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    Shearing and mixing effects on synthesis and properties of organoclay/polyester nanocomposites

    , Article Rheologica Acta ; Volume 51, Issue 11-12 , November , 2012 , Pages 1007-1019 ; 00354511 (ISSN) Rajabian, M ; Samadfam, M ; Naderi, G ; Beheshty, M. H ; Sharif University of Technology
    2012
    Abstract
    Mixing of solid nanoparticles in viscous fluids is a key stage in synthesis of nanocomposites and can affect their final properties. A multi-step preparatory mixing is developed to synthesize the nanocomposites of layered silicate in thermosetting polymers. This study aims to investigate the influences of mixing conditions and steps taken to process the thermosetting nanocomposites on the viscoelastic properties of suspensions. We also examine subsequent influences of mixing on the microstructure and dispersion state of cured hybrids of organically modified clays in a polyester resin. The nanocomposites were prepared in a sequential mixing process developed for the model nanocomposites of...