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A cheap, simple, and versatile method for acetylation of alcohols and phenols and selective deprotection of aromatic acetates under solvent-free condition
, Article Synthetic Communications ; Volume 35, Issue 3 , 2005 , Pages 483-491 ; 00397911 (ISSN) ; Saidi, M. R ; Sharif University of Technology
2005
Abstract
Acyclic and cyclic acetates of various alcohols and phenols were obtained in excellent yields under mild reaction conditions in the presence of a catalytic amount of sodium hydroxide under solvent-free conditions and microwave irradiation. Selective deprotection of acetate group from the corresponding phenolic compounds was carried out in the presence of LiClO4· 2H2O. Copyright © Taylor & Francis, Inc