, precipitation or reactive crystallization method was used for the synthesis of AgCl NPs. In this regard, silver nitrate and sodium chloride as reactants and gelatin as a surfactant were used in a continuous spinning disk reactor (SDR) at the ambient temperature and pressure. The influences of various parameters such as initial supersaturation , free ion ratio, dilution with water , disk diameter , disk rotation speed,... 

Reduction in the oil reserves level and the increasing of fossil fuel prices and GHG has led to growing value of attention to biodiesel. Reserves of fossil fuels are running out and should have proper alternative for them. Environmental benign and renewable properties of biodiesel make it consider suitable candidate to replace fossil fuels.
In this study, continuous production of biodiesel and optimization of important and influential parameters have been investigated. The method is concluded of trans esterification of soya oil with methanol as feed in presence of homogeneous catalyst of NaOH. The reactor was simple with high efficiency and low operational and investment cost. The... 

In this research work, to enhance the performance of the conventional spinning disk reactors, a novel type of spinning disk reactor has been proposed and tested successfully through the synthesis of barium sulfate nanoparticles by means of the reactive precipitation. This reactor consists of two coaxial rotating disks placed horizontally in a cylindrical chamber. The experimental results clearly indicate the capability of the proposed reactor in the synthesis of nanoparticles with the smaller mean particle size and the narrower particle size distribution compared to those obtained in various process intensification devices such that barium sulfate nanoparticles with a mean particle size of... 

In this study, low-cost and simple method of precipitation or reactive crystallization was used to synthesize nanoparticles of silver iodide. For this purpose, the reaction of silver nitrate and potassium iodide along with several surfactants in a rotating disk reactor at ambient temperature and pressure was applied. In addition, the effects of hydrodynamic conditions such as diameter and rotating speed of the disk, feed flow rate, and feed injection location, with some of the effective kinetic parameters in the synthesis such as the concentration of the reactants, type and concentration of the surfactants and free ion ratio and aging time of solutions using dynamic light scattering analysis... 

Mixing efficiency is an important performance indicator in many chemical reactors. In the present study, using a computational fluid dynamics model, the quality of micromixing in a double-disk-spinning reactor with the ability to rotate both disks using a fast iodide-iodate competitive reaction has been investigated. The purpose of this study was to investigate the effect of operational parameters such as the speed and direction of rotation of disks, radius and number of entry points of one feed, distance between disks, volumetric flow of feed, feed inlet nozzle diameter and acid concentration (H+) on quality of micromixing. The simulation results show that by increasing the rotation speed... 

High mixing efficiency and high liquid-liquid mass transfer rate are two key features of spinning disk contactors. This work presents the experimental investigation of mixing and liquid-liquid mass transfer characteristics in a new double coaxial spinning disks contactor. The micromixing efficiency was investigated using a standard system of competitive parallel reaction known as iodide/iodate test reaction. The influences of various operating conditions such as the rotational speed of the disks, the direction of rotation, the feed radial location, the feed distribution pattern, the distance between the disks, and the feed flow rate on the mixing quality were examined carefully. The obtained...