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Bromine-lithium Exchange Reaction in Organic Synthesis Using Glass Microreactor
, M.Sc. Thesis Sharif University of Technology ; Mohammadi, Aliasghar (Supervisor)
Abstract
Today, microreactors come into focus due to their exclusive characteristics including high surface-to-volume, lower consumption of reagents and fast mixing. In this study, optimization of the Br-Li exchange reaction as a consecutive reaction using glass microreactor is investigated. To construct glass microreactor, laser ablation and thermal bonding method are utilized. In order to find the best yield and selectivity of the reaction, various parameters, such as solvent, equivalent ration of the two reagents, concentration of the reagents, residence time and flow rates of the reagents are examined. In addition, atomic force microscopy (AFM) analysis was used to determine the surface...
Bromo-lithium Exchange Reaction in Organic Synthesis and Continuous Separation of Organic and Aqueous phase Reactions by Microfloid Technique
, M.Sc. Thesis Sharif University of Technology ; Mohammadi, Ali Asghar (Supervisor) ; Bastani, Dariush (Supervisor)
Abstract
Today, with the development of micro-technology in chemical reactions, the use of appropriate systems for the separation and purification of synthesized chemicals seems to be necessary. In this study, the continuous synthesis of bromide-lithium exchange reaction and the separation of organic and aqueous phase products in micro systems was investigated.The method used to construct micro-separator and micro reactor, a laser engraving technique, and thermal bonding of glass to glass.In the first step, the factors affecting the separation of organic and aqueous phase in the capillary micro-separator, such as the width of the capillary, the length of the capillary, the number of capillaries and...
Synthesis of Silica Nanosheets Using Droplet-based Microfluidics
, M.Sc. Thesis Sharif University of Technology ; Mohammadi, Aliasghar (Supervisor)
Abstract
The main purpose of this project is synthesis of the silica nano-sheets by means of microfluidic techniques. Continuous process, precise control of reaction condition, and higher production rate can be considered as main pros of silica nano-sheets synthesized by microfluidic platforms. General method can be explain as follow: first two oleic and aqueous phase are injected to the microfluidic system, then oleic phase breaks down in aqueous phase drop-wisely and by performing sol-gel reaction on the oil-water interface a silica crust is made on oil droplets. Eventually, oil droplets are left the system and broken down and silica nano-sheets are made. FESEM and microscopic images of...