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Novel and efficient method for the silylation of hydroxyl groups with hexamethyldisilazane (hmds) under solvent-free and neutral conditions
Azizi, N ; Sharif University of Technology | 2004
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- Type of Document: Article
- DOI: 10.1021/om0341505
- Publisher: 2004
- Abstract:
- Various alcohols and phenols were silylated to trimethylsilyl ethers with hexamethyldisilazane in the presence of solid lithium perchlorate under very mild, neutral, and solvent-free conditions in good to excellent yields
- Keywords:
- Ammonia ; Stoichiometry ; Solvents ; Phenols ; Lithium compounds ; Hydroxylation ; Ethers ; Catalysts
- Source: Organometallics ; Volume 23, Issue 6 , 2004 , Pages 1457-1458 ; 02767333 (ISSN)
- URL: https://pubs.acs.org/doi/10.1021/om0341505