Sharif Digital Repository

Electrical arc discharge in ambient air, vacuum, reactive gas and other environment is an appropriate method for synthesis of different nanostructures. This method can provide stable and ultra pure nanostructures with diverse applications. In this research we focus on synthesis and analysis of titanium nitride nanoparticles in liquid nitrogen(lack of oxygen)by Electrical arc discharge . At the beginning a reactor for the electrical arc discharge process designed and implemented. Titanium nanoparticles have synthesis by this method analyzed. Several characterization techniques such as X-ray diffraction (XRD), dynamic light scattering (DLS), X-ray photo electron spectroscopy (XPS), scanning... 

In this study, samples of wrought nickel-cobalt superalloy AEREX350 underwent hot tensile testing at temperatures ranging from 500 to in the solution-treated state, with subsequent investigation into their mechanical properties and microstructural changes. Anomalous yield strength behavior was observed in this alloy, characterized by an initial decrease in yield stress with rising temperature, followed by an increase and subsequent decrease. Similarly, the ultimate tensile strength exhibited a similar trend to the yield stress. Conversely, ductility parameters demonstrated an inverse relationship with alloy strength. Notably, the alloy displayed a pronounced work-hardening rate at 800 °C.... 

In this work, multi-walled carbon nanotubes (MWCNTs) and single-walled carbon nanotubes (SWCNTs) were synthesized in an aqueous solution of iron chloride and solfate via arc discharge. Thermogravimetric (TG) analysis showed that the multi layer structures including carbon nanotubes (CNTs) and multi-shell graphite particles were formed when DI-water was used. SWCNTs were synthezied in the presence of the iron ions. The effect of [Fe3+]/[Fe2+] ratio on the CNTs yield were investigated. Raman spectroscopy investigations showed that the highest yield was obtained when the ferric to ferro ratio was one. When the concentration of Fe3+ ion was higher than that of Fe2+, many short tubes were... 

Previous observation and models on the origin of linear hardening behavior in FCC polycrystals are critically reviewed. To reveal the draw backs of the previous models, selected results of an investigation on the evolution of microstructure during simple compression testing of two FCC polycrystals, Inconel 625 superalloy and AISI 316L stainless steel are reported. It is found that while a number of FCC polycrystals show linear hardening behavior, the evolution of the underlying microstructure may be quite different. It is argued that, in contrast to the current belief, deformation twinning may not be the sole cause of linear hardening in low SFE FCC polycrystals. It is suggested that only... 

A large number of metals and alloys show an irregular plastic behavior called serrated flow when being deformed in a certain temperature and strain rate range. The occurrence of this phenomenon affects the mechanical properties of the material, such as work hardening rate and ductility; consequently, it exerts limitations on the service conditions in which the alloy can be used.
IN600, IN625 and MP35N are wrought Ni based and Ni-Co based alloys which are thermo-mechanically processed. When these alloys are deformed in temperatures between 300-700 ˚C, serrated plastic flow occurs. In order to investigate the mechanisms responsible for irregularities, hot compression tests were conducted... 

In present work, nanostructured multilayer composites produced from AA1100 and St37 alloys and mechanical properties of resulted samples characterized using tension and micro hardness tests. Also dispersion pattern of second phase in matrix studied via optical microscopy. Thickness of second phase layers showed a little reduction after 2 ARB cycles; but their length decrease gradually. With increasing number of ARB cycles up to 6 cycles, sample's tensile strength first decrease rapidly and after that increased, but never reached initial value. In order to evaluation of heat treatment effects on samples grain structure, samples heat treated and tensile test carried on them. Annealing at 300... 

AEREX350 is a wrought Ni-Co base superalloy which was first developed as a fastener alloy and is a member of MP family of alloys which are thermo-mechanically processed. Due to chemical composition of AEREX350, the alloy benefits from precipitation hardening and solid solution strengthening as well as cold working and can be used in higher temperatures. To investigate the effect of deformation during precipitation, solution-treated samples was underwent hot compression test up to strain of 0.5 at range 650-800˚C, range of γ΄ formation. It is seen that work-hardening and deformation mechanism of high temperature deformation is slip and as a result its structure is dislocation but in room... 

A common heat treatment used for hardenable aluminum alloys is the retrogression process. In this process, by dissolving a specific precipitate in the alloys (η'), the strength of the alloys is reduced and their formability is enhanced. However, by applying the retrogression process and deforming the alloy, followed by an aging cycle, the strength returns to its original state. In this project the microstructural evolution during the retrogression process in 7075-aluminum alloy has been primarily studied experimentally with the help of a transmission electron microscope and the effect of retrogression time on the microstructural evolution has been assessed. In addition, since the simulation...