Sharif Digital Repository

An ultrafine-grained Al6063/Al2O3 (0.8 vol.%, 25 nm) nanocomposite was prepared via powder metallurgy route through reactive mechanical alloying and hot powder extrusion. Scanning electron microcopy, transmission electron microscopy, and back scattered electron diffraction analysis showed that the grain structure of the nanocomposite is trimodal and composed of nano-size grains (< 0.1 μm), ultrafine grains (0.1–1 μm), and micron-size grains (> 1 μm) with random orientations. Evaluation of the mechanical properties of the nanocomposite based on the strengthening-mechanism models revealed that the yield strength of the ultrafine-grained nanocomposite is mainly controlled by the high-angle... 

Ultrafine-grained (UFG) Al6063/Al2O3 (0.8 vol%, 25 nm) nanocomposite was prepared via powdr metallurgy route. The grain structure of the nanocomposite composed of nano-size grains (< 0.1 μm), ultrafine grains (0.1-1 μm) and micron-size grains (>1 μm) with random orientations. It was found that the yield strength of the UFG nanocomposite is mainly controlled by the Orowan mechanism rather than the grain boundaries. The deformation activation energy at temperature ranges of T <300 ˚C and 300 ˚C ≤T < 450 ˚C was determined to be 74 and 264 kJ mol-1, respectively. At the higher temperatures, significant deformation softening was observed due to dynamic recrystallization of non-equilibrium grain... 

Al6063 powder was subjected to severe plastic deformation via high-energy mechanical milling to prepare ultrafine-grained (UFG) aluminium alloy. Uniaxial compression test at various temperatures between 300 and 450 °C and strain rates between 0.01 and 1 s-1 was carried out to evaluate hot workability of the material. Microstructural studies were performed by EBSD and TEM. The average activation energy and strain rate sensitivity of the hot deformation process were determined to be 280 kJ mol-1 and 0.05, respectively. The deformation temperature and applied strain rate significantly affected the grain structure of UFG Al alloy. A finer grain structure was obtained at lower temperatures and... 

An ultrafine-grained Al6063/Al2 O3 (0.8vol.%, 25nm) nanocomposite was prepared via powder metallurgy route through reactive mechanical alloying and hot powder extrusion. Scanning electron microcopy, transmission electron microscopy, and back scattered electron diffraction analysis showed that the grain structure of the nanocomposite is trimodal and composed of nano-size grains (<0.1μm), ultrafine grains (0.1-1μm), and micron-size grains (>1μm) with random orientations. Evaluation of the mechanical properties of the nanocomposite based on the strengthening-mechanism models revealed that the yield strength of the ultrafine-grained nanocomposite is mainly controlled by the high-angle grain... 

The hot deformation behavior of A-286 superalloy has been characterized using hot compression experiments in the temperatures between 1000 and 1100 °C and strain rates varying between 0.001 and 0.1 s-1. In addition, hot workability of this alloy has been analyzed by employing flow-localization parameter. The results show that both kinds of softening mechanism, dynamic recovery and dynamic recrystallization, occur during hot working, where at 1000 °C the main mechanism is dynamic recovery and at higher temperatures and strain rate of 0.001-0.01 s-1 dynamic recrystallization takes place. Calculations demonstrates that this alloy mainly have a good workability for the utilized deformation... 

The hot working behavior of A286 was studied using hot compression tests over temperature range of 950-1100 °C and at strain rates of 0.001-1 s -1. The flow curves of the material over the studied temperatures and strain rates were typical of dynamic recrystallization. However, some points reflected a change in the mechanism of softening with the change of strain rate. The relation between flow stress, deformation temperature and strain rate was examined via power-law, hyperbolic sine and exponential constitutive equations and the hyperbolic sine function was found more appropriate. The peak strain increased with strain rate up to 0.01 s-1 and then unexpectedly decreased at higher strain... 

The hot deformation characteristics of 7075 aluminum alloy (AA7075) are investigated by means of hot compression tests carried out in the temperature range of 200-450 C and strain rate range of 0.0003-1 s-1. Two novel processing maps based on flow localization parameter and enhanced DMM are developed and compared with conventional DMM results. It is observed that processing maps based on flow localization parameter can be used successfully to predict AA7075 thermomechanical behavior. Also, the comparison of the DMM results indicates that the new approach to calculate DMM power dissipation efficiency and instability criteria corresponds better with experimental observations. The occurrence of... 

In the present work, hot workability of particulate-reinforced Al6061-20%SiC composite produced by direct hot extrusion technique was studied. Uniaxial hot compression test at various temperatures and strain rates was used and the workability behavior was evaluated from the flow curves and the attendant microstructures. It was shown that the presence of SiC particles in the soft Al6061 matrix deteriorates the hot workability. Bulging of the specimens and flow lines were observed, which indicates the plastic instability during hot working. Microstructure of the composites after hot deformation was found to be heterogeneous, i.e. the reinforcement clusters were observed at the flow lines. The... 

Hot compression tests were carried out on a Fe-29Ni-17Co alloy in the temperature range of 900 °C to 1200 °C and at strain rates of 0.001-1 s-1. Dynamic recrystallization was found responsible for flow softening during hot compression. The flow behavior was successfully analyzed by the hyperbolic sine equation and the corresponding material constants A, n and α were determined. The value of apparent activation energy was determined as 423 kJ/mol. The peak and steady state strains showed simple power-law dependence on the Zener-Hollomon parameter. The dynamic recrystallization kinetics was analyzed using Avrami equation and the corresponding exponent was determined to be about 2.7. This... 

Ultrafine-grained (UFG) Al6063 matrix nanocomposites reinforced with nano-size Al2O3 were produced by reactive mechanical alloying and hot powder extrusion method. Microstructural studies were performed by transmission electron microscope (TEM) and electron backscatter diffraction (EBSD). Observation of very small regions with high- and low-angle grain misorientation, i.e. grains and subgrains, showed the formation of UFG Al alloy matrix with an average grain size of ~ 0.37 μm. A uniform distribution of alumina particles with an average size of ~ 100 nm was also achieved. Compression test at various temperatures up to 450 °C was carried out to evaluate the high-temperature strength and hot... 

Hot isotherm compression tests were performed in temperature range of 350-500 °C and at strain rates of 0.0005 to 0.5 s-1 for Al6061 alloy reinforced with alumina nanoparticles. Effect of deformation parameters and optimal conditions for hot working this nanocomposite were comprehended thoroughly via hot working data analyses, electron microscopy images, and X-ray diffractograms. The results indicated the severity of hot deformation process and an increase in the activation energy to 320 kJ/mol due to the addition of nanoparticles. Dynamic recovery (DRV) was considered as the individual determinative softening mechanism during hot deformation of this nanocomposite, and no sign of dynamic... 

The texture, microstructure, and mechanical properties of severely deformed aluminum subjected to friction stir processing (FSP) with SiC nanoparticles under ambient and cryogenic temperatures are comprehensively investigated. Even one pass of FSP in the ambient temperature results in the formation of quite large grain structure with random texture in the heat affected zone (HAZ). It suggests the occurrence of static recrystallization and subsequent grain growth because of the appreciable strain stored within the base metal. One FSP pass under condition of cryogenic temperature causes to the development of bimodal grain size distribution in HAZ, including the elongated grains with interior...