Sharif Digital Repository

Syntheses of coats including nickel nano-particles by electrodeposition have been
investigated for over 10 years. A method of testing according to surface reply was chosen
to reveal the effect of each pulse parameters (including duty cycle, frequency, average
current density, off time (toff) and on time (ton)) and the effect of saccharin concentration
on electroplating cathode efficiency, nanostructure. Pulse electroplating test of nickel was
composed by 30 tests. Pulse electroplating with relatively high peak current density was
employed and saccharine was added to increase deposition and rate of nickel nucleation on
surface. According to the results of cathode... 

In recent years, indirect methods of cancer detection that utilize changes in trace element levels in various parts of the body, such as hair and nails, have garnered significant attention from researchers.The primary objective of these methods is to identify alterations in trace element levels that serve as biological markers in the presence of disease. While direct examination of affected organs remains the gold standard for cancer diagnosis, it is often expensive, time-consuming, inconvenient, and associated with potential side effects. Therefore, if the effectiveness of this approach is validated, it could serve as a cost-effective, non-invasive, safe, and early diagnostic method in... 

In this study, the effect of external filter on the various parameters of image quality in digital industrial radiography by CR method for steel and aluminum piece has been investigated. The filter reduces the noise of scattered beams by absorbing the low-energy beams in the X-ray spectrum that are most likely to be scattered, but high filter thicknesses can attenuate the more energetic beams and have a negatively effect on the image quality. On the other hand, the absorption of those low-energy beams increases the average spectrum energy and thus reduce the contrast, so it is necessary to use the appropriate material and thickness of the filter. For this purpose, to examine the filter... 

Sharif University of Technology Plasma Focus (SUT-PF) is a Mather Type DPF device which has a 39 μF capacitor bank with 14 KV charging ability at its ultimate limit corresponding to 7 KJ stored energy. In the first step of this experiment, a test has been done at three distances 5, 7, 10 cm from anode tip with the different number of shots 20, 30, and 40 at 0 constant angles.In the following, a test is done at 5 and 10 degrees with 40 shots, and PF chamber has been filled up with nitrogen gas. Various tests have carried out for survey of this experiment, the result of which are as follow:The X-ray diffraction (XRD) analysis are used in order to reveal if the Nickel or Nickel nitride have... 

One layer mirrors are inexpensive and perform robustly across a broad range of angles, wavelengths, but they exhibit limited reflectivity. Multilayer interference mirrors are routinely used for optical applications requiring high reflectivity and wavelength selectivity. Although they can be designed to achieve a wide range of optical characteristics. One of the main applications of this multilayers in accelerators is guide outpot beamline to receive user. We can optimize these mirrors to give hight reflectivities, and outpot beam with reflect in canal that is equiped this mirrors reach to user. Conditions such as: material of layers, thickness and number of layers, surface roughness, …etc.... 

A soft X-ray spectrometer based on Johann's method and an embedded curved crystal is designed and fabricated for Sharif University of Technology's Plasma Focus (SUT-PF) in this project. Focusing rays with the same wavelength at a point to increase the ray intensity is the reason of choosing the cylindrical curved crystal spectrometer since its performance is inspired to the Bragg's law.The optimal conditions for SUT-PF (pressure and voltage) is adjusted and examined by photodiode detector and the camera pinhole before spectroscopy experiments. The diameter of generated hot spots is measured as 80 microns in the optimal condition.The recorded spectral lines on the radiography film and the... 

Non-destructive Testing (NDT) methodsare among the most important ways that are used for inspection of industrial products. It can measure non-visible properties of material such as defect size and inclusions that is inside of the object.NDT is included several tests such as visual examination, eddy current testing, ultrasonic testing and radiographic testing.Radiography is one of the most common NDT methods that are used to detect the defects in objects by registering an image of the object on the radiography film. Corrosion is one of the most important defects in pipelines, where the most important concern is measuring the remaining thickness in corroded zone.
In this study, some... 

In this project we studied Soft and Hard x-ray emissions from Sharif University of Technology’s Plasma Focus (SUT-PF) device filled with Argon gas. SUT-PF is a Mather type plasma focus device ( ). Our expriments have been done in various charging voltages ( ) and various filling pressures. Using different diagnostics X-ray’s intensity in each working condition (voltage and pressure) has been measured and finally these data analysed to find optimum conditions for maximum x-ray production in this device. Used diagnostics was: Rogowski coil, photodiodes combination with ultra thin metal foils, type Plastic scintillation detectors, and pinhole camera. In each shot, time resolved Rogowski coil,... 

Virtualizing the cloud data center as multiple VMs running parallel on a cloud server is a practical solution to the exponentially grown number of cloud users. The fluctuations in the number of required resources, like networking, storage, and computing resources, can be met by dynamic VM migration. The method by which cloud providers manage VMs and hardware resources to decrease costs and ensure the quality of services is of great importance, especially when the cloud is under a heavy workload. VM migration is one of the most fundamental and practical practices in managing the clouds. Despite all the benefits of VM migration, it also brings overhead on the source host, destination host, and... 

Capturing the atmospheric CO2 and turning it into value added products is a topic that has been extensively studied in recent years. One of the methods through which CO2 is valorized is via converting it into carbon nanofiber, CNFs. CNFs can be an important material in future human activities due to its valuable properties such as wide range of electrical conductivity, their superior flexibility and strength, But it is currently obstructed in use due to the high cost of manufacturing and the complexity of the synthesis. Furthermore, in today's world, human life is heavily influenced by greenhouse gases, and avoiding emitting gases like CO2, is almost infeasible. This thesis provides an... 

In the classical theories of plasticity, plastic deformation of material is modeled with a macro- scopic viewpoint and without considering the existing physical mechanisms at the crystal scale. However, plastic deformation stems from slip phenomena and evolution of crystalline structure. Furthermore the effects of initial texture of material on its mechanical properties, like formability, and also texture evolution of material can only be calculated by considering these physical mecha- nisms.The main purpose of this thesis is to predict forming limit diagrams of sheet metals based on crystal plasticity approach by considering the effect of initial material texture and presentation of... 

The g-C3N4/Fe2O3 nanocomposite was produced by the combustion synthesis. The product was characterized by x-ray diffraction (XRD), field-emission scanning electron microscopy (FE-SEM), Fourier-transform infrared spectroscopy (FTIR), Brunauer-Emmett-Teller study (BET), Ultraviolet-visible analysis (UV-vis) and photoluminescence measurement (PL). Effect of iron nitrate on stability and photocurrent density under simulated visible-light irradiation was determined. The highest photocurrent density obtained (4.25 μA/Cm2) was twelve times the pure g-C3N4. This improvement was due to a bandgap decrease, the specific surface area increase, reduction of the electron-hole recombination, and... 

Cadmium sulfide (CdS) thin films were successfully fabricated in argon atmosphere on glass slides and Single Layer Graphene(SLG)/Cu foil stack by close space sublimation technique in three different deposition temperatures. Successive Ionic Layer Adsorption and Reaction (SILAR) technique is used as a complementary technique for better and denser layers. Analysis techniques such as Grazing Incident X-ray Diffraction (GIXRD) and Scanning Electron Microscope images were used for structural study of the deposited layers. Polycrystallinity and hexagonal wurtzite structure of the thin films is confirmed. For band gap calculations and for determination of optical behavior of the layers in different... 

Designing a system based on 2 to 5 MeV electron accelerators for X radiation of urban waste.Nowadays , the use of ionizing radiation in two cases of treatment and removal of contaminants in the waste including; 1) Pathological hospital waste 2) leachate from buried urban waste, which is studied and examined in this project. Buried urban wastes begin to break down under aerobic and anaerobic processes, and as long as the materials are not changed into sustainable materials, these processes will continue and results in landfill gas and leachate. Gas is produce due to anaerobic processes and leachate which is produced through water infiltration (atmospheric precipitation) in the landfill or... 

In this project, the aim is finding the corrosion behavior and biocompatibility of metallic biomaterials in simulated body fluids.by this study we can have a wide knowledge about the behavior and use of metallic biomaterials.in this project we use three base metals. Ti (grade 5 and grade 2), stainless steel (316L and 316) and Mg alloy(AZ91 and AZ31). the media was six physiological environment( Cigada solution, Hank solution, SBF solution, Fusayama solution, Ringer solution and Tyrod’s solution). all of these environments are related to the body fluids except Fusayama solution that is an artificial saliva and is a mouth fluid. we used polarization tests to determine the corrosion behavior... 

Although studies have shown interesting piezoelectric and dielectric properties of PZT containing composite piezoelectric ceramics, there has been no systematic investigation on the PZT-PCN, especially on the porous one.In this study, the dense ceramics of 0.8Pb (Zr1/2Ti1/2)O3–0.2Pb(Co1/3Nb2/3)O3 abbreviated to (PZTCN) systems were successfully prepared by the columbitewolframite precursor method via the mixed oxide technique. Porous PZT-PCN ceramics were prepared by burnable plastic sphere process (BURPS) technique with three types of pore forming agents (PFAs), poly vinyl chloride (PVC), stearic acid (SA), and poly methyl methacrylate (PMMA) at different weight percentages(5, 10,and 15... 

Recently, low temperature carburizing of stainless steels, especially austenitic stainless steels, have been considered by so many researchers. The improvement of tribological properties of which is so impressive so much so that such properties like hardness and wear resistance increase to manifold. In this research, low temperature carburizing was done on two kinds of precipitation hardenable stainless steels 17-4 and 13-8 Mo. After that, microstructural investigations were done on the carburized surfaces and in 5, 10, 20, 80, and 150 micrometer depths. Moreover, in each depth, in order to phase structure and tribological properties investigation, XRD and microhardness tests were done,... 

In the present study, nanocomposite of Ce-TZP/Al2O3 was synthesized via aqueous combustion synthesis. In order to investigate the effects of alumina on the morphology and the mechanical properties of this nanocomposite, four sample with 20, 40, 60 and 80 mole percent of alumina were prepared. At first, the synthesized powders were characterized with scanning electron microscope and X-ray diffraction technique. Then, in order to determine the effects of alumina mole percent on the mechanical properties of the nanocomposite, the powders were uniaxailly compacted with the press of 250 MPa followed by sintering at the temperature of 1400 °C for 4 hours. The density of the compacted powders was... 

In this study, nano-powders of copper-cobalt spinel (CuCo2O4) were fabricated by solution combustion synthesis (SCS) of Cu and Co nitrates with urea, glycine,acid citric and alanine. The method involved exothermic decomposition of viscous liquid nitrates and the fuel. Products which were synthesized by using this fuels contained less impurity constituents. Duo to low purity, other factors which have influence on synthesis process investigated and observed that pH have key role on process. X-ray diffraction (XRD) patterns gave crystal structure and the existing phases. Particle size distribution and morphology changes were studied by dynamic light scattering (DLS) and field emission scanning... 

In this study, Cu-TiC nanocomposites were produced by high energy ball milling of elemental powders and in situ formation of TiC in the copper base. Cu and 5,10,20 and 40 wt% Ti powder blend were milled for 60 h, then graphite powders were added and milling was continued for 10 h again and Finally Cu-TiC composite powders with 10.68, 20.16, 36.24 and 60.25 vol% of reinforcements (6.18, 12.2, 23.82 and 45.47 wt%) were produced. The effect of time on the solution of titanium in the copper was studied by X-Ray diffraction analysis (XRD). crystallite size and lattice strain of copper were determined 12nm and 1.04% subsequently for Cu-40wt%TiC after 60 h milling. to ensure the formation of...