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Free Content Selective synthesis of conjugated enynes from α-arylalkynols using LiCl-Acidic Al2O3 under solvent-free conditions  

7H-benzimidazo[2,1-a]benz[de]isoquinolin-7-one compounds were prepared in a selective manner by reaction between o-phenylenediamines and appropriate 1,8-naphthalenedicarboxylic anhydrides using acidic alumina under microwave irradiation  

Free vibration response of a joined shell system including cylindrical and spherical shells is analyzed in this research. It is assumed that the system of joined shell is made from a functionally graded material (FGM). Properties of the shells are assumed to be graded through the thickness. Both shells are unified in thickness. To capture the effects of through-the-thickness shear deformations and rotary inertias, first-order shear deformation theory of shells is used. The Donnell type of kinematic assumptions is adopted to establish the general equations of motion and the associated boundary and continuity conditions with the aid of Hamilton’s principle. The resulting system of equations is... 

Free vibration response of a cylindrical shell closed with two hemispherical caps at the ends (hermit capsule) is analysed in this research. It is assumed that the system of joined shell is made from functionally graded materials (FGM). Properties of the shells are assumed to be graded through the thickness. Cylindrical and hemispherical shells are unified in thickness. To capture the effects of through-the-thickness shear deformations and rotary inertias, first order theory of shells is used. Donnell type of kinematic assumptions are adopted to establish the general equations of motion and the associated boundary and continuity conditions with the aid of Hamilton's principle. The resulting... 

Free vibration response of a cylindrical shell closed with two hemispherical caps at the ends (hermit capsule) is analysed in this research. It is assumed that the system of joined shell is made from functionally graded materials (FGM). Properties of the shells are assumed to be graded through the thickness. Cylindrical and hemispherical shells are unified in thickness. To capture the effects of through-the-thickness shear deformations and rotary inertias, first order theory of shells is used. Donnell type of kinematic assumptions are adopted to establish the general equations of motion and the associated boundary and continuity conditions with the aid of Hamilton's principle. The resulting... 

In this paper, we consider a dual-sourcing model with constant demand and stochastic lead times. Two suppliers may be different in terms of purchasing prices and lead-time parameters. The ordering takes place when the inventory level depletes to a reorder level, and the order is split among two suppliers. Unlike previous works in the order splitting literature, the supply lead time between vendor and buyer as well as unit purchasing prices is considered to be order quantity dependent. The proposed model finds out the optimal reorder point, order quantity and splitting proportion, using a solution procedure. Numerical results show that neglecting the relationship between ordering batch size... 

Adsorption of human serum proteins (Albumin and total protein) onto high purity synthesis nano-hydroxyapatite (HA), Ca 10(PO 4) 6(OH) 2, has been studied in a wide temperature range by UV-visible spectrophotometer. Adsorption isotherm is basically important to describe how solutes interact with adsorbent, andiscriticalinoptimizing the use of adsorbent. Inthe present study, the experimental results werefitted tothe Langmuir, Freundlich, Temkin and Dubinin-Radushkevich (DR) models to obtain the characteristic parameters of each model and square of the correlation coefficients (R 2). According to the results, the DR isotherm model had the best agreement with the experimental data. The effect of... 

We show that a metal-organic framework (MOF) sustained by a nanosized Ag12 cuboctahedral node can be applied to selectively extract traces of lead(II) ion from environmental water samples. The MOF was characterized by thermogravimetric and differential thermal analysis, scanning electron microscopy, FTIR, and X-ray diffraction. The effects of pH value, flow rates, of type, concentration and volume of the eluent, of break-through volume and potentially interfering ions on the separation and determination of lead were evaluated. Following desorption with EDTA, Pb(II) was quantified by FAAS. The use of the MOF results in excellent analytical figures of merit including an analytical range from 2... 

In this research, copper matrix composites reinforced with different amounts of titanium carbide particles were produced by mechanical milling and in-situ formation of reinforcements. Morphology and size of milled powders were inspected by scanning electron microscopy (SEM) several times during milling process. Changes in lattice parameter, crystallite size, lattice strain, dislocation density and Gibbs free energy changes (due to increasing in dislocation densities and grain boundaries) in different samples (with different TiC particles contents) were studied by X-Ray Diffraction technique with Cu-kα radiation and using Nelson-Riley method and Williamson-Hall equation. Microstructure of...