Sharif Digital Repository

An efficient numerical method for simulation of casting solidification is presented. The presented method is based on a stable explicit finite difference solution of the heat equation in conjunction with the temperature recovery method to incorporate latent heat effect. The computational cost of the presented method is approximately the same as an explicit method (per time step), while it is free from the time step limitation due to the stability criterion. A simple domain decomposition method is included to improve the computational performance of the presented method. The efficiency, stability and accuracy of the presented method are supported with illustrative examples. Copyright © 2007... 

An experimental rheological study has been performed to evaluate the influence of TiC addition on the rheological behavior and stability of 316L stainless steel powder injection molding (PIM) feedstock. The effects of TiC concentration, solid loading, shear rate and temperature were investigated via capillary rheometer method. The stability of feedstocks was evaluated quantitatively using "instability index", which describes the threshold beyond which the variation of viscosity becomes unacceptable for PIM purposes. The results show that the rheological behavior of PIM feedstocks highly depends on the blend composition. The addition of TiC particles to the stainless steel powder increases... 

An analytical procedure for supersonic flutter analysis of two-dimensional panels was developed using unsteady potential flow aerodynamic theory. The local spatial influence was considered as an integral over the plate area. The U-g method was used for flutter prediction. Results indicate a stabilizing effect of the unsteady potential flow aerodynamics theory compared to the quasi-steady first-order piston theory  

A simple model is proposed to estimate the critical properties of alkanes-temperature, pressure, and volume. This model is dependent on normal boiling and molecular weight of hydrocarbons. The model has been expanded based on a Taylor series in the form of a polynomial function of normal boiling. Because methane has the simplest structure among hydrocarbons, this model has been calculated around methane. The coefficients of this model were assumed in the form of a linear function of molecular weight. These parameters can be obtained from regression between experimental results and results from this model. By a comparison of this model and previous models, it is shown that this model is... 

A convenient and efficient procedure for electrophilic aromatic bromination has been developed by mixing of N-bromosuccinimide and an aromatic compound at room temperature on the surface of silica gel mixed with solid anhydrous LiClO4. All of the substrates examined underwent clean electrophilic aromatic bromination in reaction times of a few minutes to afford the corresponding bromoarenes under neutral conditions in excellent yield. In the case of thiophenol, no substitution reaction occurred, and the corresponding disulfide was obtained in excellent yield. © 2005 NRC Canada  

The objective of this article is to study the estimation of an overall heat transfer coefficient in a partially filled rotating cylinder. Herein is an inverse analysis for estimating the overall heat transfer coefficient in an arbitrary cross-section of the aforementioned system from the temperatures measured on the shell. The material employs the finite-volume method to solve the direct problem. The hybrid effective algorithm applied here contains the local optimization algorithm to estimate the unknown parameter by minimizing the objective function. The data measured here are simulated by adding random errors to the exact solution. An investigation is made of the impact of the measurement... 

In this study the thermal calcination of two materials, high purity zinc carbonate hydroxide and the Calsimin zinc carbonate concentrate have been investigated. Isothermal studies have been performed on samples at different temperatures and times. Non-isothermal analysis has been carried out by TGA and DSC. It has been found that the calcination behaviour of both materials corresponds to the shrinking core model. The activation energy for the calcination of zinc carbonate hydroxide is found to be 88.7 kJ/mol, and that for the Calsimin sample is 97.3 kJ/mol. © 2006 Elsevier B.V. All rights reserved  

This paper presents the densification and microstructure of bilayer structures made from 316L and 17-4PH stainless steels powders during sintering. The requirements for such objects could be magnetic properties at one area of the part and non-magnetic properties at another area of the object. A pressureless solid state sintering method in conjunction with a powder layering technique was used. The sintering was carried out at temperatures ranging from 1100 to 1340 °C for 120 min in hydrogen and vacuum atmospheres. Non-isothermal sintering behavior was also examined by dilatometric analysis. It was found that the strain rate of 17-4PH stainless steel powder is higher than that of 316L during... 

In the present work, the sintering behavior of high strength Al-5.6Zn-2.5Mg-1.6Cu (in wt.%) alloy compacts was investigated. Green parts made by pressing of mixed elemental powders were sintered at different temperatures between 400 and 600°C The effect of the sintering temperature on density, dimensional change and microstructure of the Al alloy was studied. Microstructural evaluation was accompanied by XRD and DSC methods in order to determine the temperature and chemical composition of the liquid phases formed during sintering. It was found that three transient liquid phases are formed at 420, 439 and 450°C Microstructural study revealed the progressive formation of sintered contacts due... 

In this report the important factors affecting the levitation melting of nickel are discussed. The relationship between the temperature of a levitated sample to factors such as coil design, gas flow rate, power input, and sample weight are studied. Different coil designs were investigated and compared. It was found that for satisfactory sustained levitation melting, the sample weight, depending on the material, must be within a particular range. Furthermore, increasing the power input would result in a decrease in the droplet temperature; and increasing the weight of the sample results in an increase in the temperature. The flow rate of a cooling gas has a reverse relationship to the... 

The hot deformation behavior of A-286 superalloy has been characterized using hot compression experiments in the temperatures between 1000 and 1100 °C and strain rates varying between 0.001 and 0.1 s-1. In addition, hot workability of this alloy has been analyzed by employing flow-localization parameter. The results show that both kinds of softening mechanism, dynamic recovery and dynamic recrystallization, occur during hot working, where at 1000 °C the main mechanism is dynamic recovery and at higher temperatures and strain rate of 0.001-0.01 s-1 dynamic recrystallization takes place. Calculations demonstrates that this alloy mainly have a good workability for the utilized deformation... 

In this study, strain ageing during and after warm rolling of a carbon steel has been investigated. At the first step, the occurrence of serrated flow was studied by means of tensile tests at different temperatures and strain rates. In the next stage, warm rolling experiments were performed under different rolling conditions and then the samples were aged at the room temperature for a period of 3 months. For both aged and non-aged samples, tensile tests were employed to evaluate their mechanical properties. The results show that static strain ageing is possible to happen in the utilized ageing period and increases the yield stress of the aged steel. However, the samples that experience both... 

In this study, hot rolling behavior of a low alloy steel in the dual-phase region is studied. The effects of various process parameters such as initial temperature, soaking time, rolling speed and the cooling conditions are investigated. Then, mechanical testing and microstructural studies are performed and the effects of process parameters are studied and finally the optimum rolling program is determined based on the achieved results. The results show that rolling speed significantly alters the final microstructures and mechanical properties. Higher rolling speed results higher volume fraction of ferrite phase. In addition, the optimum dual-phase microstructure for this steel can be... 

An instrumented die was used to investigate the behaviour of metal powders during cold (ambient temperature) and warm (up to 140°C) compaction. This instrument enables simultaneous measurement of density, die wall friction coefficient, the triaxial stresses acting on the powder during the course of compaction and ejection pressure. Commercial iron, titanium, aluminium, 316L stainless steel (SS) and aluminium-silicon powders were employed for investigation. The results demonstrated the advantages of powder preheating on the compaction behaviour of metal powders concerning green density, dimensional changes, frictional behaviour, ejection characteristics and compactibiiity. However, the... 

Lead silicate glasses (LSGs) have high gamma-ray attenuation but low chemical durability properties. In this work, LSGs with (55.5-68.5 wt%) PbO content containing ZrO2 and TiO2 additions were produced. The chemical corrosion of various produced LSGs in 0.5 N HNO3 aqueous solution and determination of their gamma-ray attenuation coefficients for 60Co and 137Cs sources were investigated. The weight loss measurements, the SEM micrographs, the EDS analysis of the sample surfaces and the ICP analysis of solution were used to characterize the dissolution process. The effects of PbO content, ZrO2 and TiO2 additives on chemical corrosion, and also the effect of PbO on gamma-ray attenuation... 

Advanced gas turbine cycles use advanced blade cooling technologies to reach high turbine inlet temperature. Accurate modeling and optimization of these cycles depend on blade cooling model. In this study, different models have been used to simulate gas turbine performance. The first model is the continuous model and the second is stage-by-stage model with alternative methods for calculating coolant, stagnation pressure loss and SPR. Variation of specific heat and enthalpy with temperature are included in both models. The composition of gas stream in turbine is changed step by step due to air cooling. These models are validated by two case study gas turbine results, which show good agreement... 

In this work, after construction of a copper chloride laser, the effect of using different buffer gases on the output power has been examined. The voltage, current, laser pulses and the far field pattern of laser intensity were measured at the optimum buffer gas pressure. At these favorable conditions, the effect of using diaphragms in different diameters on the specific output power has been studied. By finding the desirable diaphragm size which creates the best temperature gradient in the laser tube the specific output record power of 123 (Watt/Lit) was obtained  

We report experimental evidence of Cu surface segregation in Ni/Cu system, during deposition of Ni film onto Cu substrate at room temperature and during heat treatment in vacuum. Auger electron spectroscopy (AES) and X-ray photoelectron spectroscopy (XPS) by Tougaard's analysis results show that surface segregation defeats in competition with increase in Ni thickness and terminates when thickness of Ni increase to more than 4 nm. Surface energy and concentration were calculated using contact angle measurements and the results confirm that segregation reduces the surface energy. Surface segregation during heat treatment at 150-220 °C range as a function of time initially shows linear mass... 

The hot deformation behavior of nickel-base superalloy UDIMET 720 in solution-treated conditions, simulating the forging process of the alloy, was studied using hot compression experiments. Specimens were deformed in the temperature range of 1000 °C to 1175 °C with strain rates of 10-3 to 1 s-1 and total strain of 0.8. Below 1100 °C, all specimens showed flow localization as shear band through the diagonal direction, with more severity at higher strain rates. A uniform deformation was observed when testing between 1100 °C and 1150 °C with dynamic recrystallization as the major flow softening mechanism above 1125 °C. Deformation above γ' solvus temperature was accompanied with grain boundary... 

This work presents the effect of co-sintering on the densification and microstructural evolution in the two-layer stepwise graded composite of INCONEL 718 and INCONEL 625 superalloys. A pressureless co-sintering method in conjunction with a powder layering technique was used. The sintering was carried out in solid state and liquid phase in temperature ranging from 1260 °C through 1300 °C for 60 minutes in a low pressure of an argon atmosphere. Nonisothermal sintering behavior was also examined by dilatometric analysis. Similarly, the sintering response of the individual layers was characterized. The results reveal an enhanced densification rate during co-sintering of the composite layers....