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The goal of this thesis is to understand the physical properties of lanthanum based manganites and barium based ruthenates. In order to obtain negative colossal magnetoresistance in manganites and fabrication of barium ruthenate in ordinary condition, the effects of variables such as ionic radii, chemical composition, temperature, magnetic field and processing in manganites and ruthenates systems are investigated. In the first part, the effects of potassium doping on structure, metalinsulator transition and magnetoresistance in )La1-yKy)0.7 Ca0.3 MnO3 and)La1-yKy)0.7 Ba0.3 MnO3 manganites systems are studied. Polycrystalline samples of manganites are synthesized by the sol‐gel method. In the...