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    Grain Size Control in Fusion Welding and Wire-Arc Additive Manufacturing of Ferritic Stainless Steels

    , M.Sc. Thesis Sharif University of Technology Alikhani, Ali Akbar (Author) ; Pouranvari, Majid (Supervisor) ; Kokabi, Amir Hossein (Supervisor)
    Abstract
    Ferritic stainless steels, despite having a good combination of mechanical properties and corrosion properties and low price, are less used than austenitic stainless steels due to their low weldability. The main challenges of welding ferritic stainless steels are coarse grain formation in the molten area as well as grain growth in the heat affected zone. In this research, in the first phase, an attempt is made to change the shape and size of the grains in the melted zone by changing the GTAW fusion welding parameters, including welding current and welding speed. In the second phase, an attempt is made to prevent the formation of columnar grains by adding micron particles to the molten pool... 

    Prediction of Temperature and Strain Distribution in the Warm Rolling of Austenite Stainless Steel

    , M.Sc. Thesis Sharif University of Technology Nemati, Elham (Author) ; Serajzadeh, Siamak (Supervisor)
    Abstract
    In this research, the hot and warm rolling of stainless steel 304 was studied. First the rolling process was simulated using Finite Element Method software ABAQUS and the distribution of temperature and strain in the process under discontinuous conditions were predicted. Next, hot and warm rolling of stainless steel 304 under different conditions was carried out. Specimens were cut and subject to mechanical testing, metallography and electron microscopic studies. Data obtained from these experiments and the predicted trends from ABAQUS were compared, therefore studying the effect of different parameters on the microstructure and mechanical properties of the rolled specimen. Results indicate... 

    Lanthanum Chromite Coating on Stainless Steel by sol–Gel Dip Coating Technique

    , M.Sc. Thesis Sharif University of Technology Rashtchi, Hamed (Author) ; Faghihi Sani, Mohammad Ali (Supervisor)
    Abstract
    Because of the high operating temperature, interconnect surface tends to be oxidized and Cr2O3 oxide layer will be created on the surface. This phenomenon is undesirable due to decreasing electrical conductivity, so a preservative coating is needed to improve the interconnect properties. In this paper, a dense perovskite thin film was successfully synthesized on a ferritic stainless steel (type 430) substrate by a sol-gel dip coating method. This coating improved chemical stability, oxidation behavior of the substrate and decreased cathode poisoning. The lanthanum chromite was coated on the substrate by sol-gel dip coating process. First, during a hydrolyze process, a stable sol was made up... 

    PVDF/SiO2 Nanocomposite Coating with Different Wettability in Contact with Oil and Water for phase Separation Propose

    , M.Sc. Thesis Sharif University of Technology Hassani, Mohammad Ebrahim (Author) ; Dolati, Abolghasem (Supervisor)
    Abstract
    increased cohesion up to 4H pencil. Results of immersion test in water showed stability of coatings. Polarization test in naphtha and water mixture for stainless steel, copper and aluminum meshes demonstrated 98.89%, 86.25% and 66.6% protection efficiency respectively. In order to study of oil and water separation efficiency, mixtures of water and naphtha with different content of naphtha were used. Separation test for 200μm St.St mesh in different slopes demonstrated that changing of slop increase separation efficiency up to 95.5% for water and up to 100% for naphtha. Separation test for meshes with different pore size demonstrated that meshes with small pore size are more appropriate for... 

    Study of Microstructure and Mechanical Properties of Austenitic Stainless Steel after Sheet Rolling Process

    , M.Sc. Thesis Sharif University of Technology Abedi, Fatemeh (Author) ; Serajzadeh, Siamak (Supervisor)
    Abstract
    Austenite in the 300 stainless steels is not a table phase in deformation processing during which martensite phase forms. This causes significant changes in the microstructures as well as the mechanical properties of deformed steel. In this work, the effects of rolling speed, reduction, temperature and strain pass on the strain-induced martensite during strip rolling operation of stainless steel 304L are studied. Cold rolling experiments under different speeds, reduction and temperature are conducted and then, the microstructural events and mechanical properties of the rolled steel are evaluated. For doing so, different testing techniques including tensile test, hardness measurement, optical... 

    A study on Warm Rolling Behavior of an Austenitic Stainless Steel and the Mechanical Properties of the Rolled Product

    , M.Sc. Thesis Sharif University of Technology Ghadamgahi, Mojtaba (Author) ; Serajzade, Siamak (Supervisor)
    Abstract
    In this study, thermo-mechanical behavior of an austenitic stainless steel AISI316L was investigated using mathematical modeling and experimental analysis during warm rolling process. First, the thermo-mechanical analysis was carried out employing the finite element software, Abaqus CAE, to assess temperature, strain, velocity and stress distribution during rolling. Then, rolling operations on 316L austenitic steel were performed under different working conditions while mechanical testing as well as microstructural observations were made on the rolled steels. Using simulation results and practical data, microstructural events and mechanical properties after warm rolling of stainless steel... 

    Deformation and Annealing Behavior of an Austenitic Stainless Steel

    , M.Sc. Thesis Sharif University of Technology Sadat Alavi, Parisa (Author) ; Serajzadeh, Siamak (Supervisor)
    Abstract
    In this research, non-isothermal annealing process at temperatures ranging between 400°C to 830 °C was investigated in warm and cold-rolled austenitic stainless steel 304L. First, the wide variety of austenitic to martensitic structure was produced by the multi-pass rolling process at room temperature -8 °C, 200 °C, and 280°C. The n exponent in Olson-Cohen equation was governed 2.83 after non-linear curve fitting to assess the fraction of deformation-induced martensite as a function of strain. Afterward, Abaqus/Explicit method was utilized to achieve the stored energy and plastic strains distribution through the thickness. Then, Cellular automata and Galerkin-finite element models were... 

    Deformation Behavior and Effect of Strain Path on Strain-Induced Martensite Transformation in Austenitic Stainless Steel

    , M.Sc. Thesis Sharif University of Technology Lotfinia, Mahshad (Author) ; Serajzadeh, Siamak (Supervisor)
    Abstract
    In some of the austenitic stainless steels, the strain-induced martensite transformation occurs during the deformation processing owing to instability of austenite phase at low temperatures. In this study, formation of strain-induced martensite as well as the impact of strain path on the rate of martensite transformation in 316L austenitic stainless steel were investigated. At first, the multi-pass cold rolling experiments at room temperature and -8 ℃ were conducted in which both direct and reverse rolling layouts were taken into account. Then, as the third path, the uni-axial tensile loading with an appropriate strain rate was considered. After that, in order to examine the mechanical and... 

    Study of The Effect of Strain Rate on Cold Deformation Behavior and Mechanical Properties of 304L Austenitic Stainless Steel

    , M.Sc. Thesis Sharif University of Technology Mahmoudi, Alireza (Author) ; Serajzadeh, Siamak (Supervisor) ; Karimi Taheri, Ali (Supervisor)
    Abstract
    The stiffness rate of the 300 series austenitic stainless steel has long been known to depend on the stability of the austenite and its susceptibility to martensite formation. In this project, the cold deformation of austenitic stainless steel (304L) and the occurrence of martensite deformation during it are studied. Experimental cold rolling experiments under different strain velocities and initial temperatures in the range of -10° C to 25° C; Performed and microstructure, mechanical properties and percentage of martensite generated in rolled steel are determined and evaluated employing different testing techniques. mathematical modeling of cold rolling operation is also performed using... 

    Study of Direct Joining of Nanostructured-Zirconia to 430L Stainless Steel Produced by Co-sintering Process

    , Ph.D. Dissertation Sharif University of Technology Dourandish Yazdi, Mahdi (Author) ; Simchi, Abdolreza (Supervisor)
    Abstract
    In this study, the joint of co-sintered zirconia/stainless steel is investigated. To this end ZrO2-3mol%Y2O3 (TZP) and 430L stainless steel powders were utilized. The joining parameters of co-sintering in zirconia/metal were studied. In order to study the microstructure, diffusion and probable reactions at the joint boundary, HRSEM, HRTEM, EPMA and micro-focused XRD methods were employed. Shear strength of the joint was also measured. Finite element simulation of residual stresses and thermodynamic studies are utilized in the next step to analyze the experimental results. It is found that the direct joining of zirconia to 430L stainless steel is feasible by co-sintering at 1350 °C under low... 

    Characterization of Ss316l Powder Produced by Flame Spraying Method for Additive Manufacturing by Selective Laser Melting by Changing Machine Parameters

    , M.Sc. Thesis Sharif University of Technology Yousefi, Dorsa (Author) ; Sadrnezhaad, Khatiboleslam (Supervisor)
    Abstract
    Selective Laser Melting (SLM) process is a powder-based metal Additive Manufacturing (AM) technique. This developing industry has many advantages like generation of geometrically complex shapes with high density. High Cost, production and characterization of powders, limited material choices and process parameters optimization are some of the challenges associated with SLM. Stainless steel 316L due to its unique properties, like corrosion resistance, high strength, biocompatibility, availability and cost is indeed a commonly used material in SLM. In this research, the characterization of the powder produced by the flame spraying device, which is a new method, was discussed. Wire with 3mm... 

    Investigation on Modeling and Analytical Study and Bonding of Multi-Layer Copper-Austenitic Stainless Steel Roll Bonded Sheets

    , M.Sc. Thesis Sharif University of Technology Nouripour, Mohammad Hossein (Author) ; Akbarzadeh, Abbas (Supervisor)
    Abstract
    In the roll bonding process, the same and non-homogeneous metals are bonded to each other by rolling deformation, and the sheet produced exhibits multi-properties. Two- and three-layer copper and stainless steel sheets are used for a variety of purposes. Stainless steel-Copper bilayer sheets are not just cost effective in production, but also have mechanical and thermal benefits from the inherent properties of copper and stainless steel. In addition to its increased strength, good ductility, reduced thermal expansion and excellent soldering are other benefits. In the past, some researchers have been studied on the bonding strength and formability of austenitic stainless steel-copper bilayer... 

    Modeling of Welding Residual Stresses in Dissimilar Joint of Stainless Steel to Plain Carbon Steel

    , Ph.D. Dissertation Sharif University of Technology Ranjbarnodeh, Eslam (Author) ; Kokabi, Amir Hossein (Supervisor) ; Serajzadeh, Siamak (Supervisor)
    Abstract
    In this study, a thermo-mechanical model was utilized to investigate the welding residual stresses as well as thermal responses in dissimilar joint of carbon steel to stainless steel. A thermo-elastic-plastic analysis was first developed to assess temperature and deformation fields during and after welding operation. The employed model was capable of considering the effects of various factors such as, dilution, welding parameters and welding sequence on the developed residual stress as well as temperature distribution. In the next stage, the achieved predicted results together with EBSD data were used to correlate micro and macro residual plastic strains in the HAZ of the stainless steel... 

    Welding Metallurgy and Weldability of Martensitic Advanced High Strength Steel and Duplex Stainless Steels during Resistance Spot Welding

    , M.Sc. Thesis Sharif University of Technology Sobhani, Saeed (Author) ; Pouranvari, Majid (Supervisor)
    Abstract
    Duplex stainless steels and advanced high strength steels are both known as new materials in automobile industry applications. Process of resistance spot welding is the main process in welding of auto-body structures. Hence investigating the welding metallurgy and weldability of similar and dissimilar joints of duplex stainless steels and advanced high strength steel are crucial. The purpose of this study is to analyse the relationship between welding process and geometric characteristic of weld nugget, phase transformations of Weld nugget and heat affected zone, mechanical properties (i.e force bearing capacity and energy absorption capability) and failure mode (interfatial or pullout). in... 

    Electrophoretic Deposition of (Mn,Co)3O4 Spinel Coating for Solid Oxide Fuel Cell Interconnects

    , M.Sc. Thesis Sharif University of Technology Mirzaei, Mohamad Mahdi (Author) ; Faghihi Sani, Mohammad Ali (Supervisor) ; Simchi, Abdol Reza (Supervisor)
    Abstract
    Solid oxide fuel cell (SOFC) is one of the promising candidates for clean energy production. Due to the high operating temperature of SOFC, a protective coating is commonly applied on the surface of interconnects to prevent oxidation. In this study, electrophoretic deposition was employed to prepare a manganese-cobalt spinel coating on the surface of ferritic stainless steel (AISISAE430) substrates. MnCo2O4 powder with an average particle size of 60 nm was utilized and the sintering behavior of the coatings at different temperatures was studied. Non-isothermal and isothermal sintering behavior of the powder compacts were examined by employing a sensitive dilatometer. Master sintering curve... 

    Design and Manufactur, Medical Stent at Stainless Steel 316L

    , M.Sc. Thesis Sharif University of Technology Moghtada, Abdolmajid (Author) ; Akbarzadeh, Abbas (Supervisor)
    Abstract
    Due to increased mortality from Coronary Heart Disease, it is important to work on ways to treat this disease. An effective method of treatment on this disease is the coronary stent implantation. There are nearly two decades passed since implanting the first heart stent. The main objective of this research is design and manufacturing of the medical stents of stainless steel 316 L. Stent materials should have excellent corrosion resistance and biocompatibility. Various materials such as stainless steel 316 L, platinum alloys, niobium alloys, cobalt alloys are used for manufacturing the stents. In this project, at the first stage seam tube was prodected with laser welding of a tube with... 

    Application of Sol-Gel Technique to Synthesis of (Cu,Co)3O4 Spinel on Ferritic Stainless Steel used for Solid Oxide Fuel Cell Interconnects

    , M.Sc. Thesis Sharif University of Technology Paknahad, Pouyan (Author) ; Askari, Masoud (Supervisor)
    Abstract
    Due to recent progresses in lowering the temperature of SOFC, using metallic interconnects instead of ceramic interconnects was possible. Among the alloys used for interconnects, ferritic stainless steels (FSS) due to thermal expansion coefficient compatible with other cell components and cheap fabrication, have become the most widely used material for interconnects. Because of improvement of oxidation resistance of these FSSs, many studies have been made on coating of oxides on FSSs and results show that the spinel oxides have the best performance. In this study, the CuCo2O4 performance as coating in SOFC's interconnects was investigated. Coating process used was sol-gel dip coating and raw... 

    Manufacture, Mechanical Properties and Interfacial Corrosion of 316L/17-4PH Bimetals with a Nanostructured Ni Layer

    , M.Sc. Thesis Sharif University of Technology Salahi, Armita (Author) ; Simchi, Abdol Reza (Supervisor) ; Dolati, Abol Ghasem (Supervisor)
    Abstract
    Transient liquid phase (TLP) bonding of 316L/17-4PH bimetals using a thin layer of nanostructured nickel was studied. The nanostructured nickel interface was deposited through pulse current coating in a Watt bath. The TLP bonding was performed at different temperatures ranging from 1000 °C to 1300 °C using a nickel interface having different thicknesses (2-17µm) and crystallite size (14-67 nm). The microstructure of the joint bimetals and phase formation were studied using the optical and scanning electron microscopes and X-ray diffraction (XRD) method. The mechanical properties of the bimetals were evaluated by micro-hardness and shear tests. To evaluate the corrosion behavior of the... 

    , M.Sc. Thesis Sharif University of Technology Shirmohammadi, Davood (Author) ; Movahedi, Mojtaba (Supervisor)
    Abstract
    Martensitic stainless steels with high strength, good corrosion resistance and formability in the annealed condition are good choices for automotive applications, but they suffer from low weldability due to high hardenability and formation of brittle martensite without tempered structure in the weld metal and heat affected zone (HAZ). In other word, martensitic stainless steels have the worst weldability among all kinds of stainless steels. On the other hand, resistance spot welding is the main method for joining sheets in the automotive industry. Therefore, in the present work, microstructure and mechanical properties of the resistance spot welds of AISI 420 martensitic stainless steel in... 

    Upset Resistance Welding of Duplex Stainless Steel to Martensitic Stainless Steel

    , M.Sc. Thesis Sharif University of Technology Ozlati, Ashkan (Author) ; Movahedi, Mojtaba (Supervisor)
    Abstract
    Upset Resistance Welding (URW) is a solid-state joining process which can be used to join a variety of parts and profiles including railways, wheel rims and pipes used in oil and petrochemical industries. This process has three primary parameters, welding current, current passage time and mechanical pressure. Martensitic Stainless Steels (MSSs) due to high strength and wear resistance, good atmospheric corrosion resistance and relatively low price and Duplex Stainless Steels (DSSs) because of higher strength and better corrosion resistance in chlorine environments, are widely used in different industries. Dissimilar MSS/DSS joints are of great importance for piping, specially in oil and...