Sharif Digital Repository

In this study, standard composite laminate specimens with micro and nano sized particle additives are made to study the effect of the additives on the fracture toughness of the specimens in standard tests. The composite laminates are made from epoxy resin and unidirectional glass fibers. The mode I and mode II fracture toughness of the specimens are measured under various loadings in standard tests. The fracture surface is then, fractogaphed by microscopic instruments. In conclusion, the fracture behavior of laminated composites, toughened by micro and nano particles is discussed. The results show that using rubber particles will improve fracture toughness of neat epoxy resin and laminated... 

Commercially pure titanium (CP-Ti) is an important groups of titanium family and because of high strength, low density, high corrosion resistance and biocompatibility, this group of titanium is a suitable choice for application at chemical, petrochemical and medicine industry. Nowadays surgeons have a tendency toward use of CP-Ti instead of Ti-6Al-4V alloy. Moreover, because of body anatomy limitation, use of thick sheets result in high volume and damage soft tissue. Therefore, for sheet thickness reduction, study of the effects of metallurgical and geometrical parameter on fracture behavior of thin sheets is important. In this study, the fracture behavior of CP-Ti thin sheets investigated.... 

Epoxy resins are relatively brittle and have low resistance to crack propagation. It is common to add rubber particles to improve crack resistance in epoxies, although these particles may deteriorate the strength of the matrix. Different nanomaterials are used to overcome the inherent brittleness of epoxies and to keep the mechanical properties. Among them, carbon nanotubes has been attracted many attentions. Fractue behavior and mechanical properties of two kind of novel nanocomposites, i.e, epoxy/carbon nanotube and epoxy/rubber/carbon nanotube are investigated in current study. Electron microscopy investigations were done to assure the CNTs distribution and fracture mechanisms as well.... 

In this research, a powder containing magnesium-aluminate spinel particles is prepared based on co-precipitation method and 5% , 10%, 15% and 20% zirconia-contained composites are produced as second phase from the synthesized powder. The raw materials used in the synthesis comprise hexa-hydrated magnesium nitrate, nona-hydrated aluminum nitrate, ammonium bicarbonate, 28% ammonium solution and distilled water. The properties of the powder is then investigated using STA, XRD and SEM tests. Also, XRD and SEM analyses as well as triple point flexural strength and Vickers hardness tests are carried out in order to investigate the effect of adding zirconia to the powders. The variations of the... 

The purpose of this thesis is the construction of hard and tough Zirconia bodies from economical raw materials using minimum sintering time and temperature.
Stabilizers cause tetragonal particles to be remained in cubic phase. Most additives are Ca, Ce, Mg and Y ions the whole of which are rare earth elements and make solid solutions with Zirconia.
In this project different percents of CaO, MgO, CeO2, and Y2O3 were mixed with ZrO2 and they were sintered after granulation, cold pressing and Cold Isostatic Pressing. Using jar milling and fast milling, the particle size of purchased ZrO2 was reduced to 0.7 um. The whole needed additives were purchased with particle size below 300 nm.... 

Hydraulic fracturing process as one of the most important ways to inhanse of production requires careful study and investigation and due to its importance has been studied for decades. The effect of this process on the production at oil and gas industry has many complexities and these complexities with the complex structure of natural gaps, would be multiplied. In this thesis effect of hydraulic fracturing operation on the production of natural fractures at naturaly fractured reservoirs from two aspects of hydraulic and geomechanics will be investigated. First we provide models for fractures network by using UDEC software after that investigate the effect of hydraulic farcture on the natural... 

Repair welding is one of the important maintenance processes that include build-up welding and surfacing.In this study, investigation of repair welding parameters has been conducted to achieve desired microstructure with the appropriate toughness and minimum residual stress.In this research, local post-weld heat treatment has been performed by Tungsten electrode arc on weld zone. Performing this process with optimum parameters leads to the best heat cycle with the tempered Martensite microstructure. Residual stress of the sample will be reduced. HAZ coarse grains will be refined to finer grains which result in to improved toughness and reduced hardness to the acceptable limit.
Results... 

Nowadays, we know that many hydrocarbon reservoirs are fractured regarding this, the investigation of the properties of these reservoirs is necessary to predict the storage, production and the drilling methods. To identify fractured reservoirs, the fracture properties and their geometries under different conditions should be investigated. Besides, the evaluation of the behavior of induced fractures in distinct under ground conditions is very important. The Mechanical properties of the drilling bed like crack propagation, layer and mass rock is impactful in planning of drilling process and hydraulic fracturing operation. In this research, at first we introduce natural and induced fractures... 

Fracture Toughness of Geopolymer Concrete Containing Blast Furnace Slag in Corrosive Environments  

Microstructure and mechanical properties developments of X80 weld metal by addition of different amounts of alloying elements such as: Nickel and Manganese in coated electrodes were investigated. For this reason samples were welded by electrodes that Ni value has been changed between 0.8%- 3.2% in tow critical amounts of Mn: 0.7 and 1.6. The weld quality was evaluated using nondestructive testing methods (NDT), such as visual inspection and radiography. Tensile test, Charpy impact test and microhardness results indicated the suitable range of Ni and Mn for achieving acceptable mechanical properties. In addition, optical microscopy and scanning electron microscopy (SEM) were applied to link... 

Polymer blending has an important role in preparation of materials with suitable properties without synthesizing new polymers. One of these blends is polypropylene (PP)/ polyethylene (PE). PE is added for improving the impact strength and toughness of PP. For improvementof the properties, a compatibilizer is used due to incompatibility of the PP/PE blend. Improving the impact properties is usually related to the reduction in stiffness. Considering the importance of stiffness in many industrial applications, mineral fillers are employed for increasing the stiffness. In this research, the goal has been to manufacture polypropylene-based ternary composite(Polypropylene/ Polyethylene/Nanometric... 

Nowadays, composites have wide applications in different industries especially in aerospace industry because of their high strength to weight ratio. Epoxy 5052 for its relatively good mechanical properties and high thermal resistance has vaidly use for manufacturing of large composite components. However; fracture toghness of epoxy resins is not good in comparison to their other exceptional properties. Therefore, researchers have endeavored to improve this characteristic with different approaches. One of these methods is nanotechnology. Since the components in aerospace industry are often under impact loads and impact strength of these materials has been less studied, effect of carbon... 

Alumina as an engineering ceramic has special characteristics such as hardness, high abrasive, fatigue and corrosion resistance but suffers from low toughness. One effective method in improving toughness is adding second phases such as tetragonal zirconia and carbon nanotubes.
In this research, alumina- zirconia nanopowders has been prepared by solution combustion method and carbon nanotubes was added to it by two different ways: 1) in situ synthesis of CNTs by CVD 2) dispersion of CNTs by heterocoagulation method. In the case of in situ synthesis of CNTs in AZ matrix, the synthesis temperature and flow ratio of N2/C2H2 gases was investigated and optimum conditions were 800̊C and 300/30,... 

Polyamide6 has many engineering applications due to its physical, mechanical and processability properties. However, its low impact resistance limits the use of polyamide6. One of the common ways to overcome this problem and extend the range of polyamide6 application is its elasticity with elastomeric materials, which reduces the strength and modulus (tensile and flexure) in comparision with neat polyamide6. To overcome this limitation, various reinforcements, often fiber or particle-shaped, are used. Today, with the development of nanoparticles, this effort is being made to use nanoparticles, especially carbon nanoparticles with unique properties. Recent research has shown that the addition... 

In this study in-situ Al/Al3Ti was fabricated by mechanical alloying, hot extrusion and subsequent heat treatment. First, initial pure powders of Al and Ti were mechanically alloyed with 5 weight percentages of Ti for 40 hours. The as-hot extruded samples containing 5 wt% of initial Ti particles, were exposed to heating at 600 oC for various time intervals up to 10 hours. Microstructure analysis by OM and SEM proved that in-situ Al3Ti phase was formed as a layer around Ti particles by solid reactive diffusion between Al and Ti particles. After 10 hours of heating, all the Ti particles were consumed and transformed to Al3Ti. Mechanical properties of samples were investigated by Brinell... 

Fe-Cr-C hardfacing alloy is the most popular alloy used in severe abrasive condition such as mining and cement industries. One of the limitation of these hardfacing alloys is their low toghness, which reduce the application of these alloys under impact wear conditions. The purpose of this thesis is to investigate the effect of microstructure on the wear and toughness properties of AISI420 hardfaced martensitic stainless steel alloy. For this purpose, after deposition of the hardfaced alloy on a steel substrate, various heat treatments such as quench, quench temper, quench and partitioning and austenite reversion are designed to change the microstructure of the hardfaced alloy from fully... 

Discontinuously reinforced aluminum matrix composites (DRA) are candidates as a substantial class of materials for improved strength, stiffness, and wear resistance. However, the low fracture resistance of DRA's has restricted the widespread use of these materials as structural components. Consequently, intrinsic and extrinsic mechanisms have been considered in order to enhance the damage tolerance of composite materials based on microstructural and architectural modification, respectively. The intrinsic toughening technique has shown to elevate fracture resistance to some extent; usually at the expense of reducing several other properties such as strength. The more recent approach to... 

Particulate ceramic reinforced aluminum matrix composites have high specific strength and stiffness; however, low fracture toughness and deformability have restricted their industrial applications. Among the methods introduced to overcome this shortcoming is fabricating the layered composites which contain alternative layers of aluminum (Al) and discontinuously reinforced aluminum (DRA). In this study, two different routes; i.e., "Powder extrusion - Casting - Rolling" and "Powder extrusion - Roll bonding" were employed to produce layered Al-DRA composites. After production of Al6061/SiCp composites via hot powder extrusion, mentioned processes were utilized to make DRA-Al-DRA laminate. In... 

Epoxy resins are used for a wide number of application due to good stiffness, chemical resistant and dimensional stability. This is the reason of their use as matrix in composite material. The incorporation of a small amount of carbon nanotubes (CNTs) in epoxy increases mechanical properties if nanocomposite have strong interfacial interaction between epoxy and CNTs, fine dispersion of CNTs and high final aspect ratio CNTs. In Noncovalent functionalization by polymer surfactant, CNTs are dispersed in a solvent/surfactant solution by ultra-sonication and then added to epoxy. In this thesis a novel study of toughening and mechanical properties of epoxy/ rubber/ CNT nanocomposite is presented.... 

The most failures caused by wear, fatigue and corrosion are very sensitive to surface of material. Since the most failures starts or occurs at the surface of material, so control and improvement of the surface properties can have a significant effect on increasing the service life and improve the overall behavior of the material. Reforming of the structure and grain size is one of the methods to improve elastic properties, hardness, softness, toughness, etc. Also the macroscopic residual stresses in fracture toughness test specimens, can have tremendous effect on fracture toughness measurements. Many methods are used to modify the surface structure and to create a compressive residual stress...