Sharif Digital Repository

Finding the optimized set of manufacturing parameters to produce strong solder-copper connections requires investigating the main and interaction effects of processing variables on the joint strength and microstructure. In this study, solder joint specimens were prepared at different levels of cooling rate, time above liquidus (TAL), and soldering temperature. Mode I fracture experiments were designed and performed at a strain rate of 0.5 s−1. The fracture load remained constant from the cooling rate of 0.1 to 1.4 °C/s and then decreased by almost 34% with further increase in the cooling rate to 34 °C/s. Increasing TAL from 60 to 120 s reduced the fracture load by almost 27%, while it was... 

Molecular dynamics (MD) simulations have been widely used to study the structure of metallic glasses (MGs) at atomic scale. However, ultrafast cooling rates in MD simulations create structures that are substantially under-relaxed. In this study, we introduce long-term pressurized annealing up to 1 μs slightly below the glass-transition temperature, Tg, in MD simulation, which effectively relaxes the structure of Cu64Zr36 MG toward experimental conditions. It is found that applying hydrostatic pressure up to 2 GPa relaxes the MG to low-energy states whereas higher pressures retard relaxation events. In the sample annealed at 2 GPa pressure, equivalent cooling rate reaches to 3.7 × 107 K/s,... 

The existence of universal semi-log linear relation between potential energy and cooling rate during the molecular dynamics simulations of metallic glasses for Cu-Zr system was formerly reported. For this purpose, different classes of metallic glasses are considered and the validity of this correlation is studied. It is shown that it holds for other thermodynamics potentials and some physical quantities like density and Wendt and Abraham parameter, too. This observation enables us to economically construct atomic scale metallic glass structures equivalent to very low cooling rates, more consistent to experimental works, not accessible using classic molecular simulations. © 2020 Elsevier B.V  

The present study investigated the effects of initial Hydrogen level and cooling rate on ultimate tensile strength of commercial Al-A319 alloys. Three hydrogen levels (0.01, 0.2, and 0.41 mL/100 grams of melt) and five cooling rate were studied. Total of 45 tensile test bars was prepared (three hydrogen levels × five cooling rate × three repeats). The UTS of the samples was determined though uniaxial tension tests. Furthermore, the microstructures of the samples were studied by standard metallographic technique and image analysis software. Finally the relationship between UTS and microstructurai features—SDAS and fraction of porosity (Fp%)—of the alloys was investigated.Results of tensile... 

Data are presented on the solidification of aluminum alloys and their macro segregation behavior. Three alloys with different solidification ranges were prepared in two temperatures. Two types of molds were also prepared by sand and metallic materials. The solidification of Al alloys were studied and the effects of four parameters were determined, including cooling rate, casting temperature, degassing and nucleation effects on solidification and a comparison was conducted to Scheil model performance. Three types of aluminum alloys (Al-12.1%Si, Al-6.9%Si and Al-4.4% Cu) with short, medium and wide solidification ranges were studied and the results showed that degassing, nucleation, increasing... 

An investigation was performed on the static strain aging behavior of warm-rolled low carbon steel during a nearly 1-year aging period, from the view point concerning with influence of changing the deformation speed and cooling media. Mechanical response of the examined material during aging period was evaluated through variations occurred in strength and hardness of the warm-deformed steel. It was shown that changing the rolling speed as well as cooling rate, may result in the occurrence of different metallurgical phenomena, consequently altering the aging kinetics of the material. It was also found that by increasing rolling speed, an increase in the value of hardness and UTS takes place,... 

In the present work, a mathematical model was developed based on finite difference method to predict the microporosity distribution in A356 aluminum alloy casting. Heat, mass, and gas conservation equations were solved in this model. Moreover, Darcy's equation was considered in the mushy zone. Results show that the distribution and concentration of microporosities in cast parts vary with both cooling rate and initial gas content. Simulation results were compared with experimental data where proportionally good agreement with experimental results was found. Finally, a complex cast part was simulated presenting the ability of the model to predict the porosities in industrial cast parts  

In this paper, effects of strain rate and mean strain on the cyclic behavior and the lifetime of aluminum-silicon alloys are investigated under thermo-mechanical and isothermal fatigue loadings. To achieve these goals, low cycle fatigue tests are accomplished at evaluated temperatures under various strain rates (by changing the loading frequency) and different strain ratios (minimum to maximum strain). Thermo-mechanical fatigue experiments are performed in an out-of-phase condition where the temperature varies between 50 and 250 °C. Various heating/cooling rates are taken into account to assess the strain rate effect and different starting temperatures are considered to study the mean strain... 

A molecular dynamics simulation study has been performed to investigate the solidification and remelting of aluminum using Sutton-Chen many body potential. Different numbers of atoms from 108 to 2048 atoms were considered to find an adequate size for the system. Three different cooling and heating rates, i.e. 10 12 K/s, 10 13 K/s and 10 14 K/s, were used. The structure of the system was examined using radial distribution function. The melting and crystallization temperatures of aluminum were evaluated by calculating the variation of heat capacity during the phase transformation. Additionally, Wendt-Abraham parameters were calculated to determine the glass transition temperature. It is shown... 

In this research, an algorithm based on the Q-state Potts model is presented for modeling the austenite to ferrite transformation. In the algorithm, it is possible to exactly track boundary migration of the phase formed during transformation. In the algorithm, effects of changes in chemical free energy, strain free energy and interfacial energies of austenite-austenite, ferrite-ferrite and austenite-ferrite during transformation are considered. From the algorithm, the kinetics of transformation and mean ferrite grain size for different cooling rates are calculated. It is found that there is a good agreement between the calculated and experimental results  

IN738LC is one of the superior nickel base superalloys utilized at high temperatures in aggressive environments. However, experiencing high temperatures and stresses during service causes microstructure deterioration and degradation of mechanical properties in this alloy. To restore the microstructure and mechanical properties of the degraded alloy, rejuvenation heat treatments can be considered. In this study, the evolution of microstructural features in a creep damaged IN738LC superalloy during different stages of rejuvenation heat treatment cycles was investigated. During solution treatment stage, dissolution of coarsened γ′ precipitates, grain boundary films and transition zone around... 

The present study investigates the evolution of γ′ precipitate microstructure in a creep damaged IN738LC superalloy during different stages of rejuvenation heat treatment cycles. Dissolution of coarsened γ′ precipitates in the creep damaged alloy occurred during different solution treatments. The precipitates that did not dissolve completely during solution treatment and those formed during subsequent cooling were considered to be as remnant and cooling precipitates respectively. It was found that higher solution treatment temperatures result in lower volume fraction of remnant precipitates and further formation of cooling precipitates. Slower cooling rates after solution treatment gave the... 

The effect of mould preheating temperature, casting modulus and graphite addition method on surface decarburisation during lost wax casting of CK 45 steel has been investigated. For this purpose, a novel image analysis program was developed to determine the carbon concentration profile. It was observed that on increasing the preheating temperature and casting modulus, the depth of decarburisation increases significantly. This behaviour was related to the decreased cooling rate of the samples which enhances the loss of carbon by reaction with the surrounding atmosphere. It was also found that the distribution of graphite in different layers of the mould and the distance of these layers from... 

The influence of thermal cycles on the properties of the coarse grained heat affected zone in X80 microalloyed steel has been investigated. The thermal simulated involved heating the X80 steel specimens to the peak temperature of 1400 °C, with different cooling rates. The four-wire tandem submerged arc welding process, with different heat input values, was used to generate a welded microstructure. The martensite/austenite constituent appeared in the microstructure of the heat affected zone region for all the specimens along the prior-austenite grain boundaries and between the bainitic ferrite laths. The blocky-like and stringer martensite/austenite morphology were observed in the heat... 

The effects of real and Gleeble simulated double pass thermal cycles on the properties of the intercritically reheated coarse grained heat affected zones in X80 microalloyed pipeline steel has been investigated. The Gleeble simulated process involved heating the X80 steel specimens to the first peak temperature of 1400°C and then reheating to the second peak temperature of 800°C, with different cooling rates. The size and area fraction of martensite/austenite (M/A) constituents were obtained by a combination of field emission scanning electron microscopes and image analysis software. In addition, misorientation was characterized by electron back-scatter diffraction analysis. It is clear that... 

This paper presents the results obtained and the deductions made from a series of microstructural studies and mechanical tests involving gray cast iron which was sand cast using a variety of modules. The effect of cooling rate on the primary dendrite arm spacing (DAS), secondary dendrite arm spacing (SDAS), thickness of ferrite-cementite layer (λe) and the hardness (HB) were evaluated. Results show that the both DAS and SDAS and also λe are highly dependent on the cooling rate, and they decreases as the cooling rate increases. More attempts were also done to correlate the HB with DAS, SDAS and λe. It was found that HB increases as DAS, SDAS and λe decreases  

The objective of this paper is to study the influence of the second peak temperature during real and simulated welding on properties of the subcritically (S), intercritically (IC) and supercritically (SC) reheated coarse grained heat affected (CGHAZ) zones. The X80 high strength pipeline microalloyed steel was subject to processing in a double-pass tandem submerged arc welding process with total heat input of 6.98 kJ/mm and thermal cycles to simulate microstructure of reheated CGHAZ zones. This involved heating to a first peak temperature (TP1) of 1400 °C, then reheating to different second peak temperatures (TP2) of 700, 800 and 900 °C with a constant cooling rate of 3.75 °C/s. Toughness of... 

It is known that the thermomechanical processing is one of the most important techniques for improving quality and mechanical properties of microalloyed steels. In this paper, the main parameters of hot forging (preheat temperature, strain and post-forging cooling rate) on the primary austenite grain size of vanadium microalloyed steel (30MSV6) were studied. From this investigation, it was found that increasing preheat temperature from 1150 °C to 1300 °C will result in a decrease in grain size number. Furthermore, it has shown that as the strain increases, the austenite grain size number increases, as is evident for the two cooling rates of 2.5 °C/s and 1.5 °C/s for primary austenite.... 

Al-20Si-5Fe melt was rapidly solidified into particles and ribbons and then consolidated to near full density by hot pressing at 400°C/250 MPa/1 h. According to the eutectic-growth and dendritic-growth velocity models, the solidification front velocity and the amount of undercooling were estimated for the particles with different sizes. Values of 0.43-1.2 cm/s and 15-28 K were obtained. The secondary dendrite arm spacing revealed a cooling rate of 6 × 105 K/s for the particles with an average size of 20 μm. Solidification models for the ribbons yielded a cooling rate of 5 × 107 K/s. As a result of the higher cooling rate, the melt-spun ribbons exhibited considerable microstructural... 

An analytical model is developed to study the effect of cooling rate on the final grain size of stirred zone of the Al5083 subjected to friction stir processing. The effect of cooling rate on the grain size of the stirred zone was investigated experimentally and numerically. A new microstructural evolution model was also suggested illustrating the mechanisms contributed in refining the microstructure. A new mechanism termed meta-dynamic recovery (MDRV) is introduced here in this regard. The simulation results also show that the rapid cooling rate resulted in superior mechanical properties through refining the microstructure of the stirred zone. However, decreasing the rotational speed and...