Search for: x-ray-diffraction-spectroscopy
Article Ceramics International ; Volume 39, Issue 3 , April , 2013 , Pages 2197-2206 ; 02728842 (ISSN) ; Eskandari, A ; Baroonian, M. H ; Berenov, A ; Razavi Hesabi, Z ; Taheri, M ; Sadrnezhaad, S. K ; Sharif University of Technology
Two different hydroxyapatite based composites reinforced by oxide ceramic (20 wt%) nano crystals were synthesized by high-energy ball milling and sintered by pressure less technique. Alumina and titania nanoparticles as secondary phases improved densification and mechanical behavior of apatite and postponed its decomposition to the tricalcium phosphate (TCP) phases at elevated temperatures. Increasing the relative density of apatite using nano reinforcements leads to enhance the bending strength by more than 40% and 27% (as compared to the pure HA) and increase the hardness from 2.52 to 5.12 (Al2O3 composite) and 4.21 (TiO2 addition) GPa, respectively. Transmission electron microscopy (TEM),...
Fabrication of a sensitive and fast response electrochemical glucose sensing platform based on co-based metal-organic frameworks obtained from rapid in situ conversion of electrodeposited cobalt hydroxide intermediates, Article Talanta ; Volume 210 , 2020 ; Ezzati, M ; Hosseini, H ; Sharif University of Technology
Elsevier B.V 2020
In this study, for the first time, we reported a fast and facile three-step in situ strategy for direct controllable growth of the Co3(BTC)2 MOFs thin films on the GCE, through the rapid conversion of the electrodeposited Co(OH)2 nano-flakes on rGO/GCE, to crystalline rectangular bar-shape structures of MOFs. X-ray diffraction spectroscopy, Fourier transform infrared spectroscopy, field emission scanning electron microscopy, energy dispersive X-ray spectroscopy and elemental mapping analysis used to the structural and morphological characterization of the well-synthesized MOFs. The as-prepared Co3(BTC)2 MOFs were used to construct a non-enzymatic sensing platform for determining the glucose...
Immobilization of synthesized phenyl-enriched magnetic nanoparticles in a fabricated Y–Y shaped micro-channel containing microscaled hedges as a microextraction platform, Article Analytica Chimica Acta ; Volume 1136 , 2020 , Pages 51-61 ; Hedeshi, M. H ; Bagheri, H ; Sharif University of Technology
Elsevier B.V 2020
In this survey, a reliable and applicable Y–Y shaped micro–channel in a microfluidic device was designed and manufactured. A number of micro–scaled hedges were precisely fabricated inside the micro–channel to facilitate the immobilization of synthesized core–shell Fe3O4@SiO2 magnetic nanoparticles (MNPs), functionalized by triethoxyphenylsilane (TEPS) by sol-gel technique. Both sample and reagents were introduced into the microfluidic device by a syringe pump to perform the extraction and desorption steps. The functionalized MNPs were characterized by transmission electron microscopy, X-ray diffraction spectroscopy and Fourier transform infrared spectroscopy. By adopting the strategy of...