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Synthesis of Magnesium Aluminate Spinel Nanoparticles Using Chemical Method and Investigation of the Effect of Zirconia on Spinel Composites Properties  

, M.Sc. Thesis Sharif University of Technology Maddahi, Vahid (Author) ; Nemati, Ali (Supervisor)
Abstract
In this research, a powder containing magnesium-aluminate spinel particles is prepared based on co-precipitation method and 5% , 10%, 15% and 20% zirconia-contained composites are produced as second phase from the synthesized powder. The raw materials used in the synthesis comprise hexa-hydrated magnesium nitrate, nona-hydrated aluminum nitrate, ammonium bicarbonate, 28% ammonium solution and distilled water. The properties of the powder is then investigated using STA, XRD and SEM tests. Also, XRD and SEM analyses as well as triple point flexural strength and Vickers hardness tests are carried out in order to investigate the effect of adding zirconia to the powders. The variations of the... 

Cataloging brief

Synthesis of Magnesium Aluminate Spinel Nanoparticles Using Chemical Method and Investigation of the Effect of Zirconia on Spinel Composites Properties  

, M.Sc. Thesis Sharif University of Technology Maddahi, Vahid (Author) ; Nemati, Ali (Supervisor)
Abstract
In this research, a powder containing magnesium-aluminate spinel particles is prepared based on co-precipitation method and 5% , 10%, 15% and 20% zirconia-contained composites are produced as second phase from the synthesized powder. The raw materials used in the synthesis comprise hexa-hydrated magnesium nitrate, nona-hydrated aluminum nitrate, ammonium bicarbonate, 28% ammonium solution and distilled water. The properties of the powder is then investigated using STA, XRD and SEM tests. Also, XRD and SEM analyses as well as triple point flexural strength and Vickers hardness tests are carried out in order to investigate the effect of adding zirconia to the powders. The variations of the... 

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