Sharif Digital Repository

An iron based powder blend has been developed for rapid tooling using a direct laser sintering process. The powder consists of a mixture of different elements including Fe, C, Cu, Mo and Ni. High sintering activities were obtained by tailoring the powder characteristics and optimizing the chemical constituents. The manufacturing of complex-shaped parts is possible at rates of 6.75 cm3/h according to CAD data. The residual porosity is less than 5 vol.%. The bending strength is around 900 MPa and the artifact hardness is 490 HV30. To further improve the service life of tools, the processed parts are sintered again in a vacuum furnace at 1260 °C for 30 min. This enables to manufacture precision... 

In this paper, a double-surface plasticity model, based on a combination of a convex yield surface consisting of a failure envelope, such as a Mohr-Coulomb yield surface and, a hardening cap model, is developed for the nonlinear behaviour of powder materials in the concept of a generalized plasticity formulation for the description of cyclic loading. This model reflects the yielding, frictional and densification characteristics of powder along with strain and geometrical hardening which occur during the compaction process. The solution yields details on the powder displacement from which it is possible to establish the stress state in the powder and the densification is derived from... 

In this study, an attempt has been made to fabricate Cu-SiC nanocomposites by flake powder metallurgy and high-pressure torsion processing techniques at room temperature. Pure Cu and a mixture of Cu and nano-sized SiC powders were mechanically milled separately for 3 h and then green compacts were prepared by uniaxial pressing under 1 GPa pressure. The green compacts experienced 6-turn high-pressure torsion under a pressure of 6 GPa to prepare bulk Cu and Cu-SiC samples. The microstructures of the consolidated samples were characterized using an X-ray diffractometer and a high resolution scanning/transmission electron microscope, and the mechanical properties were evaluated by microhardness,... 

Rod-shaped samples of maraging steel were additively fabricated in vertical and horizontal directions using laser powder bed fusion technique. The samples were first aged at 490 °C for 6 h and then subjected to dynamic compressive tests using Split Hopkinson Pressure Bar apparatus. The dynamic compression tests were conducted on vertical samples at strain rates of 190, 460, 810, 1100, 1300 s−1. However, the high strain rate tests were performed at strain rates of 120, 615, 745, 890, 2200 s−1 on horizontal samples. After applying the compressive impact loads on the samples, it was found that although horizontally built samples exhibit higher dynamic strength, vertically built samples show... 

A modified plastic yield function is proposed to predict the consolidation behavior of nanostructured metal powders and metal-matrix nanocomposite powders under uniaxial compaction. The validity of the model is verified for nanocrystalline Al6063 (~100nm) alloy reinforced without and with 0.8vol.% Al2O3 nanoparticles (~25nm). The plastic deformation propensity of these powders is analyzed by linear compaction equations. The yield stress of the powder compacts is shown to be influenced by the nano-scale grains and the reinforcement nanoparticles  

Mn1.5Co1.5O4 oxide spinels are widely used as protective coatings for stainless steel interconnects within planar solid oxide fuel cell stacks. Containing both cubic and tetragonal crystalline phases, these Mn/Co oxide spinels exhibit favorable thermal stability and electronic conductivity for the SOFC interconnect application. Slurry-based coating applications of Mn/Co oxides require precursor powders, which can benefit from being nano-structured. In this study, the sol-gel synthesis of nanocrystalline Mn1.5Co1.5O4 spinel is investigated. The decomposition of sol-gel precursors, as well as the crystalline phase structures and microstructures of the product Mn1.5Co1.5O4 are characterized by... 

High strength Al-AlN composites were synthesized via high-energy milling and sintering technique. Al-X wt.% AlN (X = 0, 2.5, 5 and 10) composite powders were milled in a planetary ball mill for 25 h. Morphology, particle size distribution, crystallite size, micro-strain, and microhardness of milled powders were studied. Ball-milled powders were degassed at 400 °C for 30 min. After uniaxial cold compaction, composite compacts were sintered at 650 °C for 20, 30 and 60 min under N2 atmosphere. Effects of reinforcement content, degassing treatment and sintering time on the sinterability of powders were investigated. The results revealed that the sinterability was degraded by increasing the... 

Addition of spinel (MgAl2O4) to Al2O3-ZrO2 composite inhibits alumina grain growth and produces phase boundaries that leads to formation of a ceramic matrix composite with special mechanical properties such as high temperature superplastic deformation. However, the room temperature mechanical properties of Alumina-zirconia-magnesia spinel composite (AZM) such as fracture toughness were rarely investigated by researchers. In this research the AZM nanocomposite powders were synthesized via the solution combustion method. The dense AZM composite samples were fabricated through gelcasting process. Phase analysis studies were performed on both powder and sintered samples and the effects of spinel... 

Foaming and crystallisation behaviours of compacted glass powders based on a diopside glass-ceramic composition were investigated using the sintering route. The foaming agent was 2 wt.% SiC particles. The effect of PbO on the foaming ability of glasses was investigated. The results showed that the addition of PbO not only improved the foaming ability, by improving the wettability of the glass-SiC particles but also increased the crystallisation temperature and widened the temperature interval between the dilatometric softening point and the onset of crystallisation. The glass-SiC wetting angle was decreased from 85°for the lead-free glass, to 55°for the glass that contains 15 wt.% PbO  

In this paper, a computational algorithm is presented in three-dimensional dynamic modeling of powder compaction processes. The contact node-to-surface algorithm is employed to impose the contact constraints in large deformation frictional contact, and the contact frictional slip is modified by the Coulomb friction law to simulate the frictional behavior between the rigid punch and the work-piece. The 3D nonlinear contact friction algorithm is employed together with a double-surface cap plasticity model within the framework of large FE deformation in order to predict the non-uniform relative density distribution during the dynamic simulation of powder die-pressing. Finally, the performance... 

The uniaxial viscosity and sintering stress of WC-10Co-0·9VC (wt-%) were obtained by a loading dilatometer as functions of fractional density (0·64<ρ<0·93) and temperature (1084