In the present work, nanocomposites consisting of nickel oxide nanostructures and a hollow carbon substrate were used to modify a glassy carbon electrode's surface for the electrooxidation of hydrazine hydrate. For this purpose, hollow carbon nanospheres were first synthesized using aniline and pyrrole copolymerization process without any template needing. The hollow carbon nanospheres prepared by this method have outstanding features such as high specific surface area and good stability. On the other hand, they did not require toxic and environmentally harmful solvents to remove the template. In this study, after preparing hollow carbon nanospheres as a suitable substrate, different...