Sharif Digital Repository

In this work, examinations on the microstructure and mechanical properties of plain carbon steel and AISI 430 ferritic stainless steel dissimilar welds are carried out. Welding is conducted in both autogenous and using ER309L austenitic filler rod conditions through gas tungsten arc welding process. The results indicate that fully-ferritic and duplex ferritic-martensitic microstructures are formed for autogenous and filler-added welds, respectively. Carbide precipitation and formation of martensite at ferrite grain boundaries (intergranular martensite) as well as grain growth occur in the heat affected zone (HAZ) of AISI 430 steel. It is found that weld heat input can strongly affect grain... 

The present study investigated the effects of initial Hydrogen level and cooling rate on ultimate tensile strength of commercial Al-A319 alloys. Three hydrogen levels (0.01, 0.2, and 0.41 mL/100 grams of melt) and five cooling rate were studied. Total of 45 tensile test bars was prepared (three hydrogen levels × five cooling rate × three repeats). The UTS of the samples was determined though uniaxial tension tests. Furthermore, the microstructures of the samples were studied by standard metallographic technique and image analysis software. Finally the relationship between UTS and microstructurai features—SDAS and fraction of porosity (Fp%)—of the alloys was investigated.Results of tensile... 

This work was carried out to investigate the effect of different Ti concentrations as a modifying agent on the microstructure and tensile properties of an in-situ Al-15 pctMg2Si composite. Cast, modified, homogenized small ingots were extruded at 753 K (480°C) at the extrusion ratio of 18:1 and ram speed of 1 mm/s. Various techniques including metallography, tensile testing, scanning electron microscopy were used to characterize the mechanical behavior, microstructural observations, fracture mechanisms of this composite. The results showed that 0.5 pctTi addition and homogenizing treatment were highly effective in modifying Mg2Si particles. The results also exhibited that the addition of Ti... 

The unique properties of NiTi alloy, such as its shape memory effect, super-elasticity and biocompatibility, make it ideal material for various applications such as aerospace, micro-electronics and medical device. In order to meet the requirement of increasing applications, great attention has been given to joining of this material to itself and to other materials during past few years. Laser welding has been known as a suitable joining technique for NiTi shape memory alloy. Hence, in this work, a comparative study on laser welding of NiTi wire to itself and to AISI 304 austenitic stainless steel wire has been made. Microstructures, mechanical properties and fracture morphologies of the... 

The variation of morphology and mechanical properties of Al6061 automotive aluminum alloy due to friction stir welding (FSW) and gas tungsten arc welding (GTAW) was investigated by optical metallography, scanning electron microscopy, microhardness measurement, X-ray diffraction, tensile testing, and fractography. The center-line dendrite emergence and microhardness reduction in the heat-affected zone were observed in the GTAW process. Although similar microhardness reduction with respect to the base metal was observed in the FSW samples, higher HVs were obtained for the FSW rather than the GTAW process at almost all heat-affected locations. Ultimate tensile strengths of the FSW and the GTAW... 

Aluminium matrix composites reinforced with submicrometre and nanosize Al 2O 3 particles were successfully manufactured in the form of sheets through eight cycles of accumulative roll bonding process. The mechanical properties of the produced composite are compared with accumulative roll bonded commercially pure aluminium. It is shown that only 1 vol.-% of submicrometre or nanosize alumina particles as reinforcement in the structure can significantly improve the yield and ultimate tensile strengths. Scanning electron microscopy revealed that particles have a random and uniform distribution in the matrix especially in the less volume fraction of alumina particles, and strong mechanical... 

As one of the key technologies for high performance electronic devices, composite solders have been recently developed to improve thermal and mechanical properties of solder joints. In this study, accumulative roll bonding process was used as an effective alternative method for manufacturing high-strength, finely dispersed, void-free and highly uniform Sn-Ag-Cu/CeO 2 nanocomposite solders. Microstructural investigation of nanocomposite solders revealed that homogenous distribution of CeO 2 nanoparticle has been achieved and the eutectic as-cast morphology of the solder changed to recrystallized fine grained structure. As a result of severe plastic deformation during rolling, brittle and... 

AISI 4340 steel bars were heated at 900 °C for one hour, annealed at 738 °C for different durations and oil-quenched in order to obtain dual phase steels with different ferrite volume fractions. A 3% prestrain at the temperature range of 150-450 °C was then imposed to the samples, and room temperature tensile tests were carried out, afterwards. Results indicate that the maximum values for both yield and ultimate tensile strength would exist for the samples pre-strained at the temperature range of 250-300 °C. Also, a sudden drop of the ductility was observed at the mentioned temperature range. The observed behavior might be attributed to the occurrence of dynamic strain aging taken place at... 

In this research, ultrahigh-molecular-weight polyethylene (UHMWPE)/multiwalled carbon nanotube (MWCNT) nanocomposites with different nanotube concentrations (0.5, 1.5, 2.5, and 3.5 wt %) were prepared via in situ polymerization with a novel, bisupported Ziegler-Natta catalytic system. Magnesium ethoxide [Mg(OEt) 2] and surface-functionalized MWCNTs were used as the support of the catalyst. Titanium tetrachloride (TiCl 4) accompanied by triethylaluminum constituted the Ziegler-Natta catalytic system. Preparation of the catalyst and the polymerization were carried out in the slurry phase under an argon atmosphere. Support of the catalyst on the MWCNTs was investigated with Fourier transform... 

High-bainite dual phase (HBDP) steels with 34. vol.% ferrite were subjected to tensile strains of 1%, 3%, and 5% at intermediate temperatures (150-450. °C). Mechanical behavior of pre-deformed steels was then investigated at room temperature. A maximum value for both yield stress and ultimate tensile strength was observed for pre-deformed steels. A minimum elongation was also found in the same pre-deformed specimens at the range of 250-350. °C. It was found that dynamic strain aging (DSA) plays the major role in mechanical properties of pre-strained HBDP steels. The DSA indicator parameter (DSAP) was introduced to evaluate DSA mechanism. Maxima of DSAP were likewise observed at the range of... 

In this study, Porous NiTi shape memory alloy has been produced by mechanical alloying of the elemental Ni and Ti powders. The compacting process was done at two temperatures (warm and cold press) and then sintering at 980 and 1050°C was performed on the specimens. Microstructure and mechanical prop-erties of the samples were investigated by optical microscopy, scanning electron microscopy (SEM) and X-ray diffraction. Moreover, shear punch test (SPT) employed to investigate the effect of compaction pressure and sintering temperature on the mechanical properties of the fabricated samples. It was revealed that warm compaction/sintering resulted in 15% yield stress improvement and 20% ultimate... 

This paper presents the effect of martensite volume fraction (VM) on mechanical properties of AISI 4340 steel with ferrite-bainite-martensite microstructures. The steel bars were austenitized at 900°C for 1h followed by intercritical annealing at 740°C for 100min and quenching into a salt bath with temperature of 300°C and holding at different times to obtain triple phase (TP) microstructures with 34vol.% fraction ferrite and various martensite (or bainite) contents. Presence of three phases in adjacent to each other was confirmed by metallographic analysis and TEM studies. TEM observation also indicates higher density of dislocations within ferrite near martensite colonies compared to that... 

A high-quality butt joint of aluminum to copper (Al/Cu) can rarely be achieved by conventional fusion and solid-state welding processes. In this research, the appropriateness of friction stir welding (FSW) for making high-quality Al/Cu welds was studied. A sound Al/Cu butt joint was achieved with relatively high strength in uni-axial tensile tests. Mechanical properties and microstructure of the sound friction stir welds were examined. The ultimate tensile strength of the joints reached about 75 percent of the aluminum base metal, with the fracture occurring at aluminum side. The metallurgical study of the welds before and after their failure in tensile tests showed that the heat affected... 

Aluminum metal-matrix nanocomposites (AMMNCs) fabricated by conventional stir-casting process usually show high porosity and poor distribution of nanoparticles within the matrix. In the current study, for the improvement of nanoparticles distribution in the aluminum matrix and enhancement of the mechanical properties, a mixture of Al/nano-Al2O3 powders were injected by pure argon gas into the molten 7075 aluminum alloy and this mixture was extruded at high temperature. Mechanical behavior of the final product was investigated by tensile and compression tests, hardness measurements, Scanning Electron Microscopy (SEM), High Resolution Transmission Electron Microscopy (HRTEM) and Optical... 

Plates of AA5052 (Al-Mg) alloy in both annealed (solution-treated) and wrought (rolled) temper conditions were subjected to friction stir processing (FSP) at various w/. v pitch ratios from 4 to 28. rev.min/mm. The role of stored strain energy on the evolution of restoration mechanisms and crystallographic texture components were assessed in terms of microstructural features evaluated using electron back-scattered diffraction (EBSD) and transmission electron microscopy (TEM) analysis. The results revealed that FSP significantly refined the grain structure and changed the crystallographic micro-texture components. The grain size of the annealed and wrought alloy was reduced from 49.4 and 9.7.... 

In-situ aluminum matrix composites were fabricated by 1-3 passes of friction stir process (FSP) using iron (Fe) particles with initial size of 10. μm. Although the initial reinforcing particles were relatively large in size and also agglomerated particles were formed in the obtained composites, all of the processed specimens fractured from the base metal during transverse tensile test. Longitudinal tensile tests revealed that the ultimate tensile strength (UTS) of the composites was up to 43% higher than that of the base metal; however, the strain to fracture of the composites reached to about 0.2. Al-Fe intermetallic compounds (IMCs) formed at the interface of the aluminum matrix and Fe... 

In this study a severe plastic deformation method called constrained groove pressing (CGP) is used for imposing a high magnitude of strain into the low carbon steel sheets. Microstructural changes during process are examined by X-ray diffraction and optical observations. The grain size evolution during severe plastic deformation is studied using Williamson-Hall analysis on XRD pattern of the deformed samples. In effective strain of 4.64, ferrite grains with a submicron size of 200-300nm are achieved. The results show that constrained groove pressing can effectively refine the coarse-grained structure to an ultra fine grain range. Mechanical properties changes due to microstructure evolution... 

Dual-phase (DP) steels with different martensite contents were produced by subjecting a low carbon steel to various heat treatment cycles. In order to investigate the effect of dynamic strain aging (DSA) on mechanical properties, tensile specimens were deformed 3% at 300 °C. Room temperature tensile tests of specimens which deformed at 300 °C showed that both yield and ultimate tensile strengths increased, while total elongation decreased. The fatigue limit increased after pre-strain in the DSA temperature range. The effects of martensite volume fraction on mechanical properties were discussed  

4340 steel bars were austenitized at 850°C for 1 hour followed by heating at 700°C (ferrite and austenite region) for 90 min and quenching into a salt bath with different temperatures of 300, 350, 400 and 450°C. The steel bars were held for 1 hour at these temperatures before air cooling to room temperature. Various ferrite-bainite microstructures with 34% volume fraction of ferrite and different bainite morphologies were obtained. The results of SEM studies showed that by increasing the austempering temperature, the morphology of bainite varies from lower to upper bainite. According to the T-T-T diagram of the studied steel, the bainite transformation will not complete for the holding time...