Sharif Digital Repository

Aluminum metal-matrix nanocomposites (AMMNCs) fabricated by conventional stir-casting process usually show high porosity and poor distribution of nanoparticles within the matrix. In the current study, for the improvement of nanoparticles distribution in the aluminum matrix and enhancement of the mechanical properties, a mixture of Al/nano-Al2O3 powders were injected by pure argon gas into the molten 7075 aluminum alloy and this mixture was extruded at high temperature. Mechanical behavior of the final product was investigated by tensile and compression tests, hardness measurements, Scanning Electron Microscopy (SEM), High Resolution Transmission Electron Microscopy (HRTEM) and Optical... 

In this research, Araldite 2011 has been reinforced using different weight fractions of Reduced Graphene Oxide (RGO). Fourier Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM) analyses were conducted and it has been shown that introduction of the RGO greatly changes the film morphology of the neat adhesive. Uni-axial tests were carried out to obtain the mechanical characteristics of the adhesive-RGO composites. It has been observed that introducing 0.5 wt% RGO enhances the ultimate tensile strength of the composites by 30%. In addition, single lap joints using neat adhesive and adhesive-RGO composites were fabricated to... 

The grain size of constrained groove pressed aluminum has been predicted through the genetic programming approach. “Sheet thickness,” “elongation,” “yield strength,” “ultimate tensile strength,” “total strain,” and “hardness,” along with “primary grain size” of the ultrafine-grained sheets were utilized as input parameters to obtain the ultimate grain size. A total number of 73 available data in the literature were gathered and randomly divided into 60 and 13 sets for algorithm training and testing, respectively. Among the presented models, the one with best performance utilized parameters of total strain, ultimate tensile strength, and primary grain size with 40 chromosomes, 10 head sizes,... 

Dual phase (DP) steels with network and fibrous martensite were produced by intercritical annealing heat treatment cycles. Some of these steels were deformed at dynamic strain aging temperatures. Room temperature tensile tests of specimens deformed at 300 °C showed that both yield and ultimate tensile strengths for both morphologies increased, while total elongation decreased. Fatigue test results before and after high temperature deformation showed that dynamic strain aging has a stronger effect on fatigue properties of dual phase steels with fibrous martensite. Cracks in DP steels with fibrous martensite propagate in a tortuous path in soft ferrite phase, while they pass of both hard and... 

In this experimental study the effect of physical and thermal properties of various FRP bars on their performance under elevated temperatures are investigated. The parameters included the bars' diameter, type of fiber, type of resin, fiber to matrix ratio, and thermal properties were studied. Moreover, ANOVA (ANalysis Of VAriance) was performed in order to investigate the contribution of each variable on the obtained results. The results showed that in addition to the temperature, the bars' diameter, type of fiber, type of resin, and thermal properties (Tg and Td) of the FRP bars have contributions to the results, while the fiber to matrix ratio was found to be an ineffective factor. It was... 

Aluminum matrix in situ nanocomposite was produced by one to six passes friction stir processing (FSP) with pre-placed Fe3O4 nanoparticles (15-20 nm). Microstructure studies showed that solid-state reactions between the aluminum matrix and Fe3O4 particles during the process led to in situ formation of Al3Fe and Al5Fe2 in the stir zone. Initial Fe3O4 as well as Al-Fe intermetallic compounds (IMCs) particles were homogeneously dispersed in a fine grain matrix after six passes of FSP. Hardness and ultimate tensile strength of the composites were increased 64 and 27%, respectively, compared to the base metal. The reasons were studied in the light of reinforcing particles distribution, formation... 

Low-carbon steel sheets are severely plastic deformed to strains of up to ≈3.48 and subsequently heat treated by conventional annealing followed by water-quenching. Four temperatures are chosen for the annealing below and over the Ac1 and Ac3 transformation lines. The effects of post-deformation heat treatment are investigated by evaluating the microstructure and mechanical properties, including strength, ductility, work hardening capability, and hardness. A maximum increase of 86% in the strength is obtained through intercritical annealing and quenching of the samples subjected to strain of 1.16. It is interesting that both the elongation and ultimate tensile strength values are higher... 

This paper presents the creep behavior of various FRP (GFRP, CFRP, and hybrid) bars in order to investigate the effects of different parameters, including the applied stress levels, bar diameter, and the type of fiber and resin in the creep behavior of FRP bars. The creep strains versus time curves were experimentally obtained for 83 days. Moreover, a statistical study, including analysis of variance (ANOVA) and linear Bayesian regression was conducted to investigate the contribution of the studied parameters. The results showed that in GFRP bars the ratio of ultimate creep strain to the initial elastic strain decreased when the applied stresses on the bars exceeded 30% of their ultimate... 

The friction stir welding of AA2024-T6 to AA6061-T6 plates with a 4 mm thickness has been studied at constant traverse and rotational speeds of 1000 rpm and 100 mm/min, respectively. The position of alloys and the effects of precipitation hardening heat treatment in retreating and advancing side in the friction stir welding were analyzed. The tool with taper threaded pin was used for welding. Macro and microstructural analysis were investigated by using Optical and Field Emission-Scanning Electron Microscopes (FE-SEM) to check out the welded joints. Micro-hardness and Tensile tests were also done to study mechanical attributes of the joints. Microstructural analysis revealed some grain... 

In this study, evolution of intermetallic layer of the cold roll bonded bilayer of Aluminum-Steel sheets, during severe plastic deformation (SPD) followed by annealing has been investigated. The effect of such evolution on mechanical properties has been discussed. For this purpose, Constrained Groove Pressing (CGP) was used as a SPD process. Field emission scanning electron microscope equipped with energy dispersive spectroscopy and optical microscopy were used for examination of intermetallic compounds morphology and composition. Meanwhile, tensile properties of the bilayer sheets were evaluated. According to microstructural observations, continuous intermetallic layer was formed during... 

This research explored the influences of shielding gases on the appearance of weld beads and the microstructures and mechanical properties of thin-wall samples using conventional gas metal arc welding as the heat source by using 5356 aluminium alloy welding wire as the raw materials and nitrogen (N2) and argon (Ar) as the shielding gases. The results showed that under the same parameters and after mono-layer single-bead welding was performed using N2 as the shielding gas, the bead height was higher, the bead width was narrower, and the penetration depth was shallower. The grain size of the thin-wall sample protected by N2 was 43.5–47.8 % smaller than that obtained under Ar protection.... 

In this research, ultrahigh-molecular-weight polyethylene (UHMWPE)/multiwalled carbon nanotube (MWCNT) nanocomposites with different nanotube concentrations (0.5, 1.5, 2.5, and 3.5 wt %) were prepared via in situ polymerization with a novel, bisupported Ziegler-Natta catalytic system. Magnesium ethoxide [Mg(OEt) 2] and surface-functionalized MWCNTs were used as the support of the catalyst. Titanium tetrachloride (TiCl 4) accompanied by triethylaluminum constituted the Ziegler-Natta catalytic system. Preparation of the catalyst and the polymerization were carried out in the slurry phase under an argon atmosphere. Support of the catalyst on the MWCNTs was investigated with Fourier transform... 

This paper presents the effect of martensite volume fraction (VM) on mechanical properties of AISI 4340 steel with ferrite-bainite-martensite microstructures. The steel bars were austenitized at 900°C for 1h followed by intercritical annealing at 740°C for 100min and quenching into a salt bath with temperature of 300°C and holding at different times to obtain triple phase (TP) microstructures with 34vol.% fraction ferrite and various martensite (or bainite) contents. Presence of three phases in adjacent to each other was confirmed by metallographic analysis and TEM studies. TEM observation also indicates higher density of dislocations within ferrite near martensite colonies compared to that... 

A high-quality butt joint of aluminum to copper (Al/Cu) can rarely be achieved by conventional fusion and solid-state welding processes. In this research, the appropriateness of friction stir welding (FSW) for making high-quality Al/Cu welds was studied. A sound Al/Cu butt joint was achieved with relatively high strength in uni-axial tensile tests. Mechanical properties and microstructure of the sound friction stir welds were examined. The ultimate tensile strength of the joints reached about 75 percent of the aluminum base metal, with the fracture occurring at aluminum side. The metallurgical study of the welds before and after their failure in tensile tests showed that the heat affected... 

Plates of AA5052 (Al-Mg) alloy in both annealed (solution-treated) and wrought (rolled) temper conditions were subjected to friction stir processing (FSP) at various w/. v pitch ratios from 4 to 28. rev.min/mm. The role of stored strain energy on the evolution of restoration mechanisms and crystallographic texture components were assessed in terms of microstructural features evaluated using electron back-scattered diffraction (EBSD) and transmission electron microscopy (TEM) analysis. The results revealed that FSP significantly refined the grain structure and changed the crystallographic micro-texture components. The grain size of the annealed and wrought alloy was reduced from 49.4 and 9.7.... 

4340 steel bars were austenitized at 850 °C for 1 h followed by heating at 700 °C for 90 min and quenching into a salt bath at the temperature range of 300-450 °C for 1 h to obtain dual structures with 34 vol.% fraction ferrite and various bainite morphologies. SEM studies showed that by increasing the austempering temperature, bainite morphology varies from lower to upper bainite. Tensile, impact and hardness tests revealed that increasing the austempering temperature from 300 to 400 °C leads to a reduction in yield and ultimate tensile strength, hardness, uniform and total elongation and impact energy. But in dual phase steel produced by austempering at 450 °C, yield and tensile strength... 

Effects of Fe particle volume percent (from 0 to 5%) and changing the tool rotation direction in each pass were studied on the microstructure evolution and mechanical properties of the in situ Al/intermetallic composites produced by three passes friction stir processing (FSP) with ∼10 µm Fe particles. Optical and scanning electron microscopes were used for the investigation of the composite homogeneity, formation of Al–Fe intermetallic compounds, and fracture surfaces. Tensile and microhardness tests were also carried out to evaluate the mechanical properties of the composites. Solid-state reactions between the aluminum matrix and Fe particles led to in situ formation of Al3Fe and Al5Fe2... 

In this study a severe plastic deformation method called constrained groove pressing (CGP) is used for imposing a high magnitude of strain into the low carbon steel sheets. Microstructural changes during process are examined by X-ray diffraction and optical observations. The grain size evolution during severe plastic deformation is studied using Williamson-Hall analysis on XRD pattern of the deformed samples. In effective strain of 4.64, ferrite grains with a submicron size of 200-300nm are achieved. The results show that constrained groove pressing can effectively refine the coarse-grained structure to an ultra fine grain range. Mechanical properties changes due to microstructure evolution... 

4340 steel bars were austenitized at 850°C for 1 hour followed by heating at 700°C (ferrite and austenite region) for 90 min and quenching into a salt bath with different temperatures of 300, 350, 400 and 450°C. The steel bars were held for 1 hour at these temperatures before air cooling to room temperature. Various ferrite-bainite microstructures with 34% volume fraction of ferrite and different bainite morphologies were obtained. The results of SEM studies showed that by increasing the austempering temperature, the morphology of bainite varies from lower to upper bainite. According to the T-T-T diagram of the studied steel, the bainite transformation will not complete for the holding time...