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Microwave-assisted rapid hydrolysis and preparation of thioamides by Willgerodt-Kindler reaction

Matloubi Moghaddam, F ; Sharif University of Technology | 2001

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  1. Type of Document: Article
  2. DOI: 10.1081/SCC-100000216
  3. Publisher: 2001
  4. Abstract:
  5. Aldehydes and aryl alkyl ketones were efficiently transformed to thioamides with the same number of carbon atoms via Willgerodt-Kindler reaction under microwave irradiation in solvent-free conditions. The thioamides obtained were hydrolyzed to corresponding carboxylic acids with microwave dielectric heating in one minute. Both reactions are very fast and the yields are excellent
  6. Keywords:
  7. Hydrolysis ; Microwave ; Monomode system ; Thioamides ; Willgerodt-Kindler reaction
  8. Source: Synthetic Communications ; Volume 31, Issue 2 , 2001 , Pages 317-321 ; 00397911 (ISSN)
  9. URL: https://www.tandfonline.com/doi/abs/10.1081/SCC-100000216