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Determination of essential oil components of artemisia haussknechtii boiss. using simultaneous hydrodistillation-static headspace liquid phase microextraction-gas chromatography mass spectrometry

Jalali Heravi, M ; Sharif University of Technology | 2007

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  1. Type of Document: Article
  2. DOI: 10.1016/j.chroma.2007.05.096
  3. Publisher: 2007
  4. Abstract:
  5. A novel method for extraction and analysis of volatile compounds of Artemisia haussknechtii Boiss., using simultaneous hydro-distillation and static headspace liquid microextraction followed by gas chromatography-mass spectrometry (SHD-SHLPME-GCMS) is developed. SHLPME parameters including nature of extracting solvent, headspace volume and design, extraction time, sample weight and microdrop volume were optimized. Comparison of hydro-distillation gas chromatography-mass spectrometry and HD-SHLPME-GCMS showed that the latter method is fast, simple, inexpensive and effective for the analysis of volatile compounds of aromatic plants. By using this method, 56 compounds were extracted and identified for Artemisia haussknechtii Boiss. The main constituents of its essential oil that were extracted by HD-SHLPME method, include camphor (41.01%), 1,8-cineole (32.35%), cis-davanone (3.68%), 4-terpineol (2.99%), linalool (2.84%), beta-fenchyl alcohol (2.72%), and borneol (2.58%). © 2007 Elsevier B.V. All rights reserved
  6. Keywords:
  7. Artemisia haussknechtii boiss ; Hydrodistillation (HD) ; Hydrodistillation-static headspace liquid phase microextraction (SHD-SHLPME) ; Single drop microextraction ; Alcohols ; Distillation ; Extraction ; Gas chromatography ; Mass spectrometry ; Plants (botany) ; Solvents ; Essential oils ; Alcohol derivative ; Beta fenchyl alcohol ; Borneol ; Camphor ; Cineole ; Davanone ; Essential oil ; Linalool ; Terpinen 4 ol ; Unclassified drug ; Volatile agent ; Analytic method ; Chemical composition ; Intermethod comparison ; Liquid phase microextraction ; Nonhuman ; Priority journal ; Artemisia ; Gas chromatography-mass spectrometry ; Oils, volatile ; Plant oils ; Time factors ; Artemisia haussknechtii ; Dryobalanops
  8. Source: Journal of Chromatography A ; Volume 1160, Issue 1-2 , 2007 , Pages 81-89 ; 00219673 (ISSN)
  9. URL: https://www.sciencedirect.com/science/article/abs/pii/S0021967307009120