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    Experimental characterization of stabilized suspensions caused by formation of nanoparticle halos

    , Article ASME 2014 12th International Conference on Nanochannels, Microchannels, and Minichannels, ICNMM 2014, Collocated with the ASME 2014 4th Joint US-European Fluids Engineering Division Summer Meeting ; 2014 ; ISBN: 9780791846278 Keramati, H ; Zabetian, M ; Saidi, M. H ; Mozafari, A. A ; Sharif University of Technology
    Abstract
    Suspension flow has an important role in various applications such as paint, material and pharmaceutical industries. Settling is considered as a resisting phenomenon in the processes dealing with suspensions. Using nanoparticles as an additive to micro-particulates has been studied in limited studies. This work presents an experimental investigation to assess the effectiveness of nanoparticles in reduction of suspension settling. Microscopic imaging and transmission measurement were used to analyze the stability factors in a container. Transmission analysis revealed that presence of nanoparticles in the suspension, decreased the sedimentation rate. Microscopy showed that the settling rate... 

    Dye-sensitized solar cells based on a single layer deposition of TiO 2 from a new formulation paste and their photovoltaic performance

    , Article Solar Energy ; Volume 86, Issue 9 , 2012 , Pages 2654-2664 ; 0038092X (ISSN) Mohammadi, M. R ; Louca, R. R. M ; Fray, D. J ; Welland, M. E ; Sharif University of Technology
    Abstract
    A new strategy for enhancing the efficiency and reducing the production cost of TiO 2 solar cells by design of a new formulated TiO 2 paste with tailored crystal structure and morphology is reported. The conventional three- or four-fold layer deposition process was eliminated and replaced by a single layer deposition of TiO 2 compound. Different TiO 2 pastes with various crystal structures, morphologies and crystallite sizes were prepared by an aqueous particulate sol-gel process. Based on simultaneous differential thermal (SDT) analysis the minimum annealing temperature to obtain organic-free TiO 2 paste was determined at 400°C, being one of the lowest crystallization temperatures of TiO 2... 

    Characterization of Microparticle Suspension Using Experimental and Image Processing Methods

    , M.Sc. Thesis Sharif University of Technology Rohani, Ramtin (Author) ; Saeedi, Mohammad Hasan (Supervisor) ; Shafiee, Mohammad Behshad (Co-Advisor)
    Abstract
    Various application of polyethylene material in different industries caused to modern techniques for controlling and measuring specifications of micro-particle suspension. Many industries try to increase stability of suspensions in front of their phase separation.
    Because of the consequences of suspension homogeneity, at first, we measured this property. Then, the stability was tested by three different methods. In the first method, the transmitted laser light was measured to assay the suspensions stability. In the second, number of sediments of particles was counted. Sedimentation velocity of particles was measured directly by using a horizontal microscope as the third method. The... 

    Stabilization of Microparticle Suspension by Means of Nanoparticle with Focus on the Optical Measurement Methods

    , M.Sc. Thesis Sharif University of Technology Keramati, Hadi (Author) ; Saidi, Mohammad Hassan (Supervisor) ; Mozafari, Ali Asghar (Co-Advisor)
    Abstract
    Many of industrial processes include suspension in their middle section of production, final product or residue. Majority of these two-phase mixtures are unstable due to their large particle size (larger than one micrometer). Therefore, Study of particle distribution in suspensions for generation of stabilized suspension becomes significant. In this study a new mechanism in stabilization of microparticle suspension known as nanoparticle halo mechanism has been assessed. Experiments have been conducted in dilute suspension and two-way coupling range. The effect of the presence of silica nanoparticle on zirconia microparticle suspension has been investigated. The effect of zeta potential of... 

    Experimental Studies for Lactase Immobilization on the Polymer base and Characterising

    , M.Sc. Thesis Sharif University of Technology Derakhshan, Elahe (Author) ; Yaghmaei, Soheyla (Supervisor)
    Abstract
    Immobilization of β-D-galactosidase represents an important approach for development of lactose hydrolysis technology.Chitosan proved to be an excellent carrier for β-Dgalactosidase immobilization, by both covalent binding and sol-gel entrapment combined with adsorption. Among different preparation methods of chitosan support particles for covalent binding, emulsion cross-linking was the most efficient, producing narrow-sized microspheres, without aggregation.The best process parameters of β-D-galactosidase immobilization by covalent coupling on chitosan microspheres were found as 3% glutaraldehyde cross-linker concentration, enzyme loading of 27 mg protein/g dry support, 6 h reaction time,... 

    Stabilization of the suspension of zirconia microparticle using the nanoparticle halos mechanism: zeta potential effect

    , Article Journal of Dispersion Science and Technology ; Volume 37, Issue 1 , 2016 , Pages 6-13 ; 01932691 (ISSN) Keramati, H ; Saidi, M.H ; Zabetian, M ; Sharif University of Technology
    Taylor and Francis Inc  2016
    Abstract
    An experimental study has been conducted to investigate the effect of silica nanoparticle halos on the stability of the zirconia aqueous suspension. The results of turbidity measurements showed that addition of nanoparticles to the suspension increases the stability of the zirconia suspension for all pH values. The achieved stability refers to the formation of nanoparticle halos around the microparticles that can be observed by scanning electron microscopy (SEM) imaging. The best stabilization is achievable when zirconia microparticles are at the isoelectric point. The minimum stabilization occurs when microparticles have relatively high zeta potential and the force between micro and... 

    Transportation and Settling Distribution of Microparticles in Low-Reynolds-Number Poiseuille Flow in Microchannel

    , Article Journal of Dispersion Science and Technology ; Volume 37, Issue 4 , 2016 , Pages 582-594 ; 01932691 (ISSN) Razaghi, R ; Saidi, M. H ; Sharif University of Technology
    Taylor and Francis Inc 
    Abstract
    In this article, velocity field and settling distribution of microparticles in a dilute suspension in low-Reynolds-number Poiseuille flow in a microchannel is experimentally investigated using microscopic image analysis. An effective technique is applied to manipulate single-particle tracking in order to determine the controlling parameters on transportation and settling of microparticles in microchannels. The results show that the velocities of dispersed phase are affected by the hydrodynamic properties, and this velocity deviation can be significant when the hydrodynamic coupling between particles and channel walls is considerable. Increasing the Reynolds number would result in decrease in... 

    Experimental Study of Pool Boiling Heat Transfer Enhancement by Presence of Magnetic Particles under the Influence of Magnetic Field

    , M.Sc. Thesis Sharif University of Technology Feizbakhshi, Morteza (Author) ; Behshad Shafii, Mohammad (Supervisor)
    Abstract
    Study on pool boiling heat transfer characteristics of water-based magnetic fluid and distilled water containing micro size particles has performed. Different concentration in each experiment has been studied to investigate the effect of magnetic fluid and micro size particles on boiling heat transfer on horizontal plate heater. The nickel particles was used as micro size particles which is expected to increase thermal performance of water due to high thermal conductivity of nickel. Experimental results showed adding nickel micro size particles to water can deteriorate the boiling heat transfer coefficient. However the amount of deterioration was the same for all concentrations of nickel... 

    Characterization of chlorella vulgaris and chlorella protothecoides using multi-pixel photon counters in a 3D focusing optofluidic system

    , Article RSC Advances ; Volume 7, Issue 8 , 2017 , Pages 4402-4408 ; 20462069 (ISSN) Vander Wiel, J. B ; Mikulicz, J. D ; Boysen, M. R ; Hashemi, N ; Kalgren, P ; Nauman, L ; Baetzold, S. J ; Powell, G. G ; He, Q ; Hashemi, N. N ; Sharif University of Technology
    Royal Society of Chemistry  2017
    Abstract
    Analysis of microparticle size and fluorescence intensity can be used to classify microparticles. We designed and fabricated an optofluidic system that characterizes microparticles, including fluorescent microparticles and microalgae. A new type of multi-pixel photon counter (MPPC) was employed to miniaturize the device, lower its power consumption, and make it insensitive to magnetic fields. The system uses a 635 nm laser for excitation of the microparticles' fluorescence. The scattered light from the fluorescent microparticles, as well as Chlorella vulgaris and Chlorella protothecoides, were measured. Additionally, we analyzed the width and height of the measured signals generated as a... 

    DEP Force Measurement on Polystyrene Beads and Red Blood Cells Using Optical Tweezers

    , Ph.D. Dissertation Sharif University of Technology Sasanpour Yazdi, Mehrzad (Author) ; Seyed Reihani, Nader (Supervisor)
    Abstract
    In the presence of spatially non-uniform electric field, a dielectric object can experience a translational force which is known as Dielectrophoresis (DEP) force. DEP is one of the most applicable methods in sorting mechanism of different biological cells. Moreover accurately measuring the DEP force in single cell level can lead to a valuable knwoledge about the electrical properties of various cells.In this thesis, first, the other electrokinetic forces in which the Electro-Osmosis (EO) force is the important one, have to be eliminated. Regarding that this effect is strongly dependent on the frequency of external E field, we have applied the external electric field at appropriate frequency... 

    Nonlinear hierarchical multiscale modeling of cortical bone considering its nanoscale microstructure

    , Article Journal of Biomechanics ; Volume 42, Issue 10 , 2009 , Pages 1560-1565 ; 00219290 (ISSN) Ghanbari, J ; Naghdabadi, R ; Sharif University of Technology
    2009
    Abstract
    We have used a hierarchical multiscale modeling scheme for the analysis of cortical bone considering it as a nanocomposite. This scheme consists of definition of two boundary value problems, one for macroscale, and another for microscale. The coupling between these scales is done by using the homogenization technique. At every material point in which the constitutive model is needed, a microscale boundary value problem is defined using a macroscopic kinematical quantity and solved. Using the described scheme, we have studied elastic properties of cortical bone considering its nanoscale microstructural constituents with various mineral volume fractions. Since the microstructure of bone... 

    A novel approach for microparticle separation based on dielectrophoresis method

    , Article Biomedical Physics and Engineering Express ; Volume 5, Issue 3 , 2019 ; 20571976 (ISSN) Rafiefard, N ; Sasanpour, P ; Fardindoost, S ; Irajizad, A ; Sharif University of Technology
    Institute of Physics Publishing  2019
    Abstract
    A novel approach for particles size separation based on dielectrophoresis (DEP) method is introduced and analyzed both computationally and experimentally. The proposed technique has been utilized for the separation of polystyrene (PS) particles with 8, 6 and 2 μm diameters passing through microchannels with planar electrodes. The performance of the technique has been computationally analyzed using the finite element method (FEM). Considering the structure of the planar electrodes, we propose an approach based on applying an electric potential between one of the global electrodes, and a needle touched the top of the cell suspension. Results of both simulation and experiment show that by... 

    The effect of the second excitation frequency mode under different conditions on the fluid streaming and microparticles acoustophoresis with the aim of separating biological cells

    , Article Computer Methods and Programs in Biomedicine ; Volume 184 , 2020 Hosseini, M ; Hasani, M. A ; Biglarian, M ; Amoei, A. H ; Toghraie, D ; Mehrizi, A. A ; Rostami, S ; Sharif University of Technology
    Elsevier Ireland Ltd  2020
    Abstract
    Background and objective: In this study, the effect of the second excitation frequency mode under different conditions on the fluid streaming and its microparticles displacement is investigated. Methods: For this purpose, some variable parameters such as the particle diameter, microchannel aspect ratio, and applied frequency modes have been selected to study. The resulted acoustic streaming was scrutinized to understand the physics of the problem under different geometrical and input conditions. Finally, the effect of the increasing the microparticle size and aspect ratio of the microchannel, simultaneously, has been evaluated. Results: The results demonstrated that increasing the... 

    Effect of collision on self-assembly of nanoparticles in zirconia microparticle suspension

    , Article Journal of Dispersion Science and Technology ; 2020 Jiryaei, Z ; Saidi, M. H ; Sharif University of Technology
    Bellwether Publishing, Ltd  2020
    Abstract
    Nanoparticle halo mechanism is a stabilization method for microparticle suspensions. This study investigates suspension pH and nanoparticles–microparticles collision effects on the stabilization of an aqueous binary suspension. The long-term turbidity measurements show that for the nanosilica suspension stability is directly correlated with pH values; however, in the cases of zirconia and binary suspensions, it is not a monotonic function of pH. It is shown that for binary suspension, the halo mechanism is the primary method affecting the stability of the suspension. The suspension is best-stabilized at pH = 5 that is associated with high halo mechanism efficiency, while increased repulsive... 

    Particle Focusing on a Lab on a Disk System

    , M.Sc. Thesis Sharif University of Technology Heydarabadipour, Adel (Author) ; Shamloo, Amir (Supervisor)
    Abstract
    In many microfluidic devices, focusing particles into a narrow stream is usually an essential step prior to counting, detecting, and sorting them. By installation of microfluidic laboratory functions on a rotating disk, new devices called Lab-on-a-disks, which have plenty of advantages in comparison to ordinary Lab-on-a-chips, shape. In this study, to the best of our knowledge for the first time, a Lab-on-a-disk device is designed and fabricated in order to focus particles prior to detecting them by a conventional CD-ROM as a strong optical system. Hydrophoresis method, using slanted obstacles to induce transverse pressure gradients, is utilized to focus particles. In this regard, the... 

    Production of uniform size cell-enclosing silk derivative vehicles through coaxial microfluidic device and horseradish crosslinking reaction

    , Article European Polymer Journal ; Volume 172 , 2022 ; 00143057 (ISSN) Badali, E ; Hosseini, M ; Varaa, N ; Mahmoodi, N ; Goodarzi, A ; Taghdiri Nooshabadi, V ; Hassanzadeh, S ; Arabpour, Z ; Khanmohammadi, M ; Sharif University of Technology
    Elsevier Ltd  2022
    Abstract
    Silk fibroin (SF) as a natural biopolymer holds great potential in biomedical research because of its biocompatibility, easy processability and high strength properties. However, slow gelation time has narrowed its applications, specifically in cell-laden microparticle production due to insufficient crosslinkable moieties. This study aimed to develop cell-laden silk fibroin-phenol (SF-Ph) microparticle through co-flow microfluidic system using SF conjugated Ph moieties whereas covalent crosslinking is mediated with horseradish peroxidase (HRP) in the presence of hydrogen peroxide (H2O2). For this, the SF-Ph was synthesized through carbodiimide condensation crosslinking reaction. Aqueous... 

    Effect of collision on self-assembly of nanoparticles in zirconia microparticle suspension

    , Article Journal of Dispersion Science and Technology ; Volume 43, Issue 6 , 2022 , Pages 787-795 ; 01932691 (ISSN) Jiryaei, Z ; Saidi, M. H ; Sharif University of Technology
    Taylor and Francis Ltd  2022
    Abstract
    Nanoparticle halo mechanism is a stabilization method for microparticle suspensions. This study investigates suspension pH and nanoparticles–microparticles collision effects on the stabilization of an aqueous binary suspension. The long-term turbidity measurements show that for the nanosilica suspension stability is directly correlated with pH values; however, in the cases of zirconia and binary suspensions, it is not a monotonic function of pH. It is shown that for binary suspension, the halo mechanism is the primary method affecting the stability of the suspension. The suspension is best-stabilized at pH = 5 that is associated with high halo mechanism efficiency, while increased repulsive...