Sharif Digital Repository

Electromagnetic levitation gas condensation (ELGC) method was used to synthesize silver nanoparticles (NPs). Silver droplets were melted and levitated stably at about 1130°C with appropriate flat coils in a 10mm OD silica tube. High purity argon, nitrogen and helium were employed as carrier gases and cooling media. Morphology and particle size of the products were investigated by scanning and transmission electron microscopy (SEM and TEM), X-ray diffraction (XRD), energy dispersive X-ray analysis (EDAX) and dynamic light scattering (DLS). The DLS, SEM and TEM studies demonstrated narrow size distribution of spherical shape silver NPs with mean particle size of about 60, 50 and 30nm... 

Mathematical simulation of non-isothermal multiphase flow in deformable unsaturated porous media is a complicated issue because of the need to employ multiple partial differential equations, the need to take into account mass and energy transfer between phases and because of the non-linear nature of the governing partial differential equations. In this paper, an analytical solution for analyzing a fully coupled problem is presented for the one-dimensional case where the coefficients of the system of equations are assumed to be constant for the entire domain. A major issue is the non-linearity of the governing equations, which is not considered in the analytical solution. In order to... 

Ultra clean NiTi shape memory alloy was produced by electron beam melting of Ni rich vacuum inductionally melted butts together with pure Ti chunks in both condensed and electrographite crucibles. A hollow cathode discharge gun was used for heating up to 1623, 1653 and 1693 K and holding the charge materials under vacuum for 300, 600, 900 and 1200 s. Effects of temperature, time and compactness of the crucible on formation/disappearance of the hard compounds like Ni3Ti, Ti4Ni2O, Ti4Ni 2C, Ti3Ni2OC and TiC were determined by X-ray diffraction, scanning electron microscopy and energy dispersive X-ray analysis. A combination of the experimental results with the kinetic rate equations indicated... 

Background: Genistein (C15H10O5) is a soy isoflavone with anti-cancer properties such as inhibition of cell growth, proliferation and tumor invasion, but effective dosage against hematopoietic malignant cells was not in non-toxic range. This property cause to impede its usage as chemotherapeutic agent. Therefore, this hypothesis raised that synthesizing biocompatible nanoparticle could assist to prevail this struggle. Methods: Genistein covalently attached on Fe3O4 nanoparticles decorated with carboxymethylated chitosan to fabricate Fe3O4-CMC-genistein in alkaline circumstance. This obtained nanoparticles were evaluated by TEM, DLS, FTIR, XRD and VSM and its anti-cancer effect by growth rate... 

Nanostructured Ag@SiO2-Penicillin was synthesized from high-purity Ag0 NPs with a mean particle size of about 10 nm produced by electromagnetic levitation gas condensation (ELGC) method. The silver and penicillin contents of the synthesized nano-antibiotic were about 34 wt% and 2.5 wt% respectively, as determined by ICP-OES and TGA analyses. The antibacterial properties and synergistic effects of nanostructured Ag@SiO2 and Ag@SiO2–Penicillin on killing the Methicillin-susceptible S. aureus (MSSA) and Methicillin-resistant S. aureus (MRSA) bacteria were also examined. The nanoparticles were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Ag@SiO2-Penicillin... 

In this paper, an analysis is presented of some bronze vessels from recent excavations at the first millennium BC site of Sangtarashan in eastern Luristan, Iran, according to metallography (OM), ICP-OES and SEM-EDS methods to identify alloying as well as manufacturing processes. This study provides new evidence for a better understanding of the bronze archaeometallurgy during the Iron Age in Iran. It concludes that the artifacts contain homogenous and single phase tin bronze (Cu-Sn) alloy. The Sn content in the artifacts also allowed to apply mechanical operations on the vessels without causing brittleness. Apart from tin, other elements that are classified as trace elements were present,... 

In this research, organic solvent composed of hexane and methanol was used for lipid extraction from dry and wet biomass of Chlorella vulgaris. The results indicated that lipid and fatty acid extraction yield was decreased by increasing the moisture content of biomass. However, the maximum extraction efficiency was attained by applying equivolume mixture of hexane and methanol for both dry and wet biomass. Thermodynamic modeling was employed to estimate the effect of hexane/methanol ratio and moisture content on fatty acid extraction yield. Hansen solubility parameter was used in adjusting the interaction parameters of the model, which led to decrease the number of tuning parameters from 6... 

Objective(s): Hepatitis B virus infection causes chronic disease such as cirrhosis and hepatocellular carcinoma. The metabolomics investigations have been demonstrated to be related to pathophysiologic mechanisms in many disorders such as hepatitis B infection. The aim of this study was to investigate the saliva metabolic profile of patients with chronic hepatitis B infection and to identify underlying mechanisms as well as potential biomarkers associated with the disease. Materials and Methods: Saliva from 16 healthy subjects and 20 patients with chronic hepatitis B virus were analyzed by nuclear magnetic resonance (NMR). Then, multivariate statistical analysis was performed to identify... 

Tissue engineering (TE) and regenerative medicine have held great promises for the repair and regeneration of damaged tissues and organs. Additive manufacturing has recently appeared as a versatile technology in TE strategies that enables the production of objects through layered printing. By applying 3D printing and bioprinting, it is now possible to make tissue-engineered constructs according to desired thickness, shape, and size that resemble the native structure of lost tissues. Up to now, several organic and inorganic materials were used as raw materials for 3D printing; bioactive glasses (BGs) are among the most hopeful substances regarding their excellent properties (e.g., bioactivity...