Sharif Digital Repository

Mechanical properties, microstructural events, residual stresses, and aging behavior of friction stir-welded AA6061-T6 were investigated in this work. Microstructural and mechanical characterizations of the friction stir-welded joints in as-welded and post-welded conditions were made by means of optical metallography, transmission electron microscopy, X-ray diffraction for determination of residual stresses, tensile testing, and hardness measurements. It was found that weld strength and hardness variations after welding are mainly dependent on the imposed heat input per unit length. Besides, the kinetics of natural aging in the welded samples was found to be noticeable within the first 14... 

Archaeological excavations in western Iran have recently revealed a significant Luristan Bronzes collection from Sangtarashan archaeological site. The site and its bronze collection are dated to Iron Age II/III of western Iran (10th-7th century BC) according to archaeological research. Alloy composition, microstructure and manufacturing technique of some sheet metal vessels are determined to reveal metallurgical processes in western Iran in the first millennium BC. Experimental analyses were carried out using Scanning Electron Microscopy-Energy Dispersive X-ray Spectroscopy and Optical Microscopy/Metallography methods. The results allowed reconstructing the manufacturing process of bronze... 

Gas tungsten arc welding of CK45 and AISI304 stainless steel was performed through preparation of different types of samples using ER308L and ERNi-1 wires. Welded samples were studied by different techniques including optical metallography, scanning electron microscopy equipped with energy dispersive X-ray spectroscopy (SEM-EDS), X-ray diffraction, hardness measurements and impact test. It was observed that in the buttered specimen, the structure of the weld metal was completely austenitic while the microstructure of unbuttered sample was duplex ferritic-austenitic. M23C6-type carbides were observed within the weld metal of both as-weld specimen types. Effects of different post-weld heat... 

Data are presented on the solidification of aluminum alloys and their macro segregation behavior. Three alloys with different solidification ranges were prepared in two temperatures. Two types of molds were also prepared by sand and metallic materials. The solidification of Al alloys were studied and the effects of four parameters were determined, including cooling rate, casting temperature, degassing and nucleation effects on solidification and a comparison was conducted to Scheil model performance. Three types of aluminum alloys (Al-12.1%Si, Al-6.9%Si and Al-4.4% Cu) with short, medium and wide solidification ranges were studied and the results showed that degassing, nucleation, increasing... 

Microstructural changes in friction-stir welding (FSW) of artificially aged AA2017 were investigated. First, FSW was performed with rotational and linear speeds of 800 rpm and 40 mm/min, respectively. Then, microstructural studies by means of optical metallography and electron microscopy were conducted in different regions of the welded plates. Hardness testing was also employed to determine local strength and subsequent natural aging progress after welding. The results indicate that the considerable hardness degradation occurs in the thermo-mechanically affected zone owing to coarsening of semi-coherent precipitates. Grain refinement also takes place in the weld nugget as a result of... 

A numerical study on mixing/segregation phenomena in a pressurized fluidized bed with large particles of Geldart D type of binary density but same diameter with high velocity gas was performed by the use of discrete particle simulation. Particle mixtures are composed of spherical particles with 2mm diameter and 1g/cm3 flotsam density and different jetsam densities of 1.25, 2 and 2.5g/cm3 with jetsam volume fraction of 0.5. The particles are initially packed approaching perfect mixing state in a rectangular bed and then fluidized by gas uniformly injected at the bottom of the bed. Effect of increase of pressure and density ratio was investigated and mixing/segregation behavior is discussed in... 

The variation of morphology and mechanical properties of Al6061 automotive aluminum alloy due to friction stir welding (FSW) and gas tungsten arc welding (GTAW) was investigated by optical metallography, scanning electron microscopy, microhardness measurement, X-ray diffraction, tensile testing, and fractography. The center-line dendrite emergence and microhardness reduction in the heat-affected zone were observed in the GTAW process. Although similar microhardness reduction with respect to the base metal was observed in the FSW samples, higher HVs were obtained for the FSW rather than the GTAW process at almost all heat-affected locations. Ultimate tensile strengths of the FSW and the GTAW... 

In this paper, the effect of molybdenum on the grain boundary segregation of other elements was studied in Incoloy 901 superalloy. Initially, five alloys were prepared with different percentages of Mo by using a vacuum induction furnace. Then, these alloys were remelted by Electro-slag remelting (ESR) process and after homogenizing at 1160 °C for 2. h followed by air cooling, were rolled. The effect of Mo on segregation of elements was evaluated with Scanning Electron Microscopy, Linear Analysis, and the mechanical tests. The results showed that the grain boundary segregations of elements in Incoloy 901 superalloy were decreased by increasing of molybdenum content up to 6.7% and the... 

In this paper, the well-known effective medium approximation (EMA) and coupled dipole approximation (CDA) methods are employed to study the optical properties of a metal nanoparticle-block copolymer (MNP-BCP) nanocomposite. This approach is applied to study a system consisting of small gold spherical nanoparticles randomly distributed in the cylindrical micelles of a di-BCP. At first, the EMA method is used to obtain the effective dielectric function of a semi-metallic cylinder. Then, the extinction spectrum of the hexagonal 2D-array of semi-metallic cylinders is obtained by the CDA method. This procedure makes it possible to study simultaneously both the electromagnetic extinction of MNPs... 

In the present study, 30MSV6 microalloyed steel was heat treated under different conditions, and the relation between its microstructure and mechanical properties was investigated. Scanning electron microscopy and transmission electron microscopy were used to characterize the microstructure of the heat-treated steel, and the effect of microstructure on tensile strength and fatigue behavior was determined. Microstructural analysis indicated that precipitates were formed at different sites such as grain boundaries and sub-grain boundaries. Furthermore, microstructural studies accompanied by the evaluation of mechanical properties revealed that the optimal heat treatment cycle of 30MSV6... 

Wrought aluminum sheets with thickness of 13. mm were square butt-welded by friction stir welding (FSW) and gas tungsten arc welding (GTAW) methods. Corrosion behavior of the welding zone was probed by Tafel polarization curve. Optical metallography (OM) and scanning electron microscopy together with energy dispersive spectroscopy (SEM-EDS) were used to determine morphology and semi-quantitative analysis of the welded zone. FSW resulted in equiaxed grains of about 1-2 μm, while GTAW caused dendritic structure of the welded region. Resistance to corrosion was greater for the FSW grains than the GTAW structure. In both cases, susceptibility to corrosion attack was greater in the welded region... 

Dissimilar friction stir welds of aluminum alloys AA5086 in annealed and AA6061 in T6 temper conditions were investigated in terms of residual stress, grain structure and precipitation distribution in different zones of the welded joints. Optical metallography and transmission electron microscopy were used to characterize microstructures of different zones of the welds. In addition, residual stress profile and local mechanical properties of different zones were evaluated employing X-ray diffraction method and digital image correlation technique. It was found that softening in the AA6061-T6 side occurs in regions with weld peak temperature higher than 300 °C. The micro-hardness profile... 

Porous NiTi shape memory alloy (SMA) was fabricated by sintering of compressed constituent elements pre-mixed with NaCl or urea spacer holders. Effect of spacer to metal volume-ratio (r S) on shape, size, distribution and openness of the voids was probed by optical metallography, X-ray diffraction (XRD) and scanning electron microscopy (SEM). Differential scanning calorimetry (DSC) was used to determine the SMA transformation temperatures. Controllable void geometry helping osteoblast proliferation and bone cell growth was gained by addition of the spacers. At r S = 0.7, percentage of the open pores reached 52% while at r S = 1.43, interconnected pores with 200 to 500 μm diameter were... 

This paper presents the effect of martensite volume fraction (VM) on mechanical properties of AISI 4340 steel with ferrite-bainite-martensite microstructures. The steel bars were austenitized at 900°C for 1h followed by intercritical annealing at 740°C for 100min and quenching into a salt bath with temperature of 300°C and holding at different times to obtain triple phase (TP) microstructures with 34vol.% fraction ferrite and various martensite (or bainite) contents. Presence of three phases in adjacent to each other was confirmed by metallographic analysis and TEM studies. TEM observation also indicates higher density of dislocations within ferrite near martensite colonies compared to that... 

Thermomechnical processing and controlled rolling of microalloyed steel sheets are affected by several factors according to the final properties of product. To create the high mechanical properties, a uniform and fine-grain structure is necessary in hot rolled final products. To produce such microstructures, every stage of the thermomechanical processing of the steel rolling has to be carefully controlled. Hence, first step is grain coarsening control that it usually occurs during reheating for slab. For this purpose, seven different reheating temperatures between 1000 to 1300 °C with 50 °C increments were chosen in this investigation for soaking treatment. By soaking the specimens in... 

In the present article, the effect of Rare Earth elements on the microstructural development of as cast and semisolid Mg-4Al alloy produced by SIMA process is studied. Investigation conducted by metallographic observation, scanning electron microscope and quantitative metallographic methods. Results showed that alloy's dendrites turn into larger fully dendritic shape with sharp and narrow arms from equiaxed rosette type as the amount of RE elements increased from 0 through 4%. The effect of RE elements on the microstructure of the treated-alloys was detectable through elimination of vast number of intragranular liquid droplets as well as by decreasing kinetic of microstructural changes. It... 

The state of solids mixing can be considered as a key factor in accomplishment of high efficiency and a uniform product in gas-solid fluidized-beds operating with several different particle sizes. In the present work, coupled DEM-CFD approach was used to carefully investigate the mixing process of binary particles in flat-bottom spouted beds. In this regard, simultaneous effects of particle specifications, operating conditions, and bed dimensions on the equilibrium mixing state of solid mixture were evaluated in detail. Moreover, taking into account the contribution of various parameters, the obtained simulation results were used to draw a correlation for predicting the equilibrium mixing... 

This paper presents the results obtained and the deductions made from a series of microstructural studies and mechanical tests involving gray cast iron which was sand cast using a variety of modules. The effect of cooling rate on the primary dendrite arm spacing (DAS), secondary dendrite arm spacing (SDAS), thickness of ferrite-cementite layer (λe) and the hardness (HB) were evaluated. Results show that the both DAS and SDAS and also λe are highly dependent on the cooling rate, and they decreases as the cooling rate increases. More attempts were also done to correlate the HB with DAS, SDAS and λe. It was found that HB increases as DAS, SDAS and λe decreases  

Thermo mechanical processing and controlled rolling of microalloyed steel sheets are affected by several factors. In this investigation, finishing temperature of rolling which is considered as the most effective parameters on the final mechanical properties of hot rolled products has been studied. For this purpose, three different finishing temperatures of 950, 900 and 850 °C below the non-recrystallization temperature and one temperature of 800 °C in the intercritical range were chosen. It is observed that decreasing the finishing temperature causes increase of strength and decrease of total elongation. This is accompanied by more grain refinement of microstructure and the morphology was...