Sharif Digital Repository

A hot filament chemical vapor deposition (HFCVD) method was used to prepare Fe-Cr thin film on Si substrate. The produced layers were used as catalysts for growing carbon nanotubes (CNTs) from liquid petroleum gas (LPG) at 825 °C by thermal CVD (TCVD) method. To characterize the obtained catalysts or CNTs, X-ray Photoelectron Spectroscopy (XPS), Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM) and Raman spectroscopy were used. CNTs were grown on HFCVD derived Fe-Cr catalyst with the LPG as carbon source successfully. It was found that an annealing process on catalysts enhances the surface concentration of Cr atoms and reduces the sizes of catalyst particles. The... 

In this study a hot filament chemical vapour deposition (HFCVD) technique was used to prepare Fe-Cr films on Si substrate as catalysts for thermal CVD (TCVD) growing of carbon nanotubes (CNTs) from liquid petroleum gas (LPG) at 800 °C. To characterize the catalysts or CNTs, X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Raman spectroscopy were used. The XPS spectra obtained at different stages of Ar+ sputtering revealed that in the depth of catalyst layers, the relative Fe-Cr concentrations are higher than the top-surface. SEM images of samples after TCVD indicate a significant CNT growing at the backside of catalyst... 

TCVD growth of multiwalled carbon nanotubes (MWCNTs) was reported by catalytic decomposition of liquefied petroleum gas (LPG) at a temperature range of 580800 °C. Laser ablation was employed as a simple and rapid technique to produce Pd nanoparticles which possess effective catalytic activities for CNT synthesis. UVvisible spectroscopy and TEM images confirmed that the Pd nanoparticles are stable for a long time and have rather spherical shape with average size of 7 nm. SEM and TEM observations and Raman spectroscopy demonstrated that the CNTs have a wavy structure, dense morphology and acceptable crystallinity. Since Pd nanoparticles are inactivated or agglomerated at extremes of the... 

Ni-Si mixed oxide nanocomposite was prepared by co-precipitation method with Ni(NO 3) 2 ·6H 2O and tetraethylorthosilicate (TEOS) at pH = 10.5 under reflux condition for 6 days. It was then used as a catalyst for the formation of carbon nanotubes (CNTs) by CVD procedure. Characterization of the catalyst and the CNTs was carried out using X-ray diffractometry (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy. The results showed that Ni-Si mixed oxides nanorods with the average diameter of 3 to 4 nm play a key role in CNTs formation  

Heat transport features of a dusty fluid flow within a resistive porous medium are numerically interpreted under the magnetohydrodynamic environment. Fluid and dust phase characteristics are overlooked against the preeminent parameters. The main concern, in this work, is to analyze how much the resistive porous media affects the dusty flow in the presence of Lorentz force. The use of convection boundary conditions will aid attain the desired heat transfer rate in engineering applications. The nonlinear partial differential equations governing the fluid and dust phase are transmuted into a system of coupled and highly nonlinear ordinary differential equations which are first discretized using... 

Gold nanoparticles (Au NPs) were synthesized by co-deposition of RF-sputtering and RF-PECVD from acetylene gas and Au target on the carbon nanotubes (CNTs). The CNTs were prepared by thermal chemical vapor deposition (TCVD) and Pd nanoparticles catalyst. TEM image shows that high-density and uniform distribution of Au NPs were grown on the CNTs. XRD analysis indicates that Au NPs have fcc crystal structure and CNTs have a good graphite structure. Raman spectroscopy results suggest that our sample includes double-walled CNTs. It is resulted that intensity of D-band reduces and G-band intensity raises and radial breathing mode (RBM) is changed by immobilizing of Au NPs on the CNTs. Raman... 

In this paper, the impacts of Maxwell nanoliquid transmission, rectangular with titanium oxide nanoparticles are explored over the triangular, chamfer blades. The innovation of this paper is the use of the number of chamfers, rectangular, and triangular blades at the top and bottom of a stretched plate to study physical nanofluid parameters such as temperature and the effects of magnetism. Also, by determining the appropriate height and length for the blades, we achieve the best optimization of temperature and velocity of nanofluid between the plate and the blades, which improves heat transfer and with a more and better effect of magnetic effects. The finite element method is utilized for... 

In real-time packet-based communication systems, one major problem is misrouted or delayed packets which results in degraded perceived voice quality. If packets are not available on time, the packet is known as lost packet. The easiest task of a network terminal receiver is to replace silence for the duration of lost speech segments. In a high quality communication system, to avoid quality reduction due to packet loss, a suitable method and/or algorithm is needed to replace the missing segments of speech. In this paper, we introduce a low order recursive linear prediction method for replacement of lost speech segment. In this method a normalized least mean square (NLMS) as an adaptive filter... 

In this paper, we study theoretically the generation of high repetition rate short pulses using fiber optical parametric amplification. We show that the pulse shape and duration depend on the signal location relatively to the pump frequency. We demonstrate that in order to get the shortest pulse width, the signal must be located at one of the extremities of the gain spectrum associated with the pump peak power. We derive the analytical expression of the pulse shape in this case and compare it to the exponential gain regime case. Using numerical simulations, we also analyze the impact of walk-off and pump phase modulation that is required to suppress Stimulated Brillouin Scattering and derive... 

This paper reports a polarization controllable and angle-insensitive perfect metamaterial absorber (PMA). The proposed PMA consists of periodically arranged asymmetric omega-shaped resonators made of metallic copper. The absorptivity was analyzed considering the microwave C-band from 4 GHz to 8 GHz. The proposed PMA shows an absorption peak with almost 100% absorptivity at 6.2 GHz. Also, wideband negative index of refraction is observed. Further, the absorber is inspected for the different rotation angles of the top metasurface (omega-shaped ring) along the optical axis, and obliquity of incidence angle for both TE and TM polarized waves. Moreover, surface electric field and surface current... 

In cloud computing, services play key roles. Services are well defined and autonomous components. Nowadays, the demand of using Fuzzy inference as a service is increasing in the domain of complex and critical systems. In such systems, along with the development of the software, the cost of detecting and fixing software defects increases. Therefore, using formal methods, which provide clear, concise, and mathematical interpretation of the system, is crucial for the design of these Fuzzy systems. To obtain this goal, we introduce the Fuzzy Inference Cloud Service (FICS) and propose a novel discipline for formal modeling of the FICS. The FICS provides the service of Fuzzy inference to the... 

The mixed nano-ferrites materials Cu0.6Zn0.4HoxFe2−xO4 (0.00 ≤ x ≤ 0.12) were prepared via the sol–gel auto combustion technique. The TGA curve established the annealing temperature (500 °C) for phase formation. The single exothermic peak on the DSC plot occurred at 341 °C temperature. XRD patterns of these nano ferrites verified single phase formation of the FCC cubic structure. The lattice constant a was increased from 8.4244 to 8.4419 Å and then its value decreased to 8.4319 Å. Crystallite size was found in the range of 7 to 16 nm. The surface morphology of the samples was observed from the scanning electron microscope (SEM) images. The grain size was found within the range of 90 nm to... 

The mixed nano-ferrites materials Cu0.6Zn0.4HoxFe2−xO4 (0.00 ≤ x ≤ 0.12) were prepared via the sol–gel auto combustion technique. The TGA curve established the annealing temperature (500 °C) for phase formation. The single exothermic peak on the DSC plot occurred at 341 °C temperature. XRD patterns of these nano ferrites verified single phase formation of the FCC cubic structure. The lattice constant a was increased from 8.4244 to 8.4419 Å and then its value decreased to 8.4319 Å. Crystallite size was found in the range of 7 to 16 nm. The surface morphology of the samples was observed from the scanning electron microscope (SEM) images. The grain size was found within the range of 90 nm to... 

In the study presented herein, a simple method for laboratory calcite cementation of a reconstituted gravelly sand was presented. This method was used to prepare cemented gravelly sand specimens, which have similar natural characteristics to alluvial deposit of the city of Tehran. The formation and distribution of calcite bonds, as well as the effectiveness of the presented calcite cementation method in increasing interparticle cohesion, as observed in weakly to moderately cemented soil in Tehran, were evaluated by means of chemical analysis, X-ray diffraction technique, and unconfined compressive strength tests. The cementation technique was used to prepare triaxial specimens with calcite... 

Machine-to-Machine (M2M) communication is an important type of communication in the Internet-of-Things (IoT). How to send data in these high-density communications using relay selection can help improve the performance of this type of communication in various applications. In addition, the possibility of simultaneous use of different Radio Frequency (RF) interfaces helps to use the spectrum more efficiently. In this work, we try to further use machine communication RF equipment and improve the average data rate of networks in some applications such as the IoT, which have their own bandwidth requirements. Therefore, we provide an optimization algorithm for relay selection as well as the... 

The development of new technologies has confronted the entire domain of science and industry with issues of big data's scalability as well as its integration with the purpose of forecasting analytics in its life cycle. In predictive analytics, the forecast of near-future and recent past - or in other words, the now-casting - is the continuous study of real-time events and constantly updated where it considers eventuality. So, it is necessary to consider the highly data-driven technologies and to use new methods of analysis, like machine learning and visualization tools, with the ability of interaction and connection to different data resources with varieties of data regarding the type of big... 

Norouzak oil seeds that are the source of bio-diesel (Norouzak) fuel grow mostly in Gonabad and Kashmar located in Khorasan, north east of Iran. Spray characteristics of Norouzak bio-diesel have been experimentally and theoretically studied in this work. Norouzak fuel is added to the conventional diesel fuel, and mixture formations of several blends have been investigated and compared with each other. Moreover, by varying ambient and injection conditions, behaviors of spray of different blends have been explored. Microscopic and macroscopic properties of spray such as Sauter Mean Diameter (SMD), Ohnesorge number, spray tip penetration, spray cone angle, spray projected area and volume have... 

Norouzak oil seeds that are the source of bio-diesel (Norouzak) fuel grow mostly in Gonabad and Kashmar located in Khorasan, north east of Iran. Spray characteristics of Norouzak bio-diesel have been experimentally and theoretically studied in this work. Norouzak fuel is added to the conventional diesel fuel, and mixture formations of several blends have been investigated and compared with each other. Moreover, by varying ambient and injection conditions, behaviors of spray of different blends have been explored. Microscopic and macroscopic properties of spray such as Sauter Mean Diameter (SMD), Ohnesorge number, spray tip penetration, spray cone angle, spray projected area and volume have...