Sharif Digital Repository

Microstructural development and phase formation at the interface of yttria stabilized zirconia (3Y-TZP)/430L stainless steel composite layers produced by co-sintering method were studied by SEM, HRTEM, micro-focus XRD, and EPMA. Formation of a rich chromium boundary layer at the interface was noticed, which revealed Cr aggregation at the interface at the elevated temperatures. Misfit dislocations were also observed at the joint interface to tackle the mismatch crystallographic orientations between the ceramic and metal layer. The results of the micro-focus XRD showed formation of no new phases at the boundary zone. Microstructural studies also revealed a retarded grain growth in the... 

Aluminum metal matrix composites (MMCs) reinforced with nanoceramics are ideal materials for the manufacture of lightweight automotive and other commercial parts. Adaptive neuro-fuzzy inference system combined with particle swarm optimization method is implemented in this research study in order to optimize the parameters in processing of aluminum MMCs. In order to solve the problems associated with poor wettability, agglomeration and gravity segregation of nanoparticles in the melt, a mixture of alumina and aluminum particles was used as the reinforcement instead of raw nanoalumina. Microstructural characterization shows dendritic microstructure for the sand cast and non-dendritic... 

The effect of temperature, pressure and bonding time on microstructure of temperature gradient transient liquid phase (TGTLP) diffusion bonded Al7075 alloy using liquid gallium interlayer was investigated. The selected bonding method relies on using the minimum amount of liquid gallium on faying surfaces, using a very fast heating rate to reach the joining temperature and imposing a temperature gradient across the bond region. The microstructure of the diffusion bonded joints was evaluated by light optical microscopy, scanning electron microscopy and energy dispersive spectroscopy (EDS). Results show that by increasing the temperature, pressure and time of joining, a more uniform... 

In this article, the effects of hot rolling parameters on static recrystallization, mechanical properties, and final microstructures of a low carbon steel have been investigated. A numerical analysis was first employed to determine distributions of temperature, strain, and strain rate during hot rolling and then the predicted results were combined with the additivity rule together with Avrami equation to evaluate the progress of non-isothermal static recrystallization after hot rolling. In the next stage, hot rolling experiments have been performed under different rolling conditions to assess the effects of rolling layout on microstructures and mechanical properties of the rolled steel. The... 

Microstructure developments of X80 weld metal by the addition of different amounts of alloying elements such as nickel and manganese to the covering of electrodes were investigated. For this reason, samples were welded with electrodes that Ni value has changed between 0.8 and 3.5% in two critical amounts of Mn 0.7 and 1.6. Optical microscopy and scanning electron microscopy were applied for peer investigation of microstructure. Different phase percentages were obtained by Clemex software and compared in all samples. Results indicated that Ni and Mn change weld microstructure in the as-deposited zone and reheated part and corresponding to each alloying element concentration, amount of... 

The wide-gap aluminothermic rail welds with root opening of 50-70 mm were produced using plain carbon steel rail and non-alloy aluminothermic charge. Mechanical properties and micro-structure of the weld metal and HAZ as well as the impact energy and the fracture toughness of the welds were investigated. The yield and tensile strength of wide-gap welds were about 98% and 95% of the base metal, respectively. Both minimum and maximum hardnesses of the joint were seen in HAZ which were related to the grain coarsening and normalizing, respectively. The mean value of wide-gap weld fracture toughness is more than narrow-gap weld. Moreover, trans-granular cleavage indicated the brittle fracture... 

Ultra-rapid annealing (URA) of deformed low-carbon steel can provide refined microstructure. In this research, severely deformed low-carbon steel is ultra-rapidly annealed to subcritical and intercritical temperature ranges at the heating rates of 75-1800°C/s and then rapidly cooled. Also, conventional annealing by the heating rate of 0.3°C/s is performed at the same temperature ranges. The results show that conventional and subcritical ultra-rapid annealing cannot lead to a fully refined microstructure. High heating rate causes the interaction between recrystallization and transformation as the temperature exceed Ac1 (intercritical temperature range). High kinetics of transformation during... 

In this research, production of ferrite - martensite dual phase Steels with different martensite morphology was considered during transient liquid phase bonding of a low carbon steel. The steel was bonded using an iron base interlayer with melting point of 1443 K and 40 μm thickness. Bonding process carried out at 1473 K, under pressure of 0.5 MPa, at different holding time of 10, 20, 30 and 40 minutes. Microstructural studies of joint region showed that isothermal solidification completed at the bonding time of 40 minutes. Microstructure of joints made at the bonding time of 10, 20, and 30 minutes consists of two distinct region, athermal and isothermal solidified zones. Microstructure of... 

It is commonly known that the properties of materials are strongly related to their microstructure. This paper introduces a method that is a combination of rapid solidification (melt spinning) and semisolid forming (thixoforming) processes, which are used to refine the microstructure of “as-cast” Al–30Si–5Fe alloy and improve its mechanical properties. Produced Al–30Si–5Fe ribbons by melt-spinning process, were pulverized and subsequently consolidated at 300 °C in argon atmosphere. Prepared specimens were thixoformed at temperatures ranging from 580 to 700 °C in various holding times. Some samples were also directly thixoformed from as-cast condition. Microstructure of the as-cast, meltspun,... 

The effect of equal channel angular pressing (ECAP) at different temperatures (room temperature, 120, 150 and 180 °C) on microstructure and mechanical properties of Al-7075 solid solution alloy was investigated. Microstructure of the specimens was examined using orientation imaging microscopy, transmission electron microscopy as well as X-ray diffractometer, and mechanical properties were measured by Vickers microhardness and tensile tests. Microstructural investigations showed that after 3 or 4 passes of ECAP, fine grains with average grain sizes in range of 300-1000 nm could be obtained at different ECAP temperatures. Increasing ECAP temperature from 120 to 180 °C caused a decrease in... 

In this study, multi-pass friction stir processing using zirconia nanoparticles was performed on AA5083 sheets to fabricate surface nanocomposites. Effect of using different number of passes on the microstructure, microhardness, tensile and wear properties of the specimens was investigated. Therefore, it was found that iteration of FSP consistently improves tensile properties and microhardness of the materials. This was mainly related to microstructural modification through FSP, including better dispersion of powders, finer grain size and minimum clustered particles. EBSD and TEM analysis indicated a large number of high angle grain boundaries and occurrence of continuous dynamic... 

A low-carbon steel sheet containing 0.05 C, 0.203 Mn, and 0.0229 Si (all in wt%) was rapidly annealed in a temperature range of 300 °C to 600 °C after severe plastic deformation by using constrained groove pressing (CGP) technique. Microstructure evolution was investigated by scanning electron and optical microscopes. Mechanical properties were evaluated by hardness measurements and shear punch test. The results showed a thermal stability up to 400 °C where recrystallization did not occur in the specimens even after 7200 s. This thermal stability is in agreement with previously reported results of conventional annealing of the same steel after CGP. However, annealing at 500 °C and 600 °C led... 

Protrusion friction spot stir welding (PFSSW) was introduced as a novel method to produce keyhole-free welds of a drawing quality special killed low carbon steel (DQSK). The effects of welding parameters such as tool rotation speed and plunging depth were investigated on the mechanical properties and metallurgical aspects. The sheet/sheet joint interface of the welds produced by PFSSW was visible and non-planar compared to the conventional FSSW method. Microstructure and hardness were affected by dynamic recrystallization and transformation hardening in the stir zone. Hardness value of the stir zone produced by the present work was much lower than that produced by resistance spot welding... 

Surface coverage as one of the most effective parameters of shot peening process has substantial influence on the functionality of the peened component. The aim of this study is to investigate the effects of surface coverage increase on the properties of treated specimens experimentally before and after re-shot peening. Different shot peening treatments from conventional to severe; were performed on the AISI 1045 steel. Microstructural observations and XRD measurements were applied to characterize the circumstance of microstructure changes. In order to investigate the mechanical properties, microhardness profiles were achieved, surface roughness was evaluated and the residual stresses... 

In this work, the effect of hot deformation temperature on microstructure and mechanical properties of micro alloyed steel was studied. The results indicated that by decreasing the deformation temperature final microstructure is refined and the volume fraction of grain boundary ferrite is increased and some pearlite is produced. Therefore both the yield strength and ultimate tensile strength is increased, while the toughness is preserved in comparison to a ferritic-pearlitic microstructure. Also a model was developed to relate the deformation condition to the volume fraction of acicular ferrite at mixed microstructure. © 2008 Elsevier Ltd. All rights reserved  

In this paper, the advantages of numerical simulation to improve the process of copper electroforming are demonstrated. In this regard, the finite element model of copper electroforming for a rotating cone electrode was first prepared and then, the effect of the key parameters, such as applied current density, solution conductivity, electrode spacing, and anode height, on the uniformity of the thickness was investigated. The model combines tertiary current distribution with Bulter–Volmer electrode kinetics and computational fluid dynamics at the turbulent condition. In order to validate the model, a cone-shaped shell was produced by electroforming method in the laboratory. The obtained... 

Abstract: Nowadays, friction stir spot welding (FSSW) is used in automotive, rail vehicle construction, the aerospace industry, and electrical industry. In the current research, a modified version of the FSSW process entitled friction stir spot vibration welding was introduced to join Al5083 specimens. The joining specimens were vibrated normal to the tool movement direction, while the joint position cooled by passing coolant through the fixture. Different characteristics of developed joint namely microstructure, mechanical properties, corrosion behavior were studied. The results showed that stir zone grain size decreased significantly as the vibration was employed and the joint position was... 

We consider the homogenization of a Robin boundary value problem in a locally periodic perforated domain which is also time-dependent. We aim at justifying the homogenization limit, that we derive through asymptotic expansion technique. More exactly, we obtain the so-called corrector homogenization estimate that specifies the convergence rate. The major challenge is that the media is not cylindrical and changes over time. We also show the existence and uniqueness of solutions of the microscopic problem. © 2020 American Institute of Mathematical Sciences. All rights reserved