Sharif Digital Repository

It is well known that the classical continuum theory does not consider size effect in predicting material’s behavior, however at the micro and nano scales, this effect is not negligible and the classical theory has deficiencies at these scales. To take into account the size effect, higher order continuum theories introduce new material constants into the formulation. One famous version of these theories is couple stress which is applied in this research. This theory considers size effect of inhomogeneity by employing Characteristic length of materials. Quasi-static couple stress and classical dynamic approaches do not include explicitly the size of the material unit cell in the formulation... 

In this study, the joint of co-sintered zirconia/stainless steel is investigated. To this end ZrO2-3mol%Y2O3 (TZP) and 430L stainless steel powders were utilized. The joining parameters of co-sintering in zirconia/metal were studied. In order to study the microstructure, diffusion and probable reactions at the joint boundary, HRSEM, HRTEM, EPMA and micro-focused XRD methods were employed. Shear strength of the joint was also measured. Finite element simulation of residual stresses and thermodynamic studies are utilized in the next step to analyze the experimental results. It is found that the direct joining of zirconia to 430L stainless steel is feasible by co-sintering at 1350 °C under low... 

IC221M is a cast Ni3AI-based intermetallic alloy which chemical composition bases on Ni- 8Al-8Cr-1.5Mo-1Zr-O.OIB %wt. Because of high strength, good high temperature oxidation, carburization and creep resistance as mechanical and physical properties, IC221M has got good attention in aeronautical, military and steel production industries nowadays. The best service temperature range is 600-800°C and melting starts at II 70°C. Since 1993 according to broad range of researches and applications, ASTM standardized it at Al002-99 and from that time researchers try to replace steel with IC221M. %80 volume of microstructure in this alloy consisted of brittle y' and remain are y and low... 

In this project, Dissimilar Friction Stir Welding (FSW) between aluminum alloys (1100-H12 and 5083-O) and Magnesium alloy (AZ31B-O) with 3mm thickness were butt joined. Fusion welding of aluminum/magnesium alloys has failed because of forming much more intermetallic compounds. By using friction stir welded samples, effect of welding parameters such as tool travel speed, tool rotation rate, tool position respect to weld centerline, and sheet position respect to tool direction on mechanical (tensile strength, yield strength and elongation) and microstructural properties of the welds were investigated. After several tests, range of optimum parameters were obtained. In both 1100 and 5083 alloys,... 

Metallic multilayer composites provide remarkable mechanical, electrical and magnetic properties. These kinds of composites have been recently processed by severe plastic deformation (SPD) methods. Accumulative roll bonding (ARB) is one of the SPD processes in which accumulation of strain by repeating cycles, leads to the ultra fine grained materials. The goal of this research is manufacturing of Al/Ni composite sheets by ARB process considering the effects of thickness and number of initial sheets on their mechanical properties and microstructures. The initial composites were produced by commercially pure Al and Ni as the matrix and the reinforcement, respectively. Thickness of the Al... 

Because of the importance and value of Superalloy, In this research has been treid to remelting scrap of gas turbine blades cobalt based Superalloy X-45, In order to restore it to the cycle of consumption. For this purpose, scraps were remelted under different conditions, for example changing the atmosphere, changing slag composition, changing type of the furnace for remelting and changing time of remelting process. Then in order to investigate effect of the above factors, microstructure were studied by optical microscope and Scanning Electron Microscopy (SEM) And also in order to investigate changings of element composition, chemical analysis were examined by atomic absorption analysis and... 

In this study, Al6063-Al203 nanocomposite powders were synthesized by reaction mechanical milling method. Nanometric reinforcement particles were formed via high- energy ball milling under a controlled oxygen containing atmosphere. Morphological and microstructural evolutions of nanocomposite powders were investigated by using X-ray diffraction (XRD), thermal analysis (DTA), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) methods at different milling times. The results showed that mechanical milling stages were accelerated and the time for reaching steady- state condition was decreased by an increase in the oxygen content in the milling atmosphere. The in-situ... 

Conventional defects in GTAW welding of Aluminum 5052 alloy are the decrease in weld zone strength because of grain growth, formation of columnar grains in the fusion line, solidification cracks and porosities. In this work, effect of strong field electromagnetic stirring on solidification structure of 5052 alloy and elimination of GTAW defects have been investigated. For arc welding processes (especially tungsten inert gas welding), a process called magnetic stirring was proposed, patented, and investigated in the 1970s. The essential aim was to improve weld quality and they indicated that the the Lurentz force is cause of weld stirring. In the earlier researches, alternating magnetic field... 

Various theoretical studies have been developed to obtain a deeper understanding of concrete behavior lead to the concrete constitutive models in the macroscale. In these models, however, the microstructure of the concrete and its effects on the concrete behavior has not been taken into account.Several numerical approaches have been incorporated to determine the effects of concrete mesostructure on the overall behavior of concrete. They may be classified at least in three main groups. In the first group, Continuum finite element methods (FEM) equipped with interface elements is incorporated. Second group is to incorporate more efficient elements, such as lattice or truss elements, instead of... 

In this research, Al-20Si-5Fe-1Mg-xMn(x= 0,3,6) ribbons were produced by Melt spinning method. Microstructure and growth morphology of ribbons were studied by optical microscope (OM), scanning electron microscope (SEM) and X-ray diffraction (XRD). The results were compared with as cast samples. In OM results, two different zones were observed. Featureless zone (with planar growth morphology) and dendrites zone. Microstructure of ribbons were completely different from the as cast samples. It consisted of just Aluminium and silicon. XRD results approved that matter. In fact, high solidification rate of ribbons increased the solubility of silicon and other alloys in aluminium and consequently... 

The aim of this research is to fabricate Mg based nanocomposite by friction stir processing and investigation of the process parameters on the microstructure and mechanical properties of the nanocomposite. In order to this aim, alumina nanoparticles as reinforcement were poured in the groove, with 5mm depth, and due to rotation of friction stir tool, these nanoparticles were mixed with the matrix and nanocomposite was produced. To reach to the best condition in nanocomposite fabrication, the effect of friction stir processing parameters such as, tool rotation speed, tool design, number of friction stir passes, cooling media and reinforcement percent on microstructure, hardness, tensile... 

The introduction of multi phase steels in recent years resulted in a considerable increase in development of some industries such as automobiles. By inducing soft and hard phases together, these steels could bring better mechanical properties than classical ones. Recent studies on 4340 ferritic- bainitic and ferritic- martensitic dual phase steels, indicate that 34 volume percent ferrite with hard phase, has the best combination of strength, toughness and fatigue properties. In present research, by proper heat treatment on a 4340 steel, it is tried to prepare specimens ferritic- bainitic- martensitic triple phase steels with 34 volume percent of ferrite and different percents of martensite.... 

Gray Cast Irons are the most important engineering Cast Irons. Gray color of fracture surface and morphology of graphite flakes are the reasons of this naming. Gray iron is relatively cheap with easy production; because of wide chemical composition range rather other cast irons. Furthermore, shrinkage and feeding in the casts from gray iron, besides surface finishing by machining are easy. The other properties of gray iron are resistance against sliding wear, high thermal conduction coefficient, low module of elasticity and thermally shock resistance. In this research, the effects of added nitrogen as an alloying element and cooling rate on microstructure, hardness and tensile properties of... 

The present work investigates joining of two MoSi2 parts through Cusil/Zr/Cusil interlayer with Cusil being a commercial eutectic of Ag-Cu alloy. The joining operation was implemented in an inert gas tube furnace by brazing. The brazing temperature ranged at 800-930°C while the operation lasted for 1hr. Interfacial microstructure was studied by Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS) and X-Ray Diffraction (XRD) techniques. Applying the temperature of 830°C was led to uniform dense joint consisting of various reaction phases with excellent bonding within interfaces. Diffusion of Si to the liquid phase will transform MoSi2 to Mo5Si3 which bears Ag to some... 

Al-20Si-5Fe-3Cu-1Mg–xCr (X=0, X=1.5) ribbons were produced by melt-spinning technique at the rotating speed of 20 and 40 ms-1. The thickness of ribbons were 40 to 80 and 15 to 35 μm, respectively. The properties of as-melt spun and as-cast specimen were investigated by optical microscopy (OM), scanning electron microscopy (SEM), X-Ray diffractometry (XRD) and the microhardness method. It was found that at the air side of ribbons the microstructure was dendritic while at the wheel side it was featureless. The microstructure of ribbons at two rotating speed showed a homogenous distribution of Si particles embedded in an α-Al matrix. XRD investigations exhibited the absence of any intermetallic... 

Equal Channel angular pressing (ECAP) is one of the most applicable Severe Plastic Deformation (SPD) Procedures which results in improvement of strength and ductility through grain refinement and an appropriate texture development. In this study, in order to achieve a proper orientation and microstructure, ECAP was performed in different routes and temperatures up to 4 passes on AZ31 magnesium alloy. Microstructure and mechanical properties were studied. X-ray diffraction analysis was performed to study the basal orientation variation and calculation of sub-grain size. In addition, cold rolling at room temperature was done on the fourth pass specimens, in order to study the effect of ECAP... 

In this research, transient liquid phase (TLP) bonding of FSX-414 superalloy was investigated using MBF-80 interlayer. The bonding was performed at different temperatures (1050-1200oC) for various times (1-120min). Also, different gap sizes were studied using the interlayer with various thicknesses (25-100µm). Homogenizing treatment was performed at different temperatures (1175-1225oC) and times (1-6h) for the samples with complete isothermal solidification. The microstructure of the samples were studied using the optical, scanning electron and transmission electron microscopes. Also, XRD, SEM/EDS, SEM/WDS and TEM/EDS analyses were used to analyse the observed phases at the joints. To... 

Several studies are already on severe plastic deformation of wrought and cast aluminum alloys. Among these studies, no evidence of applying severe plastic deformation on the structure of rheocast or rheoforgedaluminum alloy can be found. So, in this research A356 alloy with globular structure was achieved using electromagnetic stirring and rheoforging. The optimum condition of globular structure with high sphericity was achievedafter holding the produced structure in semi-solid state for 10 min. Then, the effect of severe plastic deformation on mechanical and microstructural properties of this alloy and cast alloy was studied. The results show that with applying 3 passes of multidirectional... 

One of the limitations of friction stir welding process is joining of sheets with low thickness. Interference ways for these limitations are joint in higher thicknesses and thickness reduction in included joint samples. In this study, in the first process, with the optimization of the variables affecting the process, joint was performed using visual inspection, mechanical properties and micro structural studies. In the next process, using the rolling operation for the reduction percent of different thicknesses, the most appropriate route was chosen. 1050 aluminum sheets (1050 and 6082-T6) with a thickness of 3 mm were welded using friction stir welding in tool rotary speeds of 1200 and 800... 

An increase in strength of friction stir welded (FSW) AA3003-H18 sheets is important, due to the reduction of mechanical properties in weld area such as heat affected zone and stir zone during welding. In this research, at first FSW was used to join 3003-H18 non-heat-treatable aluminum plates without adding copper powder. The specimens were joined at various rotational speeds (800, 1000 and 1200 rpm) and traverse speeds (40, 70 and 100 mm/min). In these cases, the effects of welding parameters on microstructure and mechanical properties were investigated. The average grain size of stir zone was in the range of 21.7-7.8 μm and the microhardness of them was 28-37 Hv. Then FSW was used to join...