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Versatile and large-scale synthesis of functional dithiocarbamates in water
, Article Synthetic Communications ; Volume 41, Issue 1 , Dec , 2011 , Pages 94-99 ; 00397911 (ISSN) ; Aryanasab, F ; Tourkian, L ; Saidi, M. R ; Sharif University of Technology
2011
Abstract
Structural diversity is possible in direct access to functional dithiocarbamates based on a highly efficient and simple one-pot reaction of CS2, amines, and alkyl halides in nearly quantitative yields in water
Highly efficient Michael addition reaction of amines catalyzed by silica-supported aluminum chloride
, Article Synthetic Communications ; Volume 39, Issue 6 , 2009 , Pages 1109-1119 ; 00397911 (ISSN) ; Pourshojaei, Y ; Aryanasab, F ; Sharif University of Technology
2009
Abstract
Aliphatic and aromatic amines undergo smooth nucleophilic addition to α,β-unsaturated compounds in the presence of a catalytic amount of silica-supported aluminum chloride at 60°C and under solvent-free conditions to produce the corresponding β-amino compounds in excellent yields. This method is simple and convenient and works efficiently under mild conditions. This catalyst can used again without losing its activity three times. Copyright © Taylor & Francis Group, LLC
Catalyst-free Friedel-Crafts alkylation of naphthols with nitrostyrenes in the presence of water
, Article Tetrahedron Letters ; Volume 50, Issue 13 , 2009 , Pages 1441-1443 ; 00404039 (ISSN) ; Aryanasab, F ; Saidi, M. R ; Sharif University of Technology
2009
Abstract
Accelerated Michael-type Friedel-Crafts alkylation of naphthols with nitrostyrenes in the presence of water is reported. The procedure is simple, catalyst-free, and affords good yields of the products. © 2009 Elsevier Ltd. All rights reserved
Waste-free and environment-friendly uncatalyzed synthesis of dithiocarbamates under solvent-free conditions
, Article Synlett ; Issue 18 , 2007 , Pages 2797-2800 ; 09365214 (ISSN) ; Ebrahimi, F ; Aakbari, E ; Aryanasab, F ; Saidi, M.R ; Sharif University of Technology
2007
Abstract
A mild, convenient, and practical one-pot procedure for the direct synthesis of dithiocarbamates has been developed by condensation of amines, CS2, and a Michael acceptor, under solvent-free conditions at room temperature in good to excellent yields. © Georg Thieme Verlag Stuttgart
A simple and novel eco-friendly process for the one-pot synthesis of dithiocarbamates from amines, carbon disulfide, and epoxides
, Article Synlett ; Issue 8 , 2007 , Pages 1239-1242 ; 09365214 (ISSN) ; Pourhasan, B ; Aryanasab, F ; Saidi, M. R ; Sharif University of Technology
2007
Abstract
An environmentally benign, highly efficient, and simple protocol for the synthesis of various structurally divergent dithiocarbamate derivatives in one-pot reaction of amines, carbon disulfide, and epoxides, without using any solvent and catalyst at room temperature, is presented. This new procedure has the advantages of higher yield, lower cost, reduced environmental impact, and simple work-up procedure. © Georg Thieme Verlag Stuttgart
Straightforward and highly efficient catalyst-free one-pot synthesis of dithiocarbamates under solvent-free conditions
, Article Organic Letters ; Volume 8, Issue 23 , 2006 , Pages 5275-5277 ; 15237060 (ISSN) ; Aryanasab, F ; Saidi, M. R ; Sharif University of Technology
2006
Abstract
A highly efficient and simple synthesis of dithiocarbamates is possible based on the one-pot reaction of amines, CS2, and alkyl halides without using a catalyst under solvent-free conditions. The mild reaction conditions, high yields, and broad scope of the reaction illustrate the good synthetic utility of this method. The reaction is a highly atom-economic process for production of S-alkyl thiocarbamates and successfully can be used in high quantities in the pharmaceutical or agrochemical industries. © 2006 American Chemical Society
One-pot synthesis of dithiocarbamates accelerated in water
, Article Journal of Organic Chemistry ; Volume 71, Issue 9 , 2006 , Pages 3634-3635 ; 00223263 (ISSN) ; Aryanasab, F ; Torkiyan, L ; Ziyaei, A ; Saidi, M. R ; Sharif University of Technology
2006
Abstract
Highly efficient one-pot reactions of amines and carbon disulfide with α,β-unsaturated compounds were carried out in water under a mild and green procedure with high yields. © 2006 American Chemical Society