Bromine-lithium Exchange Reaction in Organic Synthesis Using Glass Microreactor, M.Sc. Thesis Sharif University of Technology ; Mohammadi, Aliasghar (Supervisor)
Abstract
Today, microreactors come into focus due to their exclusive characteristics including high surface-to-volume, lower consumption of reagents and fast mixing. In this study, optimization of the Br-Li exchange reaction as a consecutive reaction using glass microreactor is investigated. To construct glass microreactor, laser ablation and thermal bonding method are utilized. In order to find the best yield and selectivity of the reaction, various parameters, such as solvent, equivalent ration of the two reagents, concentration of the reagents, residence time and flow rates of the reagents are examined. In addition, atomic force microscopy (AFM) analysis was used to determine the surface...
Cataloging briefBromine-lithium Exchange Reaction in Organic Synthesis Using Glass Microreactor, M.Sc. Thesis Sharif University of Technology ; Mohammadi, Aliasghar (Supervisor)
Abstract
Today, microreactors come into focus due to their exclusive characteristics including high surface-to-volume, lower consumption of reagents and fast mixing. In this study, optimization of the Br-Li exchange reaction as a consecutive reaction using glass microreactor is investigated. To construct glass microreactor, laser ablation and thermal bonding method are utilized. In order to find the best yield and selectivity of the reaction, various parameters, such as solvent, equivalent ration of the two reagents, concentration of the reagents, residence time and flow rates of the reagents are examined. In addition, atomic force microscopy (AFM) analysis was used to determine the surface...
Find in contentBookmark |
|