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    Effect of silicon carbide nanoparticles on hot deformation of ultrafine-grained aluminium nanocomposites prepared by hot powder extrusion process

    , Article Powder Metallurgy ; Volume 59, Issue 4 , 2016 , Pages 262-270 ; 00325899 (ISSN) Mobarhan Bonab, M. A ; Simchi, A ; Sharif University of Technology
    Taylor and Francis Ltd 
    Abstract
    The flow behaviour of Al–SiC nanocomposites prepared by mechanical milling and hot powder extrusion methods was studied at different temperatures (350–500°C) and strain rates (0.005–0.5 s−1). The flow of the Powder metallurgy nanocomposites exhibited a peak stress followed by a dynamic flow softening behaviour. It was shown that mechanical milling increased high-temperature strain rate sensitivity of ultrafine-grained (UFG) aluminium while decreasing its flow dependence to temperature. Constitutive analysis of the hot deformation process by Zener–Hollomon parameter (Z) also indicated a remarkable increase in the deformation activation energy (about 40%). Likewise, SiC nanoparticles (up to... 

    Fabrication and characterisation of ultrafine-grained Al-5vol%Al 2O3 nanocomposite

    , Article International Journal of Nanomanufacturing ; Volume 5, Issue 3-4 , 2010 , Pages 341-351 ; 17469392 (ISSN) Razavi Hesabi, Z ; Simchi, A ; Seyed Reihani, S. M ; Simancik, F ; Sharif University of Technology
    Abstract
    Nanocrystalline Al-5vol%Al2O3 nanocomposite was synthesised by mechanical milling of a mixture containing nanometric alumina with an average particle size of 35 nm. Morphology of as-synthesised powder was investigated by SEM while crystallite size of Al matrix was determined by XRD analysis. The results confirmed formation of nanocrystalline Al matrix induced by severe plastic deformation during mechanical milling. Nanocomposite bars were produced by hot powder extrusion route. TEM investigation of as-extruded nanocomposite revealed formation of elongated grains along the extrusion direction decorated by alumina nanoparticles. Tensile and compressive properties of as-extruded nanocomposite... 

    The effect of deformations passes on the extrusion pressure in axi-symmetric equal channel angular extrusion

    , Article Computational Materials Science ; Volume 44, Issue 4 , 2009 , Pages 1116-1125 ; 09270256 (ISSN) Eivani, A.R ; Ahmadi, S ; Emadoddin, E ; Valipour, S ; Karimi Taheri, A ; Sharif University of Technology
    2009
    Abstract
    The most applicable configuration of the equal channel angular extrusion (ECAE) dies is the axi-symmetric one. However, most of the previous analytical solutions are focused on the plane strain conditions. In this research, an upper bound model is used to investigate the deformation of the material during axi-symmetric ECAE. The analysis considers the effect of die angle, friction between the sample and the die walls, and the angle of the outer curved corner of the die, on the extrusion pressure. It is found that increasing the die angle and outer curved corner angle and decreasing the friction coefficient results in decreasing extrusion pressure. The proposed model is verified using two... 

    Oxygen barrier properties of poly(ethylene terephthalate) nanocomposite films

    , Article Macromolecular Materials and Engineering ; Volume 294, Issue 1 , 2009 , Pages 68-74 ; 14387492 (ISSN) Frounchi, M ; Dourbash, A ; Sharif University of Technology
    2009
    Abstract
    Nanocomposites of poly(ethylene terephthalate) and two different montmorillonite-based organoclays were prepared by a co-rotating twin screw extruder. Dispersion of nanoclays in the polymer matrix was examined by TEM and XRD. Nanocomposites with lower content of organoclay showed exfoliated morphology while by increasing the amount of organoclay the intercalated morphology was more prevalent. Both organoclays had a good intercalation with PET and were uniformly dispersed within the polymer. Oxygen permeability of thin films of nanocomposites showed that the nanocompo-sites had better oxygen barrier properties than the neat PET. Tensile and impact properties of the nanocomposites also were... 

    Investigating the effect of heat treatment on the fracture toughness of a hot extruded Al–Ti composite produced by powder metallurgy route

    , Article Materials Science and Engineering A ; Volume 771 , 2020 Rezaei, A ; Madaah Hosseini, H. R ; Sharif University of Technology
    Elsevier Ltd  2020
    Abstract
    An Al-5 wt% Ti composite was fabricated via powder metallurgy technique and hot extrusion. The produced composite samples were heat-treated subsequently at 600 °C for various time durations of 0, 4 and 10 h to achieve different volume fractions of the intermetallic Al3Ti phase. Pure aluminum sample was produced as a benchmark specimen to be compared to the composite samples. SEM studies were used to investigate the microstructure of the composite samples, and it was revealed that core-shell structured particles were formed in the composite heat-treated for 4 h. Triple point bending test was performed on the single edge notched beam specimens of the heat-treated Al-5 wt% Ti composite and the... 

    Comprehensive structural and mechanical characterization of in-situ Al–Al3Ti nanocomposite modified by heat treatment

    , Article Materials Science and Engineering A ; Volume 785 , 2020 Tamizi Junqani, M ; Madaah Hosseini, H. R ; Azarniya, A ; Sharif University of Technology
    Elsevier Ltd  2020
    Abstract
    Aluminum-Al3Ti reinforced MMCs were produced with a large amount (up to ~30 vol%) of Al3Ti phase via mechanical alloying, hot extrusion and heat treatment (as a supplementary process) of the Al–Ti elemental powder mixture, respectively. Samples in each stage were studied precise and comprehensive by field emission electron microscope, energy dispersive spectroscopy, X-ray diffraction, differential scanning calorimetry, densitometry, macro and micssro hardness, nanoindentation and tensile tests. The results indicated that after 4-h vibratory milling, the aluminum crystallite size reached 63 nm and Al3Ti phase formed in powder mixture. After hot extrusion, the volume percentage of Al3Ti... 

    Microstructural features, texture and strengthening mechanisms of nanostructured AA6063 alloy processed by powder metallurgy

    , Article Materials Science and Engineering A ; Volume 528, Issue 12 , 2011 , Pages 3981-3989 ; 09215093 (ISSN) Asgharzadeh, H ; Simchi, A ; Kim, H. S ; Sharif University of Technology
    Abstract
    Nanostructured AA6063 (NS-Al) powder with an average grain size of ~100. nm was synthesized by high-energy attrition milling of gas-atomized AA6063 powder followed by hot extrusion. The microstructural features of the consolidated specimen were studied by transmission electron microscopy (TEM) and electron backscatter diffraction (EBSD) techniques and compared with those of coarse-grained AA6063 (CG-Al) produced by hot powder extrusion of gas-atomized powder (without using mechanical milling). The consolidated NS-Al alloy consisted of elongated ultrafine grains (aspect ratio of ~2.9) and equiaxed nanostructured grains. A high fraction (~78%) of high-angle grain boundaries with average... 

    Development of Nanostructural Al-Mg-Si Alloys using ECAE and Ageing Processes

    , Ph.D. Dissertation Sharif University of Technology Vaseghi, Majid (Author) ; Karimi Taheri, Ali (Supervisor)
    Abstract
    The manufacture of ultra high strength materials has always been a target for aerospace and transportation industries. Currently, the limitation of energy resources even makes this goal more serious. Nowadays, more than 50% of total extrusion products are made from Al alloys and around 90% of them are the 6000 series alloys. Therefore, regarding to high strength, low weight, and hardening aluminum AA6000 alloys capabilities can play a major role in fulfilling this task. Over the last decade, a number of techniques collectively referred to as severe plastic deformation (SPD), have emerged as a promising approach for the production of bulk ultrafine-grained (UFG) nano-structured materials.... 

    Study on Hot Extrusion of AA2017-10%SiCp

    , M.Sc. Thesis Sharif University of Technology Ranjbar Motlagh, Sasan (Author) ; Serajzade, Siamak (Supervisor)
    Abstract
    In this study, hot extrusion of AA2017-10%SiC¬p composite during deformation process and effect of deformation parameters on mechanical properties have been investigated. At the first step, hot compression tests have been carried out to obtain the flow behavior of the material at different temperatures and strain rates. The activation energy of hot deformation was calculated 296 Kj/mol. In the next step, by using a finite element model in ABAQUS software and the results of uniaxial hot compression test behavior of AA2017 and AA2017-10%SiC¬p during hot and warm extrusion have been investigated. By using it temperature gradient and velocity field and strain distribution were predicted. In the... 

    Prediction of Deformation Field And Temperature Distribution in Extrusion of Composite AA6061-10%SiC(p)

    , M.Sc. Thesis Sharif University of Technology Goodarzi Hosseinabadi, Hossein (Author) ; Serajzadeh, Siamak (Supervisor)
    Abstract
    In this research, the extrusion of composite AA6061-SiC has been investigated and the temperature distribution field and energy required for the process has been predicted. In this regard, to predict the flow behavior of material, hot extrusion tests conformed at various ranges of temperatures and strain rates. Afterward, the finite element method coupled with the upper bound technique to calculate the temperature distribution and energy required during hot extrusion. This model has also used for wire drawing and cold extrusion processes. The present model is capable of considering various process parameters such as speed of extrusion, reduction and the initial billet/die temperature on the... 

    An Investigation of Strain, Temperature Distribution and Mechanical Properties of Product in Hot Extrusion of AA7075

    , M.Sc. Thesis Sharif University of Technology Imenabadi, Amir (Author) ; Karimi Taheri, Ali (Supervisor)
    Abstract
    More than 70% of the components used in aerospace, aircraft and defence industries Are made of aluminum alloys. The 7xxx series of Al alloys such as AA7075 and AA7175 are typical alloys utilized in the mentioned industries. For these alloys, the optimization of the extrusion process in term of reaching a maximum extrusion quality without jeoparding the extrudate, the surface and microstructural properties is far more complex than other aluminum alloys. It is generally accepted that product properties are closely correlated to microstructure. So it is of paramount importance to understand the way in which the structure is modified and how the forming parameters i.e. temperature, ram speed,... 

    Microstructure Optimization of In-situ Al-Al3Ti Nanocomposite Fabricated by Mechanical Alloying & Hot Extrusion for Improving the Fracture Toughness

    , Ph.D. Dissertation Sharif University of Technology Basiri Tochaee, Ensie (Author) ; Madaah Hosseini, Hamid Reza (Supervisor) ; Seyyed Reihani, Morteza (Supervisor)
    Abstract
    The aim of this research was to fabricate an in-situ Al-Al3Ti nanocomposite from pure microsized aluminum and titanium powders by mechanical alloying and hot extrusion without any usage of nanometric particles or applying secondary heat treatments. The focus of the present research was fabricating a nanocomposite material with high strength, modulus and hardness accompanied with high fracture toughness that could be comparable with aluminum alloys in terms of fracture toughness. Mechanical alloying and hot extrusion techniques were employed to produce in-situ fully dense Al-Ti composites. Platenary and high energy vibratiory mill was used to produce composites with different percent of... 

    Theoretical and Practical Study of Deformation Behavior of AlMg6 Alloy

    , Ph.D. Dissertation Sharif University of Technology Gholamzadeh, Abolfazl (Author) ; Karimi Taheri, Ali (Supervisor)
    Abstract
    Aluminum alloys are widely used in many applications in aerospace and automotive industries. Therefore, the study of the effects of different parameters such as chemical composition, temperature, strain, strain rate and recovery and recrystallization phenomena being more effective on controlling of microstructure and final properties of product, are more important. In this research, deformation behavior of AlMg6 alloy has been studied from two theoretical and experimental views as described below: In ambient temperature deformation, the mechanical properties in correlation on the microstructures developed at different temperatures have been assessed. The results of tensile test demonstrated... 

    Optimization of the Positions of Holes in Multi-hole Extrusion Dies with Unsymmetrical Holes for Minimization of the Curvature of the Exiting Profile

    , M.Sc. Thesis Sharif University of Technology Nazari Onlaghi, Sina (Author) ; Assempour, Ahmad (Supervisor)
    Abstract
    In this study, a two-hole die with unsymmetrical T-shape holes has been investigated. At first, a kinematically admissible velocity field in outlet of die has determined. Then, appropriate length of die has calculated by upper bound method. Finally, suitable position of holes has achieved in aspect of minimum pressure and curvature. To calculate curvature of exit profile, a realistic deviation function has been defined. To validation of results, finite element simulation and physical modeling have been used. Analytical, experimental and finite element results have decent agreement to each other  

    Preparation and Forming of Nerve Growth Channels from Polymeric Nanocomposite by Solution Extrusion and Studing their Properties

    , M.Sc. Thesis Sharif University of Technology Bayat, Arman (Author) ; Ramazani Saadatabadi, Ahmad (Supervisor)
    Abstract
    The nervous system is the most complex body system and controls other body systems. Damages of the peripheral nervous system will interfere with the functioning of the body. Tissue engineering is used as one of the most effective methods for repairing damaged tissues,by providing 3-dimensional (scaffold) bedding with proper properties, allows the proliferation of Myelin sheath and proliferation of axons. In this study, we used a continuous extrusion process, sodium alginate with different percentages of Polyaniline-Graphene nanoparticle (synthesized by solvent emulsion) was extruded and its properties were determined by FTIR, SEM, MTT, tensile properties, Conductivity, contact angles and... 

    Fabrication and Characterization of Al/Al3Ti-Al2O3 Composites by Powder Metallurgy and Sol Gel and Consideration of Mechanical Properties and their Correlation with the Microstructure Evolution

    , M.Sc. Thesis Sharif University of Technology Azarniya, Abolfazl (Author) ; Maddah Hosseini, Hamid Reza (Supervisor)
    Abstract
    In the present research, a novel method for the fabrication of Al/Al3 Ti-Al2O3 composites and nanocomposites based on the thermal degradation of the refectory ceramic “Aluminium Titanate (AT)” or Al2TiO5 by powder metallurgy route. This research encompasses some precise subsequent steps. At first stage, nanostructured aluminium titanate nanofibers and particles were synthesized via a citrate sol gel process in which citric acid was used as a chelating agent. At second step, the possible chemical reactions between Al and aluminium titanate were taken into consideration both in powder form and in bulk form. Thermal analysis results indicated that it is feasible to decompose aluminium titanate... 

    Study of Mechanical Properties of High Tempreture Al Nano-composites with Al2O3-Al3Ti based on theThermal Degradation of Aluminium Titanate

    , M.Sc. Thesis Sharif University of Technology Lotfi, Nasrin (Author) ; Madaah Hosseini, Hamid Reza (Supervisor)
    Abstract
    In this study, in situ Al-Al3Ti-Al2O3 nanocomposite has been fabricated on thermal decomposition of tialite (Al2TiO5 or AT) precursor in the aluminum matrix through powder metallurgy method. The high-temperature mechanical property of Al-Al3Ti-Al2O3 on this procedure has been investigated. In the first step nano-structured tialite were synthesized through citrate sol-gel methods. Then 3.5 wt.% tialite powder was mixed with aluminum by high energy vibratory milling for 3 hours. In the next step, green compacts of mechanically milled powder mixtures were sintered at 530°С for 6 hours under argon atmosphere. In the final step, hot extrusion as a consolidation method reduces the sample voids,... 

    Microstructure Features and Mechanical Properties Microtubes of WE43 Magnesium Alloys for Biodegradable Vascular Stent Application

    , M.Sc. Thesis Sharif University of Technology Torabi Kafshgari, Mehran (Author) ; Akbarzadeh, Abbas (Supervisor)
    Abstract
    Magnesium and its alloys have gained much attention in medical applications, especially bio-degradable stents. However, they have not been used extensively due to their natural limitations, such as weak mechanical properties. WE43 magnesium alloy has gained attention as a bio-alloy due to its high temperature and good corrosion resistance. The present study aims to use a combination of ECAP and direct tube extrusion to fabricate thin wall tubes with good mechanical properties using WE43 magnesium alloy. In the first phase, the ECAP process at 370°C were conducted up to 4 passes on the homogenized samples to reach ultrafine grain structure. Subsequent to ECAP, direct tube extrusion at 230 °C,... 

    An Investigation on the Diffusion Welding of Aluminum to Copper Using ECAE Process

    , M.Sc. Thesis Sharif University of Technology Eslami, Peyman (Author) ; Karimi Taheri, Ali (Supervisor)
    Abstract
    A new method for production of bimetallic rods, utilizing the equal channel angular extrusion (ECAE) process has been introduced before by previous researchers, but no attempt has been made to assess the effect of different temperatures and holding times in order to achieve a diffusional bond between the mating surfaces. In present research copper sheathed aluminum rods have been ECAEed at room temperature and subsequently held at a constant ECAE pressure, at different temperatures and holding times to produce a diffusional bond between the copper sheath and the aluminum core. The bonding quality of the joints was examined by shear strength test. The microstructure examinations were carried... 

    Characterization of anisotropic behaviour of ZK60 extrusion under stress-control condition and notes on fatigue modeling

    , Article International Journal of Fatigue ; Volume 127 , 2019 , Pages 101-109 ; 01421123 (ISSN) Pahlevanpour, A. H ; Behravesh, S. B ; Adibnazari, S ; Jahed, H ; Sharif University of Technology
    Elsevier Ltd  2019
    Abstract
    The anisotropic fatigue behavior of ZK60 is investigated through stress-control tests along two different material directions: extrusion (ED) and radial (RD) directions. The in-plane random texture along RD promotes activation of twinning/detwinning deformations in both tension and compression reversals, which brings about a sigmoidal but near-symmetric shape for hysteresis loops. The stress-strain response along ED is asymmetric, which is attributed to different deformation mechanisms in tension and compression reversals. The higher fatigue strength along ED is related to lower plastic strain energy in this direction. An energy damage parameter showed a good correlation with tests performed...