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      Development of Microextraction Methods
      for the Trace Determination of Organic Compounds in Biological and Environmental Media

      , Ph.D. Dissertation Sharif University of Technology Khalilian, Faezeh (Author) ; Bagheri, Habib (Supervisor)
      Abstract
      The approach of this thesis is to develop and simplify robust microextraction techniques and apply these developed methods to real samples and complex matrices. Firstly, a modified solvent microextraction with back extraction method (SME/BE) combined with high performance liquid chromatography and fluorescence detection (HPLC-FD) was developed for the determination of citalopram in human plasma. Extraction process was performed in a home-made total glass vial without using a teflon ring, usually employed in SME/BE. The evaluation results demonstrated that the calibration curve showed linearity in the range of 1.0–130.0 ng/mL which covers therapeutic window and even lower amounts which is... 
    Total 1 records