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Characterization and determination of fatty acids in fish oil using gas chromatography-mass spectrometry coupled with chemometric resolution techniques
, Article Journal of Chromatography A ; Volume 1024, Issue 1-2 , 2004 , Pages 165-176 ; 00219673 (ISSN) ; Vosough, M ; Sharif University of Technology
Elsevier
2004
Abstract
Characterization and determination of a complex mixture of fatty acid methyl esters was performed for commercial fish oil using two-dimensional GC-MS data coupled with resolution techniques. Various principle component analysis methods such as significant factor analysis and fixed size moving window evolving factor analysis were used for the number of factors, zero concentration and selective regions. Then, the convoluted chromatograms were resolved into pure chromatograms and mass spectra using heuristic evolving latent projections (HELP) method. Fatty acids of C16:1ω7, C18:4ω3, C18:1ω11, C18:1ω9, C18:0, C20:2ω6, C20:1ω9, C 22:1ω11, C22:1ω9 and C24:1ω9 were resolved and identified by using...